摘要
The chemical constituents of fistular onion stalk obtained by supercritical CO2 extraction were separated and purified by silica gel and sephadex LH-20 gel column chromatography and the preparative TLC method and four flavonoids were obtained. On the basis of the spectral data, they were structurally identified as (+)-catechin, (-)-epieatechin, astragalin, and 3-O-β-D(2-O-β-D-glu- copyranosyl)-glucopyranosides of kaempferol.
The chemical constituents of fistular onion stalk obtained by supercritical CO2 extraction were separated and purified by silica gel and sephadex LH-20 gel column chromatography and the preparative TLC method and four flavonoids were obtained. On the basis of the spectral data, they were structurally identified as (+)-catechin, (-)-epieatechin, astragalin, and 3-O-β-D(2-O-β-D-glu- copyranosyl)-glucopyranosides of kaempferol.
基金
supported by a grant from a National Program of Science and Research of China (No. 2006BAI09B08-07)
作者简介
Qinqin FU, E-mail: liaqinqin2004@ 163.comCorresponding author, E-mail: whzhchg@ 126.com