摘要
为实现导电银浆中银粉含量的快速测定,并确保实验室对该产品测试分析结果的准确性,本文建立了一种硝酸直接消解法滴定测试导电银浆中银粉含量的方法,并分析了滴定法测定导电银浆中银粉含量的不确定度来源.结果表明,该导电银浆中银含量为(87.90±0.30)%(k=2).该方法具有操作简单快速、准确度高等特点,适用于导电银浆中银含量的快速测定.
In order to realize the rapid determination of silver powder in conductive silver paste and ensure the accuracy of laboratory test and analysis results of the related product,a method of titrating silver powder in conductive silver paste by direct digestion with nitric acid was established.The source of uncertainty in the determination of silver powder in conductive silver paste by titration was also analyzed.The results showed that the silver content of the conductive silver paste was(87.90±0.30)%(k=2).This method is simple,fast,accurate,and suitable for the rapid determination of silver powder in conductive silver paste.
作者
贾祺
许丹
侯颖
王亮亮
李曼
徐晓元
关红艳
关荣
JIA Qi;XU Dan;HOU Ying;WANG Liang-Liang;LI Man;XU Xiao-Yuan;GUAN Hong-Yan;GUAN Rong(China Testing&Certification International Group Co.,Ltd.,Beijing 100024;Science and Technology Research Center of China Customs,Beijing 100026)
出处
《中国口岸科学技术》
2022年第S02期64-68,共5页
China Port Science and Technology
关键词
导电银浆
滴定
不确定度
conductive silver paste
titration
uncertainty
作者简介
第一作者:贾祺(1993—),男,汉族,山西原平人,硕士,工程师,主要从事材料的化学成分分析,E-mail:jiaqi@ctc.ac.cn;通讯作者:关荣(1981—),女,汉族,陕西咸阳人,学士,工程师,主要从事进出口商品检验,E-mail:xueren_0002@163.com
