摘要
以乙酸酐为介质、酸性高锰酸钾作氧化剂，制备了低硫可膨胀石墨，制备的最佳条件为：鳞片石墨∶乙酸酐∶９８％硫酸∶高锰酸钾＝１∶１．０∶０．１３∶０．０６（质量比），反应温度２５℃，反应时间２ｈ。采用ＵＶ－Ｖｉｓ、ＸＲＤ手段对产品进行了分析。
The expansible graphite with low sulfur has been prepared using acidic potassium permanganate as oxidant and acetic anhydride as medium. The best conditions of preparation are graphite:Ac 2O∶98%H 2SO 4∶KMnO 4=1∶1.0∶0.13∶0.06(mass ratio), reaction temperature 25℃, reaction time 2h. The graphite intercalation compound was determined by UV Vis and XRD.
出处
《合成化学》
CAS
CSCD
1996年第3期282-284,共3页
Chinese Journal of Synthetic Chemistry
关键词
膨胀
石墨
乙酸酐
硫酸
Low sulfur expansible graphite, Preparation, Acetic anhydride, 98% sulfuric acid.
