摘要
目的对不同批次醋京大戟饮片样品进行分析,建立醋京大戟饮片的质量标准。方法以大戟二烯醇为对照品,采用薄层层析法和高效液相色谱法对醋京大戟饮片进行了定性和定量研究;并对醋京大戟饮片进行杂质检查,对灰分、水分和浸出物含量进行了测定。结果不同批次的醋京大戟饮片在杂质、水分和浸出物含量等方面均存在差异。薄层鉴别色谱斑点清晰,分离度较好。所建立的含量测定方法操作简单、准确、重现性好。结论建立了较为完善的醋京大戟饮片质量标准,填补了醋京大戟饮片质量标准方面的空白。
Objective To establish quality standard of Euphorbia pekinensis processed with vinegar by studying different batches pieces of Euphorbia pekinensis processed with vinegar. Methods Taking euphol as reference substances,qualitative identification and quantitative detection of pieces Euphorbia pekinensis processed with vinegar was stuidied by TLC and HPLC,and impurities,moisture,ash and extract contents of pieces of Euphorbia pekinensis processed with vinegar in different batches was researched. Results the nomal and science quality standard of Euphorbia pekinensis processed with vinegar was established. Conclusion the quality standard filling a domestic gap in pieces of Euphorbia pekinensis processed with vinegar.
出处
《时珍国医国药》
CAS
CSCD
北大核心
2015年第3期628-630,共3页
Lishizhen Medicine and Materia Medica Research
基金
国家中医药管理局中医药行业科研专项(No.200807039)
关键词
醋京大戟
大戟二烯醇
质量标准
Pieces of Euphorbia pekinensis processed with vinegar
Euphol
Quality standard
作者简介
葛秀允（1968-），男（汉族），山东莒南人，山东省中医药研究院副主任中药师，博士学位，主要从事中药炮制机理和工艺研究工作．
通讯作者：孙立立（1953-），女（汉族），山东莱西人，山东省中医药研究院研究员，学士学位，主要从事中药炮制原理与中药新药研发工作．
