Cold-rolling was conducted on AZ31 magnesium alloy with fine and coarse grains to produce plates with high density of shear bands and{101^(-)1}twins,respectively.Then,these two kinds of plates are subjected to isother...Cold-rolling was conducted on AZ31 magnesium alloy with fine and coarse grains to produce plates with high density of shear bands and{101^(-)1}twins,respectively.Then,these two kinds of plates are subjected to isothermal annealing to reveal the effect of shear bands and{101^(-)1}twins on recrystallization behavior.During annealing,static recrystallization occurs firstly in shear band zones and{101^(-)1}twin zones,which has different effect on texture and mechanical properties.With the increase of annealing temperature,strong basal texture remains in annealed SG-17%while the basal texture is weakened gradually in annealed LG-15%.Recrystallized grains from twin zones have a random orientation which is responsible for the weakened basal texture in annealed LG-15%.In addition,microhardness decreases gradually with the prolonged annealing time due to static recrystallization.LG-15%has a lower recrystallization activation energy because{101^(-)1}twins are in favor of the nucleation and growth of recrystallized grains.After 500℃annealing,the yield strength decreases significantly with a significant improvement in failure strain.The annealed LG-15%has a much higher compressive strain than the annealed SG-17%due to texture weakening effect.展开更多
Co87Nb10Zr3,Co76Nb19Zr5,Co64Nb26Zr10 and Co64Nb16Zr20 amorphous films were deposited on noncrystalline glass substrates by DC unbalanced magnetron sputtering. The compositions of amorphous films were tailored in the l...Co87Nb10Zr3,Co76Nb19Zr5,Co64Nb26Zr10 and Co64Nb16Zr20 amorphous films were deposited on noncrystalline glass substrates by DC unbalanced magnetron sputtering. The compositions of amorphous films were tailored in the light of the individual deposition rate of Co,Nb and Zr. The amorphous films with the anticipated composition were prepared by means of co-sputtering Co,Nb and Zr targets simultaneously. It is indicated that there is interaction among three targets during co-sputtering. The morphology and composition of the films were observed by SEM,AFM and EDS. The structure and magnetic property were measured by XRD and physical property measurement system(PPMS) . The coercivity changes with the composition,varying from 240 to 1 600 A/m. After vacuum isothermal annealing at temperatures of 475,500,525 and 550 ℃ for 15 and 30 min,respectively,it is found that high Nb content is beneficial to improving thermal stability of amorphous films. The crystallized films have the mean grain size of 2-19 nm.展开更多
基金Project(52405369) supported by National Natural Science Foundation of ChinaProject(BK20210891) supported by the Natural Science Foundation of Jiangsu Province,ChinaProject(BX2022030) supported by the Special Project of Introducing Foreign Talents of Jiangsu Province,China。
文摘Cold-rolling was conducted on AZ31 magnesium alloy with fine and coarse grains to produce plates with high density of shear bands and{101^(-)1}twins,respectively.Then,these two kinds of plates are subjected to isothermal annealing to reveal the effect of shear bands and{101^(-)1}twins on recrystallization behavior.During annealing,static recrystallization occurs firstly in shear band zones and{101^(-)1}twin zones,which has different effect on texture and mechanical properties.With the increase of annealing temperature,strong basal texture remains in annealed SG-17%while the basal texture is weakened gradually in annealed LG-15%.Recrystallized grains from twin zones have a random orientation which is responsible for the weakened basal texture in annealed LG-15%.In addition,microhardness decreases gradually with the prolonged annealing time due to static recrystallization.LG-15%has a lower recrystallization activation energy because{101^(-)1}twins are in favor of the nucleation and growth of recrystallized grains.After 500℃annealing,the yield strength decreases significantly with a significant improvement in failure strain.The annealed LG-15%has a much higher compressive strain than the annealed SG-17%due to texture weakening effect.
基金Project(2007CB607602) supported by the National Basic Research Program of China
文摘Co87Nb10Zr3,Co76Nb19Zr5,Co64Nb26Zr10 and Co64Nb16Zr20 amorphous films were deposited on noncrystalline glass substrates by DC unbalanced magnetron sputtering. The compositions of amorphous films were tailored in the light of the individual deposition rate of Co,Nb and Zr. The amorphous films with the anticipated composition were prepared by means of co-sputtering Co,Nb and Zr targets simultaneously. It is indicated that there is interaction among three targets during co-sputtering. The morphology and composition of the films were observed by SEM,AFM and EDS. The structure and magnetic property were measured by XRD and physical property measurement system(PPMS) . The coercivity changes with the composition,varying from 240 to 1 600 A/m. After vacuum isothermal annealing at temperatures of 475,500,525 and 550 ℃ for 15 and 30 min,respectively,it is found that high Nb content is beneficial to improving thermal stability of amorphous films. The crystallized films have the mean grain size of 2-19 nm.
