摘要
采用邻苯三酚与异戊醛合成了2,8,14,20-四异丁基-邻苯三酚杯[4]芳烃。运用元素分析、红外光谱、紫外光谱以及核磁共振氢谱对其结构进行了表征,并详细解析了光谱数据,证实该化合物确为目标产物,从而验证了此合成路线的可行性和可靠性。还采用循环伏安法对取代的邻苯三酚杯[4]芳烃衍生物的电化学性能进行了初步研究。
2,8,14,20- tetra-iso-butyl-Pyrogallo [4]arene was synthesized from pyrogallol and isovaleraldehyde. The structure of the product was identified by elemental analyses, IR, UV, ^1HNMR, and the spectral data were interpreted. All of these show that this compound is our target. So conclude that the method is reliable and feasible. Moreover, its electrochemical properties have been invesitigated by cyclic voltammetry.
出处
《安徽工业大学学报（自然科学版）》
CAS
2008年第1期43-45,共3页
Journal of Anhui University of Technology（Natural Science）
关键词
2
8
14
芳烃
合成
表征
电化学性能
2,8,14,20-tetra-iso-butyl-Pyrogallo [4]arene
synthesis
characterization
electrochemistry properties
作者简介
吴芳辉（1976-），女，安徽太湖人，硕士，讲师，主要研究方向：功能配合物的合成与应用。
