期刊文献+

固相微萃取-气质联用分析锦橙果皮香气成分 被引量:16

Analysis of Aroma Components from Peel of Jinchen Orange by Solid Phase Microextraction Coupled with GC-MS
在线阅读 下载PDF
导出
摘要 为促进锦橙果皮在精细化工和食品加工中的应用,用固相微萃取-气质联用技术对锦橙果皮的香气成分进行了分析研究,通过谱库检索结合气相色谱保留指数定性方法,分离并鉴定出72个组分,已鉴定化合物占总离子流出峰面积的95.84%,主要香气成分的相对质量分数是:D-柠檬烯(68.7%)、β-月桂烯(9.92%)、芳樟醇(2.91%)、桧烯(2.15%)、香叶醛(2.14%)、橙花醛(1.46%)、α-蒎烯(1.27%)、癸醛(1.26%)。主要的香气成分是萜烯类化合物。 The aroma components from peel of Jinchen orange were analyzed by solid phase microextraction (SPME) coupled with GC - MS. Through comparison with mass spectra database and their retention indices relative to n-alkanes, 72 components were identified, covering 95.84% of the total peak areas in the GC - MS total ion current chromatogram. The main components are D-limonene (68.7%) ,β-myrcene (9.92%), linalool (2.91%), sabinene (2. 15% ), geranial (2. 14% ), neral (1.46%) ,α-pinene(1.27% ) and decanal (1.26%). Most of the identified components are terpene compounds.
出处 《精细化工》 EI CAS CSCD 北大核心 2007年第8期800-804,共5页 Fine Chemicals
基金 农业部农业结构调整重大技术研究专项项目(04-09-03B) 湖北省重点科技攻关项目(2005AA201C68)~~
关键词 锦橙 果皮 香气 固相微萃取 气质联用 Jinchen peel aroma SPME GC - MS
作者简介 乔宇(1981-),女,天津人,博士研究生,师从谢笔钧教授,主要从事柑橘挥发性成分的研究,电话:027-87280954;E-mail: qiaoyu412@sina.com.
  • 相关文献

参考文献14

  • 1汪秋安,单扬.柑桔香精油的提取与食用柑桔香精的调制[J].食品工业科技,2002,23(6):41-43. 被引量:15
  • 2黄远征,吴云伦.25个种和品种的柑桔果皮精油的化学成分[J].天然产物研究与开发,1998,10(4):48-54. 被引量:22
  • 3H(o)gnadóttir(A),Rouseff R L.Identification of aroma active compounds in orange essence oil using gas chromatography-olfacotmetry and gas chromatography-mass spectrometry[J].J Chromatogr A,2003,998:201-211.
  • 4Minh Tu N T,Thanh L X,Une A,et al.Volatile constituents of Vietnamese pummelo,orange,tangerine and lime peel oils[J].Flavour Fragr J,2002,17:169-174.
  • 5Jacqueline S,Philippe R,Alain Shum Cheong Sing.Volatile constituents of five Citrus petitgrain essential oils from reunion[J].Flavour Fragr J,2005,20:399-402.
  • 6Moshonas M G,Shaw P E.Quantitative determination of 46 volatile constituents in fresh,unpasteurized orange juices using dynamic headspace gas chromatography[J].Journal of Agricultural and Food Chemistry,1994,42:1525-1528.
  • 7Shaw P E,Moshonas M G,Jack Hearn C,et al.Volatile constituents in fresh and processed juices from grapefruit and new grapefruit hybrids[J].Journal of Agricultural and Food Chemistry,2000,48:2425-2429.
  • 8Petersen M A,Tonder D,Poll L.Comparison of normal and accelerated storage of commercial orange juice-changes in flavour and content of volatile compounds[J].Food Quality and Preference,1998,9:43-51.
  • 9高余朵,李保国.柑橘精油的超临界CO_2萃取实验研究[J].上海理工大学学报,2005,27(3):207-210. 被引量:20
  • 10Goto M,Sato M,Kodama A,et al.Application of supercritical fluid technology to citrus oil processing[J].Physical B,1997,239:167-170.

二级参考文献9

共引文献50

同被引文献251

引证文献16

二级引证文献223

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部