摘要
目的:建立一种直接进样毛细管气相色谱法测定花露水中甲醇含量的方法。方法:进样1μl,用氢火焰离子化检测器测定,并进行相应的方法学验证。结果:甲醇在0.04 mg/ml～1.58 mg/ml范围内呈现良好的线性关系,γ=1.0000,最低检出限为4μg/ml,平均回收率为99.84%,RSD为2.33%(n=9)。结论:该法简便、快速、灵敏、结果准确可靠,可用于花露水中甲醇的含量测定。
Objective：To develop a new capillary GC method for determination of methanol in floral water.Methods： The chromatogram of test solution was recorded with FID,the injection volume was 1 μl,and the new method was validated.Results： The linear responses range were from 0.04 mg/ml～1.58 mg/ml for methanol（γ=0.9997）.The limit of detection was 4 μg/ml.The average recovery of methanol was 99.84% with RSD 2.33%（n=9）.Conclusion： The method was proved to be simple,rapid,sensitive and reliable and it could be used for determination of methanol in floral water.
出处
《中国卫生检验杂志》
CAS
2010年第10期2465-2466,共2页
Chinese Journal of Health Laboratory Technology
作者简介
楼永军（1978-），男，硕士，主管药师，主要从事药品分析与质量控制。
