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反相高效液相色谱法测定绿麦隆 被引量:1

Determination of Chlorotoluron in Technical Product and Formulation by Reversed-Phase High Performance Liquid Chromatography (RP-HPLC)
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摘要 反相高效液相色谱法测定绿麦隆王以燕,孙绮丽,张百臻(农业部农药检定所,国家农药质量监督检测中心北京100026)1前言绿麦隆(chlorotoluron)是一取代脲类麦田除草剂,它具有选择性内吸传导作用,目前是我国广泛使用的除草剂之一。绿麦隆分析方法... n RP-HPLC method for the quantitative determination of chlorotoluron in technical product and formu-lation was developed. Operating conditions are μBondapak C_(18) column,250mm × 4. 6mm i.d.;methanolwater glacial acetic acid(60 :40: 0.1,volume ratio)eluent and UV-243nm detection,The method is veryeffective,The coefficient of variation is less than 0.5%。
出处 《色谱》 CAS CSCD 北大核心 1994年第4期291-292,共2页 Chinese Journal of Chromatography
关键词 绿麦隆 高效液相色谱 反相 reversed-phase high performance liquid chromatography, chlorotoluron, herbicide
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  • 1徐远金,李永库.蔬菜中阔草清等8种农药残留量的高效液相色谱-质谱分析[J].分析试验室,2006,25(11):74-78. 被引量:6
  • 2宋宁慧,朱红梅,杨红.差示扫描量热法测定除草剂绿麦隆的纯度[J].分析科学学报,2007,23(1):54-56. 被引量:5
  • 3RICHTER W. Primary Methods of Measurement in Chemical Analysis[J]. Accreditation and Quality Assurance, 1997, 2(8): 353- 354.
  • 4LIU S Y, HU C Q. A Comparative Uncertainty Study of the Calibration of Macrolide Antibiotic Reference Standards Using Quantitative Nuclear Magnetic Resonance and Mass Balance Methods[J]. Analytica Chimica Acta, 2007, 602(1): 114-121.
  • 5WHO Expert Committee on Specifications for Pharmaccutial Preparations. General Guidelines for the Establishment, Maintenance and Distribution of Chemical Reference Substance[S]. Geneva, World Health Organization, 1999(WHO Technical Reports Series, No.885, Annex 3).
  • 6WHO Expert Committee on Specifications for Pharmaccutial Preparations. Evaluation of Chemical Reference Substance, in International Pharmacopoeia[S]. Geneva, World Health Organization, 2003.
  • 7The Directorate for the Quality of Medicines of the Council of Europe. European Pharmacopoeia[S]. Strasbourg, Council of Europe, 2007.
  • 8American Society for Testing and Materials (ASTM), E928, Standard Test Method for Determination of Purity by Differential Scanning Calorimetry[S]. 2001.
  • 9黎源倩,牟文萱,孙成均,张继英,向仕学,杨庆.粮食中绿麦隆残留量的气相色谱分析[J].环境化学,1997,16(1):87-91. 被引量:4
  • 10汤鋆,马冰洁,王天娇,应英,倪竹南.高效液相色谱法同时测定玉米及土壤中莠去津和绿麦隆的残留量[J].中国卫生检验杂志,2009,19(10):2272-2273. 被引量:2

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