CdS nanoparticles with different sizes have been successfully synthesi zed by microwave-assisted solid state reaction between Cd(CH3COO)2·2H2O and Na2 S·9H2O at the presence of surfactant PEG400. The process...CdS nanoparticles with different sizes have been successfully synthesi zed by microwave-assisted solid state reaction between Cd(CH3COO)2·2H2O and Na2 S·9H2O at the presence of surfactant PEG400. The process of heating has influen ce on the crystallinity of CdS. The products were characterized by XRD, SEM, TEM , and the formation mechanism of CdS nanoparticles has also been discussed.展开更多
Nanoporous gamma aluminum oxide (γ-Al2O3) was synthesized by solvothermal method in the presence of AlCl·36H2O, urea and alcohol. The calcined sample was characterized by XRD, FTIR, TEM, and Nitrogen ad- sorptio...Nanoporous gamma aluminum oxide (γ-Al2O3) was synthesized by solvothermal method in the presence of AlCl·36H2O, urea and alcohol. The calcined sample was characterized by XRD, FTIR, TEM, and Nitrogen ad- sorption-desorption measurement. Results show that the obtained γ-Al2O3 is well-dispersed nanoparticles with par- ticle size of 4￣7 nm and the product has nano-pore structure with a narrow pore size distribution of 5￣20 nm.展开更多
文摘CdS nanoparticles with different sizes have been successfully synthesi zed by microwave-assisted solid state reaction between Cd(CH3COO)2·2H2O and Na2 S·9H2O at the presence of surfactant PEG400. The process of heating has influen ce on the crystallinity of CdS. The products were characterized by XRD, SEM, TEM , and the formation mechanism of CdS nanoparticles has also been discussed.
文摘Nanoporous gamma aluminum oxide (γ-Al2O3) was synthesized by solvothermal method in the presence of AlCl·36H2O, urea and alcohol. The calcined sample was characterized by XRD, FTIR, TEM, and Nitrogen ad- sorption-desorption measurement. Results show that the obtained γ-Al2O3 is well-dispersed nanoparticles with par- ticle size of 4￣7 nm and the product has nano-pore structure with a narrow pore size distribution of 5￣20 nm.
