摘要
合成了一个希夫碱 :苯甲醛缩 N-氨基 -N -(2 ,6-二甲基 )苯基硫脲 ,测定了其晶体结构 ,晶体属三斜晶系 ,P-I空间群 ,晶胞参数为 :α=7.883 3 (1 6) ,b=8,1 888(1 6) ,c=1 2 .3 3 7(3 ) ,α=1 0 8.64(3 ) ,β=93 .85 (3 ) ,γ=76.78(3 ) ,V=744.7(3 ) 3 ,Z=1 ,Dc=0 .91 1 kg/m3。初步生物活性表明该化合物对葡萄球菌和枯草杆菌均有一定的抑菌活性。
A shiff base,2,6-xylidene bendaizehyde thiosemicarbazone,was synthesized and studied by X-ray crystallography.Crystal structure of the target compound belongs to triclinic system with space group P-I .The unit cell parameters are: α =7.8833(16), b =8.1888(16), c =12.337(3), α =108.64(3), β =93.85(3), γ =76.78(3), V =744.7(3) 3, Z =1, D c =0.911 kg/m 3.Preliminary biological study showed that it exhibited fair fungicidal activity against staphylococcus aurers and bacillus subtilis.
出处
《承德石油高等专科学校学报》
CAS
2003年第3期15-18,共4页
Journal of Chengde Petroleum College
