摘要
以丙酮、氯仿、正癸醇为原料,经成盐反应和酸化反应,制备癸氧基异丁酸粗品,粗品经减压精馏得癸氧基异丁酸,收率为75.9%,纯度为98%。
By using acetone, chloroform . 1 - decanol as the starting material, Decyloxyisobutyric acidwas prepared through salificafion reaction and Acidizing Reaction. The decyloxyisobutyric acid was obbtaine from raw product by vacuum distillation. The overall yield and purity of decyloxyisobutyric acid obtained by this routes was 75.9% and 98% ,respectively.
出处
《山东化工》
CAS
2013年第6期16-17,共2页
Shandong Chemical Industry
关键词
癸氧基异丁酸
合成
精馏
decyloxyisobutyric acid
synthesis
distillation
作者简介
胡永玲（1974-），女，副研究员，硕士，主要从事精细化学品合成。
