Surfactant template synthesis of mesoporous silica monolith was carried out via modified fast sol gel process. It was easy to obtain crack free silica monolith due to low volume shrinkage during the gelation. The morp...Surfactant template synthesis of mesoporous silica monolith was carried out via modified fast sol gel process. It was easy to obtain crack free silica monolith due to low volume shrinkage during the gelation. The morphology of the titled silica was characterized by transmission electron microscopy and X ray diffraction. The results showed that the pores were worm like and the pore size was about 4 nm. Further nitrogen isothermal absorption experiment indicated that the specific area of the titled material was 391 m 2/g, which was comparable with the reported value 306 m 2/g in literature.展开更多
文摘Surfactant template synthesis of mesoporous silica monolith was carried out via modified fast sol gel process. It was easy to obtain crack free silica monolith due to low volume shrinkage during the gelation. The morphology of the titled silica was characterized by transmission electron microscopy and X ray diffraction. The results showed that the pores were worm like and the pore size was about 4 nm. Further nitrogen isothermal absorption experiment indicated that the specific area of the titled material was 391 m 2/g, which was comparable with the reported value 306 m 2/g in literature.
