摘要
目的:建立顶空气相色谱测定一次性医疗用品中环氧乙烷残留量的方法。方法:取适量样品置于顶空瓶中,60℃恒温水浴中平衡60 min,取液上气1.0 ml进行气相色谱分析测定。结果:方法在线性范围98.3μg~491.2μg内呈良好线性关系(r=0.9999),最低检出浓度为0.1μg/g,相对标准偏差为2.3%~5.5%。结论:该方法简单、可靠,适用于一次性医疗用品中环氧乙烷残留的测定。
Objective:To establish Headspace GC amethod for disposable sanitary products.Methods:A sample was heated at headspace incubation temperature 60℃for 60 min,detected by Gas chromatography.Results:The linear ranges were 98.3 μg~491.2 μg(r=0.9999),and the detection limit was 0.1 μg/g,standard deviations were 2.3%~5.5%.Conclusion:This method is suitable,reliable and effective to determine Ethylene Qxide in disposable sanitary products.
出处
《中国卫生检验杂志》
CAS
2010年第6期1345-1346,共2页
Chinese Journal of Health Laboratory Technology
关键词
环氧乙烷
顶空气相色谱
一次性医疗用品
Ethylene qxide
Headspace
Gas chromatography
Disposable sanitary products
作者简介
杨君,女,副主任技师,主要从事卫生理化检验工作。