FeCrAl(f)/HA biological functionally gradient materials(FGMs) were successfully fabricated by the hot pressing technique.Scanning electron microscope(SEM),energy dispersive spectrometer(EDS) and bending strength test ...FeCrAl(f)/HA biological functionally gradient materials(FGMs) were successfully fabricated by the hot pressing technique.Scanning electron microscope(SEM),energy dispersive spectrometer(EDS) and bending strength test machine were utilized to characterize the microstructure,component,mechanical properties and the formation of the Ca-deficient apatite on the surface of these materials.The results indicate that an asymmetrical FeCrAl(f)/HA FGM,consolidating powders prepared by mixing HA with 3%–15%(volume fraction) is successfully prepared.Both of the matrix and FeCrAl fiber are integrated very tightly and bite into each other very deeply.And counter diffusion takes place to some extent in two phase interfaces.The elemental compositions of the FeCrAl(f)/HA FGM change progressively.Ca and P contents increase gradually with immersion time increasing,and thereafter approach equilibrium.The bone-like apatite layer forms on the materials surface,which possesses benign bioactivity,and the favorable biocompatibility can provide potential firm fixation between FeCrAl(f)/HA asymmetrical FGM implants and human bone.展开更多
为解决激光定向能量沉积(laser-directed energy deposition,L-DED)成型工艺制备的镍钴基功能梯度材料(NiCo-FGMs)磨削后表面质量一致性较差这一问题,基于正交试验分析了磨削工艺参数对NiCo-FGMs的磨削力和表面粗糙度的影响规律,并建立...为解决激光定向能量沉积(laser-directed energy deposition,L-DED)成型工艺制备的镍钴基功能梯度材料(NiCo-FGMs)磨削后表面质量一致性较差这一问题,基于正交试验分析了磨削工艺参数对NiCo-FGMs的磨削力和表面粗糙度的影响规律,并建立相应的预测模型.针对粗加工与精加工的不同加工目标,利用第二代非支配排序遗传算法(NSGA-Ⅱ)结合熵权法与逼近理想解的排序方法即熵权TOPSIS(technique for order proference by similarity to ideal solution)法进行了多目标磨削工艺参数优化,并进行验证.结果表明:粗加工磨削参数采用a_(p)=53.61μm,v_(s)=29.99 m/s,v_(w)=311.89 mm/min;精加工磨削参数采用ap=14.96μm,v_(s)=29.99 m/s,v_(w)=300.92 mm/min.经两道工序加工,表面粗糙度标准差从0.195μm降至0.101μm,有效提高NiCo-FGMs的表面粗糙度一致性.展开更多
基金Project(51274247)supported by the National Natural Science Foundation of ChinaProject(2012BAE06B00)supported by the National High Technology Research and Development Program to China+1 种基金Project(2011QNZT046)supported by the Fundamental Research Funds of Central South Universities of ChinaProject supported by Hunan Postdoctoral Scientific Program,China
文摘FeCrAl(f)/HA biological functionally gradient materials(FGMs) were successfully fabricated by the hot pressing technique.Scanning electron microscope(SEM),energy dispersive spectrometer(EDS) and bending strength test machine were utilized to characterize the microstructure,component,mechanical properties and the formation of the Ca-deficient apatite on the surface of these materials.The results indicate that an asymmetrical FeCrAl(f)/HA FGM,consolidating powders prepared by mixing HA with 3%–15%(volume fraction) is successfully prepared.Both of the matrix and FeCrAl fiber are integrated very tightly and bite into each other very deeply.And counter diffusion takes place to some extent in two phase interfaces.The elemental compositions of the FeCrAl(f)/HA FGM change progressively.Ca and P contents increase gradually with immersion time increasing,and thereafter approach equilibrium.The bone-like apatite layer forms on the materials surface,which possesses benign bioactivity,and the favorable biocompatibility can provide potential firm fixation between FeCrAl(f)/HA asymmetrical FGM implants and human bone.
文摘为解决激光定向能量沉积(laser-directed energy deposition,L-DED)成型工艺制备的镍钴基功能梯度材料(NiCo-FGMs)磨削后表面质量一致性较差这一问题,基于正交试验分析了磨削工艺参数对NiCo-FGMs的磨削力和表面粗糙度的影响规律,并建立相应的预测模型.针对粗加工与精加工的不同加工目标,利用第二代非支配排序遗传算法(NSGA-Ⅱ)结合熵权法与逼近理想解的排序方法即熵权TOPSIS(technique for order proference by similarity to ideal solution)法进行了多目标磨削工艺参数优化,并进行验证.结果表明:粗加工磨削参数采用a_(p)=53.61μm,v_(s)=29.99 m/s,v_(w)=311.89 mm/min;精加工磨削参数采用ap=14.96μm,v_(s)=29.99 m/s,v_(w)=300.92 mm/min.经两道工序加工,表面粗糙度标准差从0.195μm降至0.101μm,有效提高NiCo-FGMs的表面粗糙度一致性.
