摘要
采用HF＋HClO4＋HNO3分解试样，氢化物发生-原子荧光光谱法（HGAFS）测定非金属矿凹凸棒石及泥质岩中的硒．其方法回收率在98．2％～103．0％之间，相对标准偏差为0．95％-5．80%，方法检出限可达到3．5×10^-11g／mL．经实验证实方法具有简便、快速、灵敏度高等优点．
The sample was dissolved in HF, HClO4 and HNO3, then directly determine selenium of industrial minerals with HG-AFS. The relative stand deviation was 0. 95%-5. 80% and the recovery was 98.2%-103.0%. The detection limit was 3. 5×10^-11 g/mL. The method is simple, quick and high sensitivity.
出处
《分析测试技术与仪器》
CAS
2007年第3期222-224,共3页
Analysis and Testing Technology and Instruments
关键词
HG-AFS自动进样
非金属矿
硒
HG-AFS
automatic sampling
industrial minerals
selenium
作者简介
武学军（1957-），男，工程师，从事岩矿分析工作．
