FeCrAl(f)/HA biological functionally gradient materials(FGMs) were successfully fabricated by the hot pressing technique.Scanning electron microscope(SEM),energy dispersive spectrometer(EDS) and bending strength test ...FeCrAl(f)/HA biological functionally gradient materials(FGMs) were successfully fabricated by the hot pressing technique.Scanning electron microscope(SEM),energy dispersive spectrometer(EDS) and bending strength test machine were utilized to characterize the microstructure,component,mechanical properties and the formation of the Ca-deficient apatite on the surface of these materials.The results indicate that an asymmetrical FeCrAl(f)/HA FGM,consolidating powders prepared by mixing HA with 3%–15%(volume fraction) is successfully prepared.Both of the matrix and FeCrAl fiber are integrated very tightly and bite into each other very deeply.And counter diffusion takes place to some extent in two phase interfaces.The elemental compositions of the FeCrAl(f)/HA FGM change progressively.Ca and P contents increase gradually with immersion time increasing,and thereafter approach equilibrium.The bone-like apatite layer forms on the materials surface,which possesses benign bioactivity,and the favorable biocompatibility can provide potential firm fixation between FeCrAl(f)/HA asymmetrical FGM implants and human bone.展开更多
The method of lines(MOL) for solving the problems of functionally gradient materials(FGMs) was studied. Navier’s equations for FGMs were derived, and were semi-discretized into a system of ordinary differential (equa...The method of lines(MOL) for solving the problems of functionally gradient materials(FGMs) was studied. Navier’s equations for FGMs were derived, and were semi-discretized into a system of ordinary differential (equations(ODEs)) defined on discrete lines with the finite difference. By solving the system of ODEs, the solutions to the problem can be obtained. An example of three-point bending was given to demonstrate the application of MOL for a crack problem in the FGM. The computational results show that the more accurate results can be obtained with less computational time and resources. The obvious difficulties of numerical method for crack problems in FGMs, such as the effect of material nonhomogeneity and the existence of high gradient stress and strain near a crack tip, can be overcome without additional consideration if this method is adopted.展开更多
为解决激光定向能量沉积(laser-directed energy deposition,L-DED)成型工艺制备的镍钴基功能梯度材料(NiCo-FGMs)磨削后表面质量一致性较差这一问题,基于正交试验分析了磨削工艺参数对NiCo-FGMs的磨削力和表面粗糙度的影响规律,并建立...为解决激光定向能量沉积(laser-directed energy deposition,L-DED)成型工艺制备的镍钴基功能梯度材料(NiCo-FGMs)磨削后表面质量一致性较差这一问题,基于正交试验分析了磨削工艺参数对NiCo-FGMs的磨削力和表面粗糙度的影响规律,并建立相应的预测模型.针对粗加工与精加工的不同加工目标,利用第二代非支配排序遗传算法(NSGA-Ⅱ)结合熵权法与逼近理想解的排序方法即熵权TOPSIS(technique for order proference by similarity to ideal solution)法进行了多目标磨削工艺参数优化,并进行验证.结果表明:粗加工磨削参数采用a_(p)=53.61μm,v_(s)=29.99 m/s,v_(w)=311.89 mm/min;精加工磨削参数采用ap=14.96μm,v_(s)=29.99 m/s,v_(w)=300.92 mm/min.经两道工序加工,表面粗糙度标准差从0.195μm降至0.101μm,有效提高NiCo-FGMs的表面粗糙度一致性.展开更多
Based on the deep understanding of the requirements of cutting conditions on ceramic tools, a design model for functionally gradient ceramic tool materials with symmetrical composition distribution was presented in th...Based on the deep understanding of the requirements of cutting conditions on ceramic tools, a design model for functionally gradient ceramic tool materials with symmetrical composition distribution was presented in this paper, according to which an Al 2O 3-TiC functionally gradient ceramic tool material FG-1 was synthesized by powder-laminating and uniaxially hot-pressing technique. The thermal shock resistance of the Al 2O 3-TiC functionally gradient ceramics FG-1 was evaluated by water quenching and subsequent three-point bending tests of flexural strength diminution. Comparisons were made with results from parallel experiments conducted using a homogeneous Al 2O 3-TiC ceramics. Functionally gradient ceramics exhibited higher retained strength under all thermal shock temperature differences compared to homogeneous ceramics, indicating the higher thermal shock resistance. The experimental results were supported by the calculation of transient thermal stress field. The cutting performance of the Al 2O 3-TiC functionally gradient ceramic tool FG-1 was also investigated in rough turning the cylindrical surface of exhaust valve of diesel engine in comparison with that of a common Al 2O 3-TiC ceramic tool LT55. The results indicated that the tool life of FG-1 increased by 50 percent over that of LT55. Tool life of LT55 was mainly controlled by thermal shock cracking which was accompanied by mechanical shock. While tool life of FG-1 was mainly controlled by mechanical fatigue crack extension rather than thermal shock cracking, revealing the less thermal shock susceptibility of functionally gradient ceramics than that of common ceramics.展开更多
电子信息系统小型化、轻量化、无人化、一体化的发展趋势要求电子封装持续减小尺寸、降低重量和减少功耗(SWaP,即Size,Weight and Power)。传统的基于可伐合金、铝合金和高硅铝的微电子封装材料难以同时满足大跨度热匹配、良好的钎焊与...电子信息系统小型化、轻量化、无人化、一体化的发展趋势要求电子封装持续减小尺寸、降低重量和减少功耗(SWaP,即Size,Weight and Power)。传统的基于可伐合金、铝合金和高硅铝的微电子封装材料难以同时满足大跨度热匹配、良好的钎焊与激光熔焊性能、高导热、高比刚度、高比强度和良好的可制造性,无法适应SWaP要求。功能梯度铝基复合材料综合了铝合金与铝硅、碳化硅铝等先进复合材料的优点,既具备大跨度热匹配、高导热率的特点,又具备精细加工和良好的激光熔焊等工艺性能,是新一代微电子封装材料的研究热点。本文综述了功能梯度铝基复合材料的优势、制备方法和封装应用情况,并对该材料制备与应用中存在的问题进行了总结,最后对其未来研究方向进行了展望。展开更多
基金Project(51274247)supported by the National Natural Science Foundation of ChinaProject(2012BAE06B00)supported by the National High Technology Research and Development Program to China+1 种基金Project(2011QNZT046)supported by the Fundamental Research Funds of Central South Universities of ChinaProject supported by Hunan Postdoctoral Scientific Program,China
文摘FeCrAl(f)/HA biological functionally gradient materials(FGMs) were successfully fabricated by the hot pressing technique.Scanning electron microscope(SEM),energy dispersive spectrometer(EDS) and bending strength test machine were utilized to characterize the microstructure,component,mechanical properties and the formation of the Ca-deficient apatite on the surface of these materials.The results indicate that an asymmetrical FeCrAl(f)/HA FGM,consolidating powders prepared by mixing HA with 3%–15%(volume fraction) is successfully prepared.Both of the matrix and FeCrAl fiber are integrated very tightly and bite into each other very deeply.And counter diffusion takes place to some extent in two phase interfaces.The elemental compositions of the FeCrAl(f)/HA FGM change progressively.Ca and P contents increase gradually with immersion time increasing,and thereafter approach equilibrium.The bone-like apatite layer forms on the materials surface,which possesses benign bioactivity,and the favorable biocompatibility can provide potential firm fixation between FeCrAl(f)/HA asymmetrical FGM implants and human bone.
基金Projects(90305023 59731020) supported by the National Natural Science Foundation of China
文摘The method of lines(MOL) for solving the problems of functionally gradient materials(FGMs) was studied. Navier’s equations for FGMs were derived, and were semi-discretized into a system of ordinary differential (equations(ODEs)) defined on discrete lines with the finite difference. By solving the system of ODEs, the solutions to the problem can be obtained. An example of three-point bending was given to demonstrate the application of MOL for a crack problem in the FGM. The computational results show that the more accurate results can be obtained with less computational time and resources. The obvious difficulties of numerical method for crack problems in FGMs, such as the effect of material nonhomogeneity and the existence of high gradient stress and strain near a crack tip, can be overcome without additional consideration if this method is adopted.
文摘为解决激光定向能量沉积(laser-directed energy deposition,L-DED)成型工艺制备的镍钴基功能梯度材料(NiCo-FGMs)磨削后表面质量一致性较差这一问题,基于正交试验分析了磨削工艺参数对NiCo-FGMs的磨削力和表面粗糙度的影响规律,并建立相应的预测模型.针对粗加工与精加工的不同加工目标,利用第二代非支配排序遗传算法(NSGA-Ⅱ)结合熵权法与逼近理想解的排序方法即熵权TOPSIS(technique for order proference by similarity to ideal solution)法进行了多目标磨削工艺参数优化,并进行验证.结果表明:粗加工磨削参数采用a_(p)=53.61μm,v_(s)=29.99 m/s,v_(w)=311.89 mm/min;精加工磨削参数采用ap=14.96μm,v_(s)=29.99 m/s,v_(w)=300.92 mm/min.经两道工序加工,表面粗糙度标准差从0.195μm降至0.101μm,有效提高NiCo-FGMs的表面粗糙度一致性.
文摘Based on the deep understanding of the requirements of cutting conditions on ceramic tools, a design model for functionally gradient ceramic tool materials with symmetrical composition distribution was presented in this paper, according to which an Al 2O 3-TiC functionally gradient ceramic tool material FG-1 was synthesized by powder-laminating and uniaxially hot-pressing technique. The thermal shock resistance of the Al 2O 3-TiC functionally gradient ceramics FG-1 was evaluated by water quenching and subsequent three-point bending tests of flexural strength diminution. Comparisons were made with results from parallel experiments conducted using a homogeneous Al 2O 3-TiC ceramics. Functionally gradient ceramics exhibited higher retained strength under all thermal shock temperature differences compared to homogeneous ceramics, indicating the higher thermal shock resistance. The experimental results were supported by the calculation of transient thermal stress field. The cutting performance of the Al 2O 3-TiC functionally gradient ceramic tool FG-1 was also investigated in rough turning the cylindrical surface of exhaust valve of diesel engine in comparison with that of a common Al 2O 3-TiC ceramic tool LT55. The results indicated that the tool life of FG-1 increased by 50 percent over that of LT55. Tool life of LT55 was mainly controlled by thermal shock cracking which was accompanied by mechanical shock. While tool life of FG-1 was mainly controlled by mechanical fatigue crack extension rather than thermal shock cracking, revealing the less thermal shock susceptibility of functionally gradient ceramics than that of common ceramics.
文摘电子信息系统小型化、轻量化、无人化、一体化的发展趋势要求电子封装持续减小尺寸、降低重量和减少功耗(SWaP,即Size,Weight and Power)。传统的基于可伐合金、铝合金和高硅铝的微电子封装材料难以同时满足大跨度热匹配、良好的钎焊与激光熔焊性能、高导热、高比刚度、高比强度和良好的可制造性,无法适应SWaP要求。功能梯度铝基复合材料综合了铝合金与铝硅、碳化硅铝等先进复合材料的优点,既具备大跨度热匹配、高导热率的特点,又具备精细加工和良好的激光熔焊等工艺性能,是新一代微电子封装材料的研究热点。本文综述了功能梯度铝基复合材料的优势、制备方法和封装应用情况,并对该材料制备与应用中存在的问题进行了总结,最后对其未来研究方向进行了展望。
