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Microstructure and mechanical properties of Al-Zn-Cu-Mg-Sc-Zr alloy after retrogression and re-aging treatments 被引量:8
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作者 李文斌 潘清林 +2 位作者 肖艳苹 何运斌 刘晓艳 《Journal of Central South University》 SCIE EI CAS 2011年第2期279-284,共6页
The mechanical properties and stress corrosion cracking (SCC) resistance of an Al-Zn-Cu-Mg-Sc-Zr alloy under different aging conditions were investigated. The dependence of microstrueture and mechanical properties o... The mechanical properties and stress corrosion cracking (SCC) resistance of an Al-Zn-Cu-Mg-Sc-Zr alloy under different aging conditions were investigated. The dependence of microstrueture and mechanical properties on aging parameters was evaluated by tensile test, hardness test and conductivity measurement. The results show that for the alloys with retrogression and re-aging treatment (RRA), the conductivity increases with the retrogression time and temperature, while the tensile strength decreases. The transmission electron microscopy (TEM) results show that the precipitates η(MgZn2) at grain boundary aggregate apparently with retrogression time and the precipitates inside the matrix exhibit the similar distribution to T6 temper, which comprises fine GP zones, large η'(MgZn2)and η(MgZn2) phases. According to the mechanical properties and microstructure observations, the optimal RRA regime is recommended to be 120℃, 24h + 180 ℃, 30 min + 120 ℃, 24 h. The strength level of the alloy after the optimum RRA treatment is similar to that in T6 condition and the SCC resistance is improved obviously in contrast to T6 condition. 展开更多
关键词 Al-Zn-Cu-Mg-Sc-Zr alloy retrogression and re-aging treatment microstructure mechanical properties stress corrosioncracking
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Physical and mechanical properties of Beishan granite after different high temperature treatments 被引量:4
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作者 WANG Zi-hui ZHOU Hong-wei +2 位作者 HEINZ Konietzky LI Shu-min WANG Ting-zheng 《Journal of Central South University》 SCIE EI CAS CSCD 2022年第6期1957-1972,共16页
In China,Beishan granite is chosen as a potential host surrounding rock of a high-level radioactive waste(HLW)repository.For this research,Beishan granite specimens were heated up to 300℃,400℃ and 500℃,respectively... In China,Beishan granite is chosen as a potential host surrounding rock of a high-level radioactive waste(HLW)repository.For this research,Beishan granite specimens were heated up to 300℃,400℃ and 500℃,respectively.And conventional triaxial compression tests were conducted after cooling down the samples.The results show that after 300℃,400℃ and 500℃ heating treatment,the diameter of samples increases by 0.066%,0.143%and 0.409%,respectively,which is a little larger than the axial length changes.Mechanical tests show that peak strength increases slightly with increasing temperature.However,the dilatancy threshold is lower than that observed for samples which have not experienced heating treatment.Peak strain and dilatancy threshold strain show a strong temperature dependence.The higher the temperature,the greater the strain.Furthermore,increasing temperature has negative influence on threshold elastic modulus E_(c) and tangent elastic modulus E_(t).Poisson ratio decreases when temperature increases from 300℃ to 500℃,but it is still larger than that observed for samples which have not experienced heating treatment.In addition,AE monitoring shows a quiet period in the initial loading stage,which proves that the micro cracks are closed during heating and contribute to the increase of peak strength. 展开更多
关键词 Beishan granite heating treatment DEFORMATION thermo-mechanical properties acoustic emission
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EFFECT OF HEAT TREATMENTS ON TENSILE PROPERTIES AND MICROSTRUCTURE OF 2195 ALLOY 被引量:3
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作者 Zheng Ziqiao Huang Biping(Department of Materials Science and Engineering, Central South University of Technology, Changsha 410083, China) 《Journal of Central South University》 SCIE EI CAS 1998年第1期15-18,共4页
EFFECTOFHEATTREATMENTSONTENSILEPROPERTIESANDMICROSTRUCTUREOF2195ALLOY*ZhengZiqiaoHuangBiping(DepartmentofMat... EFFECTOFHEATTREATMENTSONTENSILEPROPERTIESANDMICROSTRUCTUREOF2195ALLOY*ZhengZiqiaoHuangBiping(DepartmentofMaterialsScienceandE... 展开更多
关键词 2195 ALLOY AGING treatment TENSILE PROPERTIES MICROSTRUCTURE
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Research on the intermediate phase of 40CrMnSiB steel shell under different heat treatments 被引量:1
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作者 Wei-bing Li Zhi-chuang Chen +1 位作者 Xiao-ming Wang Wen-bin Li 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2021年第3期1032-1041,共10页
In this study, 40 Cr Mn Si B steel cylindrical shells were tempered at 350, 500 and 600 ℃ to study the effect of tempering temperature on the dynamic process of expansion and fracture of the metal shell. A midexplosi... In this study, 40 Cr Mn Si B steel cylindrical shells were tempered at 350, 500 and 600 ℃ to study the effect of tempering temperature on the dynamic process of expansion and fracture of the metal shell. A midexplosion recovery experiment for the metal cylinder under internal explosive loading was designed, and the wreckage of the casings at the intermediate phase was obtained. The effects of different tempering temperatures on the macroscopic and microscopic fracture characteristics of 40 Cr Mn Si B steel were studied. The influence of tempering temperatures on the fracture characteristic parameters of the recovered wreckage were measured and analyzed, including the circumferential divide size, the thickness and the number of the circumferential divisions. The results show that as the tempering temperature was increased from 350 to 600 ℃, at first, the degree of fragmentation and the fracture characteristic parameters of the recovered wreckage changed significantly and then became essentially consistent. Scanning electron microscopy analysis revealed flow-like structure characteristics caused by adiabatic shear on different fracture surfaces. At the detonation initiation end of the casing, fracturing was formed by tearing along the crack, which existed a distance from the initiation end and propagated along the axis direction. In contrast, the fracturing near the middle position consists of a plurality of radial shear fracture units. The amount of alloy carbide that was precipitated during the tempering process increased continuously with tempering temperature, leading to an increasing number of spherical carbide particles scattered around the fracture surface. 展开更多
关键词 Explosive mechanics Mid-explosion recovery experiment Explosion and fracture Heat treatment SEM(Scanning electron microscope)fracture analysis
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Spectroscopic Evaluation of Effects of Heat Treatments on the Structures and Emulsifying Properties of Caseins
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作者 ZHANG Hao WANG Peng-jie +4 位作者 LEI Xin-gen YANG Hong-ju ZHANG Lu-da REN Fa-zheng ZHENG Li-min 《光谱学与光谱分析》 SCIE EI CAS CSCD 北大核心 2013年第5期1275-1280,共6页
The effects of heat treatment(heating temperature and pH) on the structures and emulsifying properties of caseins were systematically studied by spectroscopy.Heat treatment from 60to 100℃resulted in an increase in th... The effects of heat treatment(heating temperature and pH) on the structures and emulsifying properties of caseins were systematically studied by spectroscopy.Heat treatment from 60to 100℃resulted in an increase in their fluorescence intensity,hydrodynamic diameter,turbidity and emulsifying activity index,but decreased the size polydispersity of caseins.In the pH range of 5.5to 7.0,the fluorescence intensity,hydrodynamic diameter,turbidity and emulsifying properties decreased with increased heating pH,but the size polydispersity of caseins increased with increased pH.The relationship between the surface fluorescence intensity and emulsifying activity was also investigated,revealing a correlation coefficient of 0.90.These results suggested that heat treatment could be used to modify the structures and emulsifying properties of caseins by appropriately selecting heating conditions. 展开更多
关键词 CASEINS Heat treatment STRUCTURES Emulsifying properties Fluorescence spectrometry Dynamic light scattering TURBIDITY
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Cotton seed management:traditional and emerging treatment approaches for enhanced productivity
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作者 MYLSAMY Preethi TAMILMANI Eevera +2 位作者 VENUGOPAL Rajanbabu MURUGAIYAN Senthilkumar RANGANATHAN Umarani 《Journal of Cotton Research》 2025年第1期143-161,共19页
Cotton,a crucial commercial fibre crop,depends heavily on seed-associated characteristics like germination rate,vigour,and resistance to post-harvest deterioration for both production and lint quality.Serious cellular... Cotton,a crucial commercial fibre crop,depends heavily on seed-associated characteristics like germination rate,vigour,and resistance to post-harvest deterioration for both production and lint quality.Serious cellular damage dur-ing post-harvest processes such as delinting,prolonged seedling emergence periods,decreased viability,increased susceptibility to infections,and lipid peroxidation during storage pose serious problems to seed quality.The perfor-mance of seeds and total crop productivity are adversely affected by these problems.Traditional methods of seed improvement,like physical scarification and seed priming,have demonstrated promise in raising cotton seed vigour and germination rates.Furthermore,modern approaches including plasma therapies,magnetic water treatments,and nanotechnology-based treatments have shown promise in improving seed quality and reducing environmen-tal stresses.By offering sustainable substitutes for conventional approaches,these cutting-edge procedures lessen the need for fungicides and other agrochemicals that pollute the environment.This review explores various con-ventional and emerging strategies to address the detrimental factors impacting cotton seed quality.It emphasizes the importance of integrating classical and advanced approaches to enhance germination,ensure robust crop estab-lishment,and achieve higher yields.In addition to promoting sustainable cotton production,this kind of integration helps preserve the ecosystem and create resilient farming methods. 展开更多
关键词 Cotton Seed vigour Physical scarification Seed priming Plasma treatment Magnetic water treatments Nanotechnology-based treatments
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Super Adsorption Behavior of Electrospinning-derived Porous Carbon Nanofibers towards Methyl Blue
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作者 JIANG Zhong-wei LI Xia-chu-qin +2 位作者 HU Cong-yi LI Yuan-fang HUANG Cheng-zhi 《分析测试学报》 北大核心 2025年第9期1878-1888,共11页
Adsorption as an effective technique for the remediation of wastewater has been widely used in industrial wastewater treatment due to the advantage of cost-effectiveness,availability of the adsorbent and ease of opera... Adsorption as an effective technique for the remediation of wastewater has been widely used in industrial wastewater treatment due to the advantage of cost-effectiveness,availability of the adsorbent and ease of operation.However,the low adsorption capacity of the reported adsorbents is still a challenge for wastewater treatment with highefficiency.Here,we developed a super adsorbent(SUA-1),which was a kind of porous carbon nanofibers derived from a composite of PAN-based electrospinning and ZIF-8(PAN/ZIF-8)via simple heat treatment process.The asprepared SUA showed an ultra-high adsorption capacity for adsorbing methyl blue(MB)at nearly three times its own weight,as high as 2998.18 mg/g.A series tests demonstrated that the pore-making effect of ZIF-8 during heat treatment process endowed high BET surface area and generated ZnO components as chemical adsorption center.Under the synergistic effect of bonding and non-bonding forces including ionic bond,electrostatic interaction,andπ-πinteraction,the adsorption capacity has been greatly improved.In view of promising efficiency,this work provides guidance and insights for the preparation of highly efficient adsorbents based on electrospinning derived porous carbon nanofibers. 展开更多
关键词 ELECTROSPINNING porous carbon nanofibers pore-making effect wastewater treatment ADSORPTION
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Domestic research on extra-gastrointestinal stromal tumors:A ten-year review
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作者 WANG Shengjin SUN Feng WANG Xinghong 《中南大学学报(医学版)》 北大核心 2025年第2期237-250,共14页
Objective:There is currently no consensus on whether extra-gastrointestinal stromal tumors(EGISTs)and gastrointestinal stromal tumors(GISTs)are the same type of tumor,and whether the diagnosis and treatment of EGISTs ... Objective:There is currently no consensus on whether extra-gastrointestinal stromal tumors(EGISTs)and gastrointestinal stromal tumors(GISTs)are the same type of tumor,and whether the diagnosis and treatment of EGISTs can directly replicate the current diagnostic and treatment standards for GISTs.This study aims to further elucidate the clinical and pathological characteristics,diagnosis,treatment,and prognosis of EGISTs by analyzing the research results of domestic scholars in the field of EGISTs in the past decade.Methods:A review was conducted on original Chinese and English research articles published from 2013 to 2022 focusing on EGISTs.A descriptive approach was used to extract key information from the literature,including patient demographics,tumor location,tumor diameter,mitotic figures,risk stratification,immunohistochemical markers,cell type,and prognostic factors.The data were subjected to statistical analysis.Results:A total of 12 articles containing 780 EGIST patients were included.The male-to female incidence of EGISTs was 0.92꞉1.The most common sites of EGISTs were mesentery(30.96%),peritoneum or retroperitoneum(28.53%),omentum(20.32%),and pelvic cavity(12.52%).52.77%of EGISTs had tumor diameters greater than 10 cm,and the proportions of EGISTs with nuclear fission patterns greater than 5/50 high power field(HPF)and greater than 10/50 HPF were 51.24%and 26.11%,respectively.The proportion of high-risk EGISTs was 79.05%.The positive rates of immune markers CD117,CD34,and DOG-1 in EGISTs were 82.3%,69.0%,and 79.5%,respectively.The proportion of Ki-67>5%was 49.2%,and the proportion of Ki-67>10%was 24.8%.The proportions of EGISTs in spindle cells,epithelial cells,and mixed cells were 74.4%,14.8%,and 13.1%,respectively.The diameter of the tumor,resection method,risk level,Ki-67 index,mitotic counts,presence of rupture/bleeding/necrosis/peripheral tissue invasion/recurrence and metastasis,as well as the use of imatinib treatment after surgery were important factors affecting the prognosis of EGISTs.Conclusion:Current medical research is relatively well cognizant of GISTs with primary sites in the gastrointestinal tract.Compared with GISTs,EGISTs have large tumor diameters,high mitotic counts,a high percentage of high-risk grades,relatively unique molecular expression,and high aggressiveness.EGISTs differ from GISTs in clinicopathological characteristics.Whether EGISTs and GISTs share a common origin remains unclear.If they are distinct tumor entities,separate diagnostic and treatment guidelines for EGISTs should be established.If EGISTs are ultimately confirmed to be a special subtype of GISTs,then directly applying existing GIST-based standards to EGISTs may be inappropriate.A more scientific approach would involve subclassifying EGISTs based on anatomical location and then tailoring treatment strategies accordingly with reference to GIST guidelines. 展开更多
关键词 extra-gastrointestinal stromal tumors gastrointestinal stromal tumors pathological features DIAGNOSIS treatment PROGNOSIS
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Roles of Sn-promoter and carbon nanotubes treatment on supported CoB catalysts for hydrogen production
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作者 SHI Limin LI Yanbo +2 位作者 LEI Qiang REN Rongzhi WANG Yujing 《燃料化学学报(中英文)》 北大核心 2025年第5期703-712,共10页
Carbon nanotubes(CNTs)supported CoB and CoBSn catalysts were synthesized for hydrogen production via NaBH4 hydrolysis.The roles of Sn-promoter and the effect of CNTs treatment on CoB catalysts were evaluated and discu... Carbon nanotubes(CNTs)supported CoB and CoBSn catalysts were synthesized for hydrogen production via NaBH4 hydrolysis.The roles of Sn-promoter and the effect of CNTs treatment on CoB catalysts were evaluated and discussed.It is found that after the addition of Sn promoter,the specific surface area and the generation of active CoB phase are increased,while the oxidation treatment of CNTs results in more loading amounts of active components and enrichment of electron at active sites as well as large surface area.Consequently,the Sn-doped CoB catalysts supported on CNTs with oxidation treatment exhibits a significantly improved activity with a high H_(2)generation rate of 2640 mL/(min·g).Meanwhile,this catalyst shows a low activation energy of 43.7 kJ/mol and relatively high reusability. 展开更多
关键词 sodium borohydride hydrolysis CoB-based catalysts Sn promoter carbon nanotubes oxidation treatment
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Toric-ICL shows better predictability and efficacy than FSLASIK for myopia correction in patients with moderate to high myopia and astigmatism
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作者 LI Hongyang LIAO Wenxiong +7 位作者 LEI Peng YANG Chunyuan LI Yanying XUE Liping TAN Duo LIU Sijing WU Yi CHEN Meilan 《南方医科大学学报》 北大核心 2025年第6期1113-1121,共9页
Objective To compare the efficacy of toric implantable collamer lens(Toric-ICL)and femtosecond laser-assisted in situ keratomileusis(FS-LASIK)for myopia correction in patients with moderate to high myopia complicated ... Objective To compare the efficacy of toric implantable collamer lens(Toric-ICL)and femtosecond laser-assisted in situ keratomileusis(FS-LASIK)for myopia correction in patients with moderate to high myopia complicated with astigmatism.Methods We retrospectively collected data from 64 patients(aged 18-42 years)with moderate to high myopia complicated with astigmatism(128 eyes)undergoing either Toric-ICL(28 patients/56 eyes)or FS-LASIK(36 patients/72 eyes)at our department between January,2019 and December,2020.The changes of uncorrected distance visual acuity(UCVA),spherical equivalent(SE),mean astigmatism correction index(CI),corneal endothelial cell density(ECD)and intraocular pressure(IOP)following the procedures were compared between the two groups.Results In FS-LASIK group,all the eyes(72/72)achieved an UCVA≥1.0,similar to the rate in Toric-ICL group(55/56 eyes;P=0.2374).The postoperative SE was also comparable between FS-LASIK and Toric-ICL groups[0.43±0.06 D(range:-1.0 to 1.50 D)vs 0.38±0.05 D(range:-0.75 to 1.00 D);P=0.56].The mean astigmatism CI was significantly higher in FS-LASIK group than in Toric-ICL group(0.8561 vs 0.7176;P<0.0001),and 88.89%of the eyes in FS-LASIK group and 69.64%in Toric-ICL group had postoperative astigmatism≤0.50 D.No significant changes were observed in postoperative corneal ECD in FS-LASIK group,whereas ECD decreased significantly after the procedure in Toric-ICL group(P=0.0057).The patients undergoing Toric-ICL exhibited no significant changes of postoperative IOP,but the patients receiving FS-LASIK had significantly reduced IOP after the procedure(P<0.001).Conclusion Although the patients included in Toric-ICL group had higher myopia and astigmatism,Toric-ICL still showed better predictability and efficacy for astigmatic correction in Toric-ICL group.Toric-ICL is an effective and safe equivalent of FS-LASIK for correcting moderate myopia but can be more advantageous for correcting high myopia with astigmatism. 展开更多
关键词 toric implantable collamer lens femtosecond laser-assisted in situ keratomileusis MYOPIA ASTIGMATISM treatment effect
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Immunoregulatory Role of In vitro-induced Regulatory T Cells in The Treatment of Ischemic Stroke
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作者 MA Yin-Zhong 《生物化学与生物物理进展》 北大核心 2025年第4期803-803,共1页
Kang et al.published a research article on the treatment of ischemic stroke using engineered Treg cells(Kang et al.,Prog Biochem Biophys,2025,52(4):946-956.DOI:10.16476/j.pibb.2025.0019).Their study mainly explores th... Kang et al.published a research article on the treatment of ischemic stroke using engineered Treg cells(Kang et al.,Prog Biochem Biophys,2025,52(4):946-956.DOI:10.16476/j.pibb.2025.0019).Their study mainly explores the immunoregulatory role of regulatory T(Treg)cells in ischemic stroke,providing an innovative therapeutic strategy.Neuroinflammation is a major driver of secondary injury after stroke.Existing treatments focus on vascular recanalization while neglecting immune regulation.Their study proposes to modulate neuroinflammation through in vitro-induced Treg cells,offering a novel approach distinct from traditional thrombolysis and endovascular interventions. 展开更多
关键词 therapeutic strategyneuroinflammation NEUROINFLAMMATION immune regulationtheir regulatory T cells treatment ischemic stroke engineered treg cells kang vascular recanalization ischemic stroke
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美国《保健物理》(Health Physics)杂志英文摘要(2025年128卷第6期)
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《辐射防护》 北大核心 2025年第5期539-544,共6页
Evaluation of Gamma Index Analysis for Detecting Errors in Patient-specific Quality Assurance in Intensity Modulated Radiotherapy Taylan Tugrul1(1.Department of Radiation Oncology,Medicine Faculty of Van Yüzü... Evaluation of Gamma Index Analysis for Detecting Errors in Patient-specific Quality Assurance in Intensity Modulated Radiotherapy Taylan Tugrul1(1.Department of Radiation Oncology,Medicine Faculty of Van YüzüncüYıl University,Van,Turkey)Abstract:Quality assurance practices performed before treatment are believed to identify various potential errors.In this study,2-dimensional(2D)dosimetric results were analyzed by making some intentional mistakes in six different treatment plans.In this way,the detectability of errors was investigated.In all segments of all treatment plans,one of the multileaf collimators was kept fixed at different positions on the central axis.In addition to multileaf collimators error,gantry error was also examined in the study.The dose distribution results obtained by Treatment Planning System(TPS)were compared with those obtained by the 2D array device,both as local calculation and global calculation methods,using the gamma analysis method.When the results are examined in the case where the Multi-leaf collimators(MLC)is fixed at the 1 cm position. 展开更多
关键词 making some intentional mistakes six different treatment plansin multileaf collimators patient specific quality assurance gantry error intensity modulated radiotherapy assurance practices gamma index analysis
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Anisotropy of rapidly solidified 2195 alloy rolled sheets:Effect of pre-thermal treatment prior to rolling and aging treatment
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作者 PENG Xiang LI Xin-xing +3 位作者 WANG Ri-chu FENG Yan YAN Shuai-jiang CAI Zhi-yong 《Journal of Central South University》 2025年第5期1660-1677,共18页
The pronounced anisotropy in mechanical properties presents a major obstacle to the extensive application of aluminum-lithium(Al-Li)alloys,primarily attributed to heterogeneous precipitate distribution,grain structure... The pronounced anisotropy in mechanical properties presents a major obstacle to the extensive application of aluminum-lithium(Al-Li)alloys,primarily attributed to heterogeneous precipitate distribution,grain structure variations,and crystallographic texture.This study investigates the impact of pre-thermal treatment prior to hot rolling and aging treatment on the anisotropy of mechanical properties of 2195 alloy sheet fabricated by gas atomization,hot pressing and hot rolling.The results demonstrate that pre-treatment at 450℃for 4 h promotes finer and more uniform distribution of precipitates,effectively mitigating mechanical anisotropy of the alloy sheet.Additionally,this treatment facilitates recrystallization during hot rolling,further reducing mechanical anisotropy.The in-plane anisotropy(IPA)factors for ultimate tensile strength(UTS)and yield strength(YS)are 1.15%and 0.77%,respectively.Subsequent aging treatment enhances grain refinement and the uniformity of the T_(1) phase,suppresses the formation of precipitation-free zones(PFZs),significantly improving the strength and toughness of the alloy sheet.After peak aging at 165℃for 48 h,the alloy sheet exhibits YS of 547 MPa,UTS of 590 MPa,and elongation(EL)of 7.7%. 展开更多
关键词 aluminum-lithium alloy hot rolling pre-thermal treatment ANISOTROPY aging treatment
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Continuous-flow columns packed with zero-valent iron and iron sulfide as a feasible strategy to remediate the persistent contaminant nitroguanidine
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作者 Youngjae Yu Erika E.Rios-Valenciana +3 位作者 Robert A.Root Reyes Sierra-Alvarez Jon Chorover Jim A.Field 《Defence Technology(防务技术)》 2025年第1期26-34,共9页
The insensitive munitions compound nitroguanidine(NQ)is used by the U.S.Army to avoid unintended explosions.However,NQ also represents an emerging contaminant whose environmental emissions can cause toxicity toward aq... The insensitive munitions compound nitroguanidine(NQ)is used by the U.S.Army to avoid unintended explosions.However,NQ also represents an emerging contaminant whose environmental emissions can cause toxicity toward aquatic organisms,indicating the need for effective remediation strategies.Thus,we investigated the feasibility of treating water contaminated with NQ in continuous-flow columns packed with zero-valent iron(ZVI)or iron sulfide(FeS).Initially,the impact of pH on NQ transformation by ZVI or FeS was evaluated in batch experiments.The pseudo first-order rate constant for NQ transformation(k_(1,NQ))by ZVI was 8-10 times higher at pH 3.0 compared to pH 5.5 and 7.0,whereas similar k_(1,NQ)values were obtained for FeS at pH 5.5-10.0.Based on these findings,the influent p H fed to the ZVIand Fe S-packed columns was adjusted to 3.0 and 5.5,respectively.Both reactors transformed NQ into nitrosoguanidine(Nso Q).Further transformation of Nso Q by ZVI produced aminoguanidine,guanidine,and cyanamide,whereas Nso Q transformation by Fe S produced guanidine,ammonium,and traces of urea.ZVI outperformed Fe S as a reactive material to remove NQ.The ZVI-packed column effectively removed NQ below detection even after 45 d of operation(490 pore volumes,PV).In contrast,NQ breakthrough(removal efficiency<85%)was observed after 18 d(180 PV)in the Fe S-packed column.The high NQ removal efficiency and long service life of the ZVI-packed column(>490 PV)suggest that the technology is a promising approach for NQ treatment in packed-bed reactors and in situ remediation. 展开更多
关键词 Continuous water treatment Iron-based minerals Chemical reduction pH AMINOGUANIDINE GUANIDINE
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Effect of pre-rolling temperature on microstructures, tensile properties and fracture behaviors of Al-5.9Zn-1.9Mg alloy during thermomechanical treatment
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作者 CHENG Jun-hua GUO Xiao-fang +3 位作者 LIU Chang SHAO Hong-bang LIU Yu HUANG Yuan-chun 《Journal of Central South University》 2025年第9期3237-3254,共18页
The microstructures,mechanical properties,and fracture behaviors of an Al-5.9Zn-1.9Mg alloy subjected to thermomechanical treatment across different pre-rolling temperatures have been exhaustively investigated in pres... The microstructures,mechanical properties,and fracture behaviors of an Al-5.9Zn-1.9Mg alloy subjected to thermomechanical treatment across different pre-rolling temperatures have been exhaustively investigated in present work.The pre-deformation temperature exerts a modest influence on grain morphology,while it profoundly impacts the dislocation configurations and precipitation behaviors.Elevating the rolling temperature from ambient to 170℃results in a reduction in dislocation density within grains accompanied by a notable enhancement in their distributional uniformity.While advancing the temperature to 320℃prompts the premature formation of precipitates during deformation,which diminishes the precipitation during the subsequent ageing.Tensile results reveal that the thermomechanical treatment incorporating pre-rolling at 170℃confers a substantial strengthening effect on the alloy on the basis of both grain boundary strengthening and dislocation strengthening stemmed from pre-deformation along with the precipitation strengthening generated by ageing.Furthermore,the microstructure exhibits a relatively scarce presence of inhomogeneous features such as dislocation pile-ups and micro shear bands,contributing favorably to enhance the ductility of the alloy that presents the mixture of cleavage fracture and dimple-induced failure. 展开更多
关键词 Al-Zn-Mg alloy thermomechanical treatment deformation temperature MICROSTRUCTURES tensile properties
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Enhancing wear resistance of TiN-coated 1.3343 high-speed steel punches through deep cryogenic treatment and tempering
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作者 Ferhat CERİTBİNMEZ Fatih HayatiÇAKIR Berkent PARİM 《Journal of Central South University》 2025年第2期350-362,共13页
In this study,samples obtained from 1.3343 high-speed steel punches with TiN coatings were tested.The samples were subjected to heat treatment at different cryogenic temperatures(<196℃)and durations(12,24 and 36 h... In this study,samples obtained from 1.3343 high-speed steel punches with TiN coatings were tested.The samples were subjected to heat treatment at different cryogenic temperatures(<196℃)and durations(12,24 and 36 h),followed by tempering at two different temperatures(200,500℃).For performance testing,a ball-on-disk wear test setup was utilized and a total of 6 groups of samples were examined.The effects of cryo-treatment and tempering on microstructure were revealed through microstructural analysis with scanning electron microscopy(SEM),X-ray(XRD diffraction),and Rietveld analysis.Additionally,the hardness of the punches was measured with microhardness measurements.The optimal wear resistance was observed in the 36 h deep cryo-treated and 200℃tempered samples.The characterization study indicates that by cryogenic treatment a significant portion of the retained austenite transformed into martensite and secondary carbides formed,resulting in improved wear resistance and a slight increase in hardness. 展开更多
关键词 cryogenic treatment high-speed steel PUNCH TIN secondary carbides retained austenite Rietveld analysis
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Effects of applying electroshocking treatment at different stages of cold rolling-quenching-tempering process on microstructure and properties of M50 steel
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作者 WEI Wen-ting LI Lai-yu +2 位作者 LIU Guo-cheng LIU Yan-xiong HUA Lin 《Journal of Central South University》 2025年第7期2432-2445,共14页
Electroshocking treatment(EST),an efficient and rapid material treatment method,promotes microstructure evolution and improves mechanical properties.This study incorporates EST into the conventional cold rolling-quenc... Electroshocking treatment(EST),an efficient and rapid material treatment method,promotes microstructure evolution and improves mechanical properties.This study incorporates EST into the conventional cold rolling-quenching tempering process of M50 steel and investigates the influence and mechanism of applying EST at different stages of the process on the microstructure and mechanical properties.Scanning electron microscope(SEM),transmission electron microscope(TEM),and X-ray diffraction(XRD)were used to characterize the effect of EST on microstructure.The results show that EST can refine the grains of M50(average reduction of 10.1%in grain size),homogenize the grain size distribution,reduce the dislocation density(20.9%in average),promote the dissolution of carbides in the matrix and distribute them more uniformly along the grain boundaries,resulting in the improvement of mechanical properties.The mechanical properties of the specimen with the process flow of rolling-quenching-tempering-electroshocking showed excellent performance,with an increase in hardness of 1.4%,tensile strength of 17.7%,and elongation at break of 24.3%as compared to the specimen without EST.The tensile properties of the specimen with the process flow of rolling electroshocking-quenching-tempering showed the best performance,with an increase in tensile strength of 30.0%and elongation at break of 30.7%as compared to the specimen without EST. 展开更多
关键词 electroshocking treatment M50 bearing steel cold rolling mechanical properties
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Effect of pre-heat treatment and subsequent ECAP-CU on microstructure and corrosion behavior of 7075 Al alloy fasteners
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作者 ZHANG Jun-jie HE Tao +4 位作者 DU Xiang-yang ALEXER Vereschaka SONG Miao CHEN Xi-lin LI Jian 《Journal of Central South University》 2025年第7期2383-2403,共21页
It is of great significance to study the corrosion process of aluminum(Al)alloys fasteners in order to mitigate corrosion for their widespread applications.In this paper,a method for enhancing the corrosion resistance... It is of great significance to study the corrosion process of aluminum(Al)alloys fasteners in order to mitigate corrosion for their widespread applications.In this paper,a method for enhancing the corrosion resistance of Al alloy fasteners is proposed.7075 Al alloy parts with a fine-grained microstructure were prepared by pre-heat treatment(PHT),combined subsequent equal channel angular pressing(ECAP)and cold upsetting(CU).The corrosion behavior of the specimens was investigated by intergranular corrosion and electrochemical test.Microstructure investigations were carried out by field emission scanning electron microscopy,energy dispersive spectrometer and transmission electron microscopy.The relationship between microstructural evolution and corrosion resistance changes was also explored.The results show that both PHT and ECAP-CU significantly improved the corrosion resistance of the samples and modified the corrosion process.The open circuit potential,corrosion current density and corrosion rate of the alloy on electrochemical test were(-0.812±8.854)×10^(-5) V(vs.SCE),(6.379±0.025)×10^(-6) A/cm^(2) and 0.066 mm/year,respectively,and the intergranular corrosion depth was(557±8)μm.The main factor controlling the corrosion behavior was the microstructure evolution.After PHT,the disappearance of the dendritic structure and the dissolution of the nonequilibrium second phase eliminated the potential difference between the phases,reducing the free energy in the as cast state.When ECAP-CU was used after PHT,the grain refinement was accompanied by a high density of grain boundaries and dislocations,which led to the formation of a denser passivation film on the alloy surface,improving the corrosion resistance in an aggressive environment. 展开更多
关键词 aluminum alloy fasteners heat treatment equal channel angular pressing cold upsetting MICROSTRUCTURE corrosion resistance
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High-temperature stability and mechanical property optimization of laser powder bed fusion 316L steel after controlled annealing
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作者 LI Wen-qi MENG Li-xin +3 位作者 ZHANG Qian-fen LU Hui-hu NIU Xiao-feng HOU Hua 《Journal of Central South University》 2025年第4期1179-1193,共15页
The research demonstrated that laser powder bed fusion(LPBF)coupled with controlled annealing at 1200°C,could significantly increase the proportion of coincidence site lattice(CSL)grain boundary,thereby achieving... The research demonstrated that laser powder bed fusion(LPBF)coupled with controlled annealing at 1200°C,could significantly increase the proportion of coincidence site lattice(CSL)grain boundary,thereby achieving an outstanding synergy of enhanced strength and exceptional ductility.The plastic deformation behavior,strain hardening behavior,and fracture behavior of LPBF 316L steel annealing at 1200℃for 20 h were studied through quasi-in-situ tensile process.It was found that LPBF 316L steel formed a certain proportion of deformation twins during the tensile process,and the formation of twins changed the crystal orientation,thus promoting further slip and crystal deformation.The synergistic effect of slip and twin promoted higher plasticity.LPBF process coupled with controlled annealing at 1200°C for 20 h leads to a ultimate tensile strength of 613 MPa and total elongation of 73.8%. 展开更多
关键词 laser powder bed fusion heat treatment microstructural evolution mechanical behavior plastic deformation behavior
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Influence of cryogenic treatment on mechanical and ballistic properties of AA5754 alloy friction stir welded joints
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作者 V.Manoj Mohan Prasath S.Dharani Kumar Saurabh S.Kumar 《Defence Technology(防务技术)》 2025年第4期184-198,共15页
In the present study,the mechanical and ballistic properties of friction stir welded(FSW)aluminum alloy(AA5754)samples were investigated,both untreated and cryogenically treated,when impacted by a 7.62 mm armour-pierc... In the present study,the mechanical and ballistic properties of friction stir welded(FSW)aluminum alloy(AA5754)samples were investigated,both untreated and cryogenically treated,when impacted by a 7.62 mm armour-piercing(AP)bullet at an impact velocity of 682±20 m/s.The FSW technique was used to prepare the welded samples for AA5754,with an axial force of 7 kN,a feed rate of 20 mm/min,and a speed of 1200 rpm.The cryogenic treatments performed after welding,including deep cryogenic treatment(DCT)at196℃ and shallow cryogenic treatment(SCT)at80℃,for 6 and 72 h,respectively.The microstructure and mechanical characteristics of cryogenically treated and untreated joints were examined.The cryogenic treatment refined the grain size(1.05 μm)and enhanced the microhardness(93 Hv).Moreover,DCT-FSW significantly improved the tensile strength(13.93%)and impact strength(8.45%)compared to untreated FSW sample.Additionally,in untreated FSW samples,the fracture behaviour varied:the impact fracture mode primarily exhibited ductile failure,while the tensile fracture exhibited a mixed fracture mode.In contrast,the tensile and impact fracture modes of the DCT-FSWwere dominated by a ductile failure mode.The DCT-FSW target demonstrated a lower depth of penetration(DOP)of 31 mm compared to the SCT-FSWand untreated FSW targets.Post-ballistic SEM analysis in the crater region of all three zones revealed the formation of frictional grooves,small cracks,and adiabatic shear bands(ASBs). 展开更多
关键词 AA5754 alloy Ballistic and mechanical properties Cryogenic treatment Depth of penetration
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