摘要
目的：建立用毛细管ＧＣ法测定二妙丸、三妙丸、四妙丸中β－桉叶醇和茅术醇含量的方法。方法：以丹皮酚为内标物，用毛细管ＧＣ法对二妙丸、三妙丸、四妙丸中β－桉叶醇和茅术醇的含量进行测定。结果：对３０种成药的含量测定表明，大部分成药中含有β－桉叶醇和茅术醇，β－桉叶醇含量最高的二妙丸为Ｒ４，含量达２．９５％；三妙丸为Ｓ９，含量达３．３１％；四妙丸为Ｆ２，含量达１．３６％。茅术醇含量最高的二妙丸为Ｒ４，含量达１．３９％；三妙丸为Ｓ９，含量达２．５３％；四妙丸为Ｆ２，含量达０．９５％。结论：本法为科学评价二妙丸、三妙丸、四妙丸的质量提供了有效化学手段。
OBJECTIVE:To observe the effect of capillary used to determine the content of β-eudesmol and hinesol in Ermiao Pill,Sanmiao Pill and Simiao Pill. METHOD:β-eudesmol and hinesol content was determined,using capillary GC method.RESULT:Content determination for 30 kinds of patent medicines has indicated that most patent medicines contain β-eudesmol and hinesol.The content of β-eudesmol is R 4 in Ermiao Pill(2.95%),S9 in Sanmiao Pill(3.31%) and F2 in Simiao Pill(1.36%).The content of hinesol is R4 in Ermiao Pill(1.39%),S9 in Sanmiao Pill(2.53%) and F2 in Simiao Pill(0.95%). CONCLUSION:This determination method has provided effective means for the evaluation of the quality of Ermiao Pill,Sanmiao Pill and Simiao Pill.
出处
《南京中医药大学学报》
CAS
CSCD
1999年第1期30-32,共3页
Journal of Nanjing University of Traditional Chinese Medicine
关键词
二妙丸
三妙丸
四妙丸
Β-桉叶醇
茅术醇
Capillary GC method,Ermiao Pill,Sanmiao Pill,Simiao Pill,β-eudesmol and hinesol
