摘要
目的:研究桑科榕属植物瘦柄榕Ficus ischnopoda茎的化学成分。方法:采用硅胶、反相硅胶、凝胶柱色谱等方法进行分离纯化,通过理化常数和波谱分析鉴定化合物的结构。结果:从水石榴茎的95%乙醇提取物中分离并鉴定了12个化合物,分别为儿茶素(1),表儿茶素(2),芹菜素(3),licoflavone C(4),6-prenylapigenin(5),槲皮素(6),木犀草素(7),6-甲氧基-7-羟基香豆素(莨菪亭)(8),3-O-trans-p-Coumaroyltormentic Acid(9),N-trans-feruloyltyramine(10),N-trans-3,4-Odimethylcaffeoyl dopamine(11),氧化前胡素水合物(12)。结论:以上化合物均为从该植物中分离得到,其中化合物11为新天然产物。
Objective: To study the chemical constituents from the stem of Ficus ischnopoda. Method: The chemical constituents were isolated and purified by silica gel column,RP C18 and sephadex LH-20 column chromatography. Their structures were identified by physicochemical properties and spectral data. Result: The twelve components were isolated and identified as catechin (1), epicatechin (2), apigenin (3), licoflavone C (4), 6-prenylapigenin (5), quercetin (6), luteolin (7), scopleton (8), 3-O-trans-p-coumaroyltormentic acid (9), N-trans-feruloyltyramine (10), N-trans-3,4-O-dimethylcaffeoyl dopamine (11)and oxypeucedanin hydrate (12). Conclusion: All compounds were isolated from this plant for the first time, and compound 11 was isolated from the natural source for the first time
出处
《中国实验方剂学杂志》
CAS
北大核心
2013年第24期152-155,共4页
Chinese Journal of Experimental Traditional Medical Formulae
关键词
水石榴
化学成分
结构鉴定
Ficus ischnopoda
chemical constituents
structure identification
作者简介
许赞杉,硕士,从事中药化学成分与质量标准研究,Tel:021-50271708,E.mail:xzs327@126.com
[通讯作者]侴桂新,博士生导师,研究员,从事中药化学成分与质量标准研究,Tel:021-50271706,E-mail:chouguixinmsn@hotmail.com