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3-四氢呋喃甲醇的合成工艺研究 被引量:2

Study on the Synthesis Process of 3-Hydroxymethyltetrahydrofuran
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摘要 在调研已报道文献的基础上,选取了一条可行的合成呋虫胺中间体3-四氢呋喃甲醇的路线,并以此为依据,通过优化工艺过程和工艺条件,高收率地得到了产品。 Based on the previous reports,synthetic route of 3-hydroxymethyl tetrahydrofuran suitable to industrialization was selected,according to which technological process and conditions were optimized as high yield of product gained.
作者 汪兴玉
出处 《安徽化工》 CAS 2012年第2期23-24,共2页 Anhui Chemical Industry
关键词 3-四氢呋喃甲醇 合成 硼氢化钠还原 醚化关环 3-hydroxymethyltetrahydrofuran synthesis sodium borohydride reduction etherification cyclization
作者简介 汪兴玉(1979-),男,毕业于西北大学,助理工程师,目前从事基础化学研究及环境影响评价工作,13295603947,wangxingyunwu@126.com.
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参考文献6

  • 1Wakita T, Kinoshita K, Yamada E, et al. The Discovery of Dinotefuran: A Novel Neonicotinoid [J]. Pest Manag Sci, 2003, 59: 1016-1022.
  • 2Kodaka K, Kinoshita K, Shiraish S, et al. Furanyl Insecticide: EP, 0649845 [P]. 1995,04-26.
  • 3Applied Catalysis, A: General, 2006,303( 1 ) : 23-28.
  • 4Synthetic Communications,2005, 35(7) :971-978.
  • 5Gilbert I, Nguyen C, Filippo R G, et al. Dutpase Inhibitors:WO, 2005065689 [P]. 2005,07-21.
  • 6刘安昌,张良,谭珍友,刘芳.新型烟碱类杀虫剂呋虫胺的合成研究[J].世界农药,2009,31(2):22-23. 被引量:28

二级参考文献9

  • 1Takeo Wakita, Katsutoshi Kinoshita, Eiichi Yamada, Naoko Yasui, Nobuyuki Kawahara, Atsuko Naoi, Michihiko Nakaya, Koichi Ebihara, Hirozumi Matsuno and Kenji Kodaka. The discovery of dinotefuran: a novelneonicotinoid[J]. Pest Manag Sci, 2003,59,1016-1022
  • 2Qi-Huang Zheng , Ji-Quan Wang, Xuan Liu, Xiangshu Fei, Bruce H. Mock, Barbara E. Glick-Wilson, Michael L. Sullivan, Sudhanshu P. Raikwar, Thomas A. Gardner, Chinghai Kao,and Gary D. Hutchins. An Improved Total Synthesis of PET HSV-tk Gene Reporter Probe 9-(4-[^18F] Fluoro -3- hydroxymethylbutyl)guanine ([^18F]FHBG) [J]. Synthetic Communications, 2004, 34(4), 689-704.
  • 3Mayahara, Kunio; Omatsu, Toshihiro; Onishi, Koji. Preparation of 3-hydroxymethyl tetrahydrofuran [P]. 1997,11,25.
  • 4Malladi,Pardhasaradhi;Potluri,Sri Nagesh Kumar.Process for the preparation of 3 -(hydroxymethyl)tetrahydro furan from 9-hydroxymethyl-7,12-dioxaspiro [5.6]dodecane in the presence of an alcohol and an acid catalyst[P]. U.S. 2002,3,12.
  • 5Bhatti, Balwinder Singh; Gatto, Gregory J.; Klucik, Jozef. Preparation of N-aryl diazaspirocyclic compounds in the treatment of drug addiction[P]. WO 2006023630, 2006,03,02.
  • 6Wakita, Takeo; Kinoshita, Katsutoshi; Yamada, Eiichi; Yasui, Naoko; Kawahara, Nobuyuki; Naoi, Atsuko; Nakaya, Michihiko; Ebihara, Koichi; Matsuno, Hirozumi; Kodaka, Kenji. The discovery of dinotefuran: A novel neonicotinoid [J]. Pest Management Science, 2003, 59(9), 1016-1022.
  • 7Maienfisch, Peter Kristiansen, Odd; Gsell, Laurenz. Preparation of 2- (nitroimino)-1,3,5-triazacyclohexane pesticides[P]. EP 483055, 1992, 4,29.
  • 8Cottrell, Ian W.; Ahn, Albert; Dorneval, Linda. High-concentration dinotefuran topical insecticide formulations[P]. US 2007254951, 2006,4,28.
  • 9张亦冰.新内吸杀虫剂——呋虫胺[J].世界农药,2003,25(5):46-47. 被引量:47

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