The accuracy of thermal analysis measurements is critical to analyze material properties correctly,making the improvement of measurement precision and proper uncertainty analysis of test results absolutely essential.A...The accuracy of thermal analysis measurements is critical to analyze material properties correctly,making the improvement of measurement precision and proper uncertainty analysis of test results absolutely essential.As a primary thermal analysis instrument,the simultaneous thermal analyzer(STA)has unique advantages,which combines the functionalities of thermogravimetric(TG)analyzersand differential scanning calorimeters(DSC).However,the absence of standard quality control procedures has resulted in poor measurement reproducibility,low accuracy,and inadequate traceability of analytical results.This study utilized a multi-point temperature calibration method based on national certified reference materials to reduce instrument temperature indication errors.On this basis,we innovatively established a comprehensive quality control system encompassing laboratory environmental control,standard method selection,instrument performance verification,reference material traceability,and uncertainty analysis,thereby achieving standardized operational procedures for thermal analysis measurement.Taking the"determination of initial melting temperature of unknown substances"as a representative case study,a component resolution model for thermal analysis test uncertainty was developed.Through systematic analysis of both the reference material-introduced component and measurement repeatability component,complete traceability of test results was achieved.This approach ensures data validity and enhances the accuracy of test results.This provides crucial technical support and practical reference for the standardization of thermal analysis measurement procedure and assessment of result reliability.展开更多
The technologies of software architecture are introduced, and the software analysis-and-design process is divided into requirement analysis, software architecture design and system design. Using these technologies, a ...The technologies of software architecture are introduced, and the software analysis-and-design process is divided into requirement analysis, software architecture design and system design. Using these technologies, a model of architecture-centric software analysis and design process（ACSADP） is proposed. Meanwhile, with regard to the completeness, consistency and correctness between the software requirements and design results, the theories of function and process control are applied to ACSADP. Finally, a model of integrated development environnment （IDE） for ACSADP is propcsed. It can be demonstrated by the practice that the model of ACSADP can aid developer to manage software process effectively and improve the quality of software analysis and design.展开更多
文摘The accuracy of thermal analysis measurements is critical to analyze material properties correctly,making the improvement of measurement precision and proper uncertainty analysis of test results absolutely essential.As a primary thermal analysis instrument,the simultaneous thermal analyzer(STA)has unique advantages,which combines the functionalities of thermogravimetric(TG)analyzersand differential scanning calorimeters(DSC).However,the absence of standard quality control procedures has resulted in poor measurement reproducibility,low accuracy,and inadequate traceability of analytical results.This study utilized a multi-point temperature calibration method based on national certified reference materials to reduce instrument temperature indication errors.On this basis,we innovatively established a comprehensive quality control system encompassing laboratory environmental control,standard method selection,instrument performance verification,reference material traceability,and uncertainty analysis,thereby achieving standardized operational procedures for thermal analysis measurement.Taking the"determination of initial melting temperature of unknown substances"as a representative case study,a component resolution model for thermal analysis test uncertainty was developed.Through systematic analysis of both the reference material-introduced component and measurement repeatability component,complete traceability of test results was achieved.This approach ensures data validity and enhances the accuracy of test results.This provides crucial technical support and practical reference for the standardization of thermal analysis measurement procedure and assessment of result reliability.
文摘The technologies of software architecture are introduced, and the software analysis-and-design process is divided into requirement analysis, software architecture design and system design. Using these technologies, a model of architecture-centric software analysis and design process（ACSADP） is proposed. Meanwhile, with regard to the completeness, consistency and correctness between the software requirements and design results, the theories of function and process control are applied to ACSADP. Finally, a model of integrated development environnment （IDE） for ACSADP is propcsed. It can be demonstrated by the practice that the model of ACSADP can aid developer to manage software process effectively and improve the quality of software analysis and design.
