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正交实验法优选WO_3-TiO_2复合光催化剂的制备条件 被引量:2

Optimizing synthesis conditions of TiO_2-WO_3 composite catalyst by orthogonal design
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摘要 用溶胶-凝胶法制备WO3-TiO2复合粉体光催化剂,以甲基橙光催化降解率作为指标,采用正交实验法对光催化剂的制备条件WO3掺杂量、焙烧温度、焙烧时间3个因素进行优选。研究结果表明:因素的影响顺序为WO3掺杂量>焙烧温度>焙烧时间,WO3-TiO2复合粉体光催化剂的最佳制备条件为:钨酸钠加入量X(WO3)=2%,焙烧时间5h,焙烧温度600℃。 TiO2-WO3 composite catalyst was prepared by Sol-gel method. The photocatalytic activity of the catalyst was investigated for photocatalytic degradation of methyl orange. Synthesis conditions of TiO2-WO3 composite catalyst were optimized by amount of dopped WO3, calcining temperature and time by orthogonal test. Results show that the influencing factors were amount of dopped WO3 〉 calcining temperature 〉 calcining time. Conclusion : The photodegradation activity of TiO2-WO3 with X ( WO3 ) = 2% and calcined at 600℃ for 9 hour is the best.
出处 《贵州师范大学学报(自然科学版)》 CAS 2011年第4期80-82,共3页 Journal of Guizhou Normal University:Natural Sciences
关键词 光降解 溶胶-凝胶法 TiO2-WO3复合光催化剂 正交实验 photodegradation sol-gel method TiO2-WO3 composite catalyst orthogonal test
作者简介 作者简介:廖莉玲(1963-),女,硕士,教授,硕士生导师,研究方向:无机材料,E—mail:lll6383@163.com.
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