摘要
目的:研究地枫皮氯仿部位的化学成分。方法:将传统分离方法与现代色谱分离技术相结合分离纯化化合物,经波谱数据分析和文献比对鉴定化合物结构。结果:从地枫皮的氯仿提取物中分离得到14个化合物,分别鉴定为:tashironin(1)、tashironin A(2)、14-O-benzoylfloridanolide(3)、magnolol(4)、dehydrodieugenol(5)、isodunnianol(6)、difengpin(7)、dihydrocubebin(8)、sakuraresinol(9)、rel-(2α,3β)-7-O-methylcedrusin(10)、2-[4-(3-hydroxypropyl)-2-methoxyphenoxy]-propane-1,3-diol(11)、bursephenylpropane(12)、3,3'-dimethoxy-4,8'-oxyneoligna-9,4',7',9'-tetraol(13)、(7R,8R)-4-O-(glycer-2-yl)-7,9,9'-trihydroxy-3,5,3'-trimethoxy-8-O-4'-neolignan(14)。结论:其中,化合物1、3、6、8、12为首次从该植物中分离得到。
Objective： To study the chemical constituents of chloroform of Illicii Cortex. Methods： The compounds were isolated and purified by combining conventional separation methods and modern chromatographic separation technology,and their chemical structures were elucidated by spectral data analysis and comparing with the previous literatures. Results： 14 compounds were obtained from chloroform extract of Illicii Cortex and their structures were identified as tashironin（ 1）,tashironin A（ 2）,14-O-benzoylfloridanolide（ 3）,magnolol（ 4）,dehydrodieugenol（ 5）,isodunnianol（ 6）,difengpin（ 7）,dihydrocubebin（ 8）,sakuraresinol（ 9）,rel-（ 2α,3β）-7-O-methylcedrusin（ 10）,2-[4-（ 3-hydroxypropyl）-2-methoxyphenoxy]-propane-1,3-diol（ 11）,bursephenylpropane（ 12）,3,3＇-dimethoxy-4,8＇-oxyneoligna-9,4＇,7＇,9＇-tetraol（ 13） and（ 7 R,8 R）-4-O-（ glycer-2-yl）-7,9,9＇-trihydroxy-3,5,3＇-trimethoxy-8-O-4＇-neolignan（ 14）. Conclusion： Compounds 1,3,6,8 and 12 are separated from this plant for the first times.
作者
宁德生
符毓夏
程玲
谢运昌
潘争红
NING De-sheng1 , FU Yu-xia1 , CHENG Ling2, XIE Yun-chang1 , PAN Zheng-hong1(1. Guangxi Key Laboratory of Functional Phytochemicals Research and Utilization, Guangxi Institute of Botany, Chinese Academy of Sciences, Guilin 541006, China ; 2. School of Chemical Science and Technology, Yunnan University, Kunming 650031, Chin)
出处
《中药材》
CAS
北大核心
2017年第9期2093-2097,共5页
Journal of Chinese Medicinal Materials
基金
广西科技开发项目(桂科合14125008-2-23)
广西植物功能物质研究与利用重点实验室自主研究课题(ZRJJ2014-2
ZRJJ2016-16)
关键词
地枫皮
化学成分
结构鉴定
Illicii Cortex
Chemical constituents
Structural identification
作者简介
宁德生（1982-），男，硕士，主要从事天然植物化学成分研究；Tel：13036933374，E-mail：65392586@qq．com。;通讯作者：潘争红，E—mail：pan7260@126．com。
