摘要
目的:建立苏子降气丸(苏子、陈皮、当归、甘草等)的质量标准。方法:采用TLC法对苏子降气丸中当归、甘草进行了定性鉴别;应用HPLC法对方中有效成分橙皮苷进行了含量测定。结果:本品定性鉴别薄层色谱特征明显,专属性强;本品中橙皮苷含量测定线性范围为0.32～1.60μg,平均回收率为98.94,RSD为1.05。结论:鉴别和含量测定方法简便可靠,重复性好,作为药品标准可有效地控制苏子降气丸的质量。
AIM To establish the quality standard for Suzi Jiangqi Pills (Fructus Perillae,Pericarpium Citri Reticulatae,Radix Angelicae Sinensis,Radix Glycyrrhieae,etc.) METHODS TLC was performed to identify Radix angelicae sinensis and Radix et Rhizocua Glycyrrhizae.HPLC was used to determine hespiridin content. RESULTS The study on the quality control showed that the characteristic of identification by TLC was distinct and highly specific.The quantification method had the linearity range of 0.32-1.60 μg.The average recovery was 98.94 % TBZ# and RSD was 1.05 % . CONCLUSION The methods of identification and quantification are simple,realizable and reproducible.It can be used effectively for the quality control of Suzi Jiangqi Pills.
出处
《中成药》
CAS
CSCD
北大核心
2005年第7期775-777,共3页
Chinese Traditional Patent Medicine
关键词
苏子降气丸
当归
甘草
TLC
橙皮苷
HPLC
质量标准
Suzi Jiangqi Pills
Radix Angelicae Sinensis
Radix et Rhizoma Glycyrrhizae
TLC
hespiridin
HPLC
quality standard.
