期刊文献+

高效液相色谱法测定茄科植物废弃物中茄尼醇 被引量:8

HPLC Determination of Solanesol in Waste of Solanaceae Plants
在线阅读 下载PDF
导出
摘要 采用高效液相色谱法对我国东北地区茄科植物废弃物马铃薯、茄子、番茄和辣椒的叶片中茄尼醇进行了定性和定量分析。结果表明:马铃薯和茄子的叶片中茄尼醇质量分数较高,分别可达到0.331%和0.207%;番茄和辣椒的叶片中茄尼醇的质量分数分别为0.092%和0.089%。方法的线性范围为0.61-6.10μg,回收率为99.5%-103.3%。 HPLC was applied to the identification and determination of solanesol in leaves of solanaceae plants (i. e. potato, eggplant, tomato and capsicum) grown in the northeastern part of our country. It was found that contents of solanesol in potato and eggplant leaves were relatively high, achieved to values of (w) 0. 331% and 0. 207% respectively and that only (w) 0. 092% and 0. 089% of solanesol were found in leaves of tomato and capsicum respectively. Linearity range of the proposed method was from 0. 61- 6. 10μg, and results of recovery test were in the range from 99. 5%-103. 3%.
出处 《理化检验(化学分册)》 CAS CSCD 北大核心 2007年第6期454-456,共3页 Physical Testing and Chemical Analysis(Part B:Chemical Analysis)
基金 科技部中德政府间合作项目(CHN03/028) 科技部科研条件升级改造项目(JG-2004-09)资助
关键词 高效液相色谱法 茄科作物 农业废弃物 茄尼醇 HPLC Solanaceae plants Agricultural waste Solanesol Leaves
作者简介 高敏(1981-),女,黑龙江哈尔滨人,主要从事天然产物化学研究。 联系人
  • 相关文献

参考文献10

二级参考文献39

  • 1孙振钧.中国生物质产业及发展取向[J].农业工程学报,2004,20(5):1-5. 被引量:171
  • 2姚文,宋爱民,栾和林.废弃烤烟中游离茄尼醇的测定[J].矿冶,1994,3(3):97-99. 被引量:7
  • 3Keca M, Gross S, Malnar I, et al. Isolation of solanesol from tobacco (Nicotiana tabacum L. ) by classic extraction and ultrasound extraction [J]. Farm Glas, 1997, 53(6) : 173-182.
  • 4Wang Z. Process and equipment for rectifying tobacco by supercritical multi-element fluid extraction [P].CN: 1302568, 2001-07-11 (CA 2001, 135 : 369346).
  • 5Yang Q, Wu J. Process for extracting solanesol [P].CN: 1294111, 2001-05-09. (CA 2001, 135 :355492).
  • 6Planta CV. Ultraviolet-absorptionsspektren von isoprenverbindungen im nahen Schumann-Gebiet [J].Helv Chim Acta, 1962, 45(1) : 84-87.
  • 7Severson R F. Ellington J J, Scholtzhauer PF, et al.Gas chromatographic method for the determination of free and total solanesol in tobacco[J]. J Chromatogr,1977, 139(2) : 269-282.
  • 8Rowland L. Flue-Cured tobacco. I. Isolation of solanesol, an unsaturated alcohol [J]. J Am Chem Soc, 1956, 78(18) : 4680-4683.
  • 9Yoshiyuki Tahara,Michiko Nagai,Katsura Kogure, et al. US 4 221 810[P] ,1980.
  • 10Shizumasa Kijima,Isao Yamatsu,Yuichi Inai, et al. US 4 175 139[P],1979.

共引文献460

同被引文献107

引证文献8

二级引证文献20

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部