摘要
提出一种以各物相的X射线衍射系数K为未知量组成的方程组求解K值,进而求解各物相含量的无标定量相分析方法.该方法不需加入参比物相,允许待测样品含有一个非晶相.采用了最小二乘方程组的抛弃平均法处理数据求其最优解.
A new satandardless method of the quantitative phase analysis of the sample containing an amorphous phase by X-ray diffraction is proposed. In this method, a reference phase is not required to be added into the sample under analysis. The set of equations is established, with the unknown quantity K which is the X-ray diffraction coeffcient of the phase to be analyzed. The data is processed using the least square equation set to obtain the best solution.
出处
《物理学报》
SCIE
EI
CAS
CSCD
北大核心
1995年第10期1679-1683,共5页
Acta Physica Sinica
