摘要
本文通过温和可控的水热合成法制备出钼酸钙纳米柿子材料。并通过XRD和SEM对材料物相组成和微观形貌进行测试。结果发现,纳米柿子是由厚度70~150nm的纳米片通过有序组装形成的,组装后的纳米柿子厚度1.7~3.5μm,直径4~6μm,形貌规整且尺寸均一。该合成工艺路线有望为其他钼酸盐微/纳米材料的制备提供技术支持和实验经验。
In this paper,calcium molybdate nano-persimmon material was prepared by mild and controlled hydrothermal synthesis.The phase composition and microstructure of the material were tested by XRD and SEM.The results showed that nano-persimmons were formed by ordered assembly of nanosheets with the thickness of 70-150 nm.The assembled nano-persimmon was 1.7-3.5滋m in thickness and 4-6滋m in diameter with uniform morphology and uniform size.The synthetic route was expected to provide technical support and experimental experience for the preparation of other molybdate micro/nano materials.
作者
魏鑫杰
王莉娜
张鑫荣
WEI Xin-jie;WANG Li-na;ZHANG Xin-rong(Qian'an College,North China University of Technology,Tangshan 064400,China)
出处
《价值工程》
2018年第10期181-182,共2页
Value Engineering
基金
华北理工大学大学生创新创业训练计划(Q201701)资助项目
关键词
钼酸钙
纳米柿子
水热合成
calcium molybdate
nano-persimmon
hydrothermal synthesis
作者简介
魏鑫杰（1995-），男，山西大同人，学生，专科，研究方向为应用化工;王莉娜（1986-）（通讯作者），女，河北张家口人，讲师，硕士，研究方向为无机纳米材料制备;张鑫荣（1998-），女，河北邢台人，学生，专科，研究方向为工业分析检验。
