摘要
目的 优化桑黄蜜炙工艺。方法 采用正交实验设计结合层次分析法,以内在质量(麦角甾醇、原儿茶醛、原儿茶酸含量)和外观性状评分为评价指标,对影响桑黄蜜炙工艺中的关键因素(蜜水比、蜜水与桑黄质量比、炒制温度、炒制时间)进行考察,确定桑黄蜜炙最佳工艺参数。结果 桑黄蜜炙最佳工艺为取桑黄生品(1 cm3方块状),加适量辅料拌匀(每100 kg的桑黄用炼蜜与水各25 kg),闷润2 h至辅料被吸尽,置于炒制容器内,在炒制温度130~140℃下炒制5 min,取出,置于50℃烘箱内2 h,取出,晾凉。3次验证实验结果的RSD为0.68%。结论 优选出的桑黄蜜炙工艺稳定、可行。
OBJECTIVE To optimize the honey processing technology of Phellinus igniarius.METHODS The key factors of honey processing technology of P.igniarius(honey-water ratio,the mass ratio of honey-water to P.igniarius,the frying temperature and the frying time)were investigated by orthogonal test combined with analytic hierarchy process to determine the optimal technological parameters,using the internal quality(the contents of ergosterol,protocatechuic aldehyde and protocatechuic acid)and appearance traits as evaluation indexes.RESULTS The optimal process of honey-roasting P.igniarius was to take raw P.igniarius(1 cm3 square block),add the appropriate amount of auxiliary materials(with 25 kg of refined honey and water for every 100 kg of P.igniarius),mix well,moisten for 2 h until the auxiliary materials were completely absorbed;put it in a frying container,fry at the frying temperature of 130-140℃for 5 min;take it out,put it in an oven at 50℃for 2 h;take it out,and let it cool.The RSD of the results of three validation experiments was 0.68%.CONCLUSIONS The optimized honey processing technology of P.igniarius is stable and feasible.
作者
洪艺丹
王巍
张立强
张一美
李利华
鞠成国
HONG Yidan;WANG Wei;ZHANG Liqiang;ZHANG Yimei;LI Lihua;JU Chengguo(College of Pharmacy,Liaoning University of Traditional Chinese Medicine,Liaoning Dalian 116600,China;TCM Processing Technology Inheritance Base(Liaoning),National Administration of Traditional Chinese Medicine,Liaoning Dalian 116600,China)
出处
《中国药房》
CAS
北大核心
2024年第11期1309-1314,共6页
China Pharmacy
基金
国家中医药管理局中药炮制技术传承创新项目(No.GZY-KJS-2022-049)。
关键词
桑黄
蜜炙工艺
正交实验
层次分析法
外观性状
内在质量
Phellinus igniarius
honey processing technology
orthogonal test
analytic hierarchy process
appearance traits
internal quality
作者简介
第一作者:洪艺丹,硕士研究生。研究方向:中药炮制工艺及原理。E-mail:1349014530@qq.com;通信作者:鞠成国,教授,博士生导师,博士。研究方向:中药炮制工艺及原理。电话:0411-85890146。E-mail:jcg7092357@163.com。
