摘要
目的:研究红海榄的化学成分。方法:利用硅胶柱色谱和葡聚糖凝胶Sephadex LH-20柱色谱进行分离纯化;采用化合物的理化性质和NMR,IR,MS等波谱方法对各单体化合物进行结构鉴定。结果:从红海榄中分离得到了7个化合物,它们分别是:β-香树脂醇(1)、豆甾醇(2)、白桦脂酸(3)、胡萝卜苷(4)、芦丁(5)、D-甘露醇(6)和六十炔烃(7)。结论:化合物1,2,3,6,7为首次从该植物中分离得到。
Objective:To study the chemical constituents of Rhizophora stylosa.Method:The constituents were isolated and purified by silica gel column chromatograph and Sephadex LH-20 column chromatograph.Their structures were elucidated through their physicochemical properties and spectroscopic analysis such as 1H-NMR,13C-NMR and FT-IR.Result: Eight compounds were isolated from R.stylosa,they were identified as β-amyrin(1),stigmasterol(2),betulinic acid(3),daucosterol(4),rutin(5),D-mannitol(6) and sixty alkyne(7).Conclusion: Compounds 1,2,3,6 and 7 were isolated from the plant for the first time.
出处
《中国实验方剂学杂志》
CAS
北大核心
2011年第2期76-79,共4页
Chinese Journal of Experimental Traditional Medical Formulae
关键词
红海榄
化学成分
结构鉴定
Rhizophora stylosa
chemical constituents
structure identification
作者简介
梁成钦,助理研究员,硕士,研究方向:天然药物化学。Tel:13788571020,E-mail:lichqixing@163.com
[通讯作者]苏小建,学士,教授级高级工程师,从事天然药物化学研究,Tel:13707835706,E-mail:xiaojiansu@163.com