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Key techniques for precise measuring gas content in deep coal mine:In-situ pressure-and gas-preserved coring
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作者 Ju Li Jianan Li +4 位作者 Tianyu Wang Guikang Liu Zhiqiang He Cong Li Heping Xie 《International Journal of Mining Science and Technology》 2025年第4期589-607,共19页
Gas content serves as a critical indicator for assessing the resource potential of deep coal mines and forecasting coal mine gas outburst risks.However,existing sampling technologies face challenges in maintaining the... Gas content serves as a critical indicator for assessing the resource potential of deep coal mines and forecasting coal mine gas outburst risks.However,existing sampling technologies face challenges in maintaining the integrity of gas content within samples and are often constrained by estimation errors inherent in empirical formulas,which results in inaccurate gas content measurements.This study introduces a lightweight,in-situ pressure-and gas-preserved corer designed to collect coal samples under the pressure conditions at the sampling point,effectively preventing gas loss during transfer and significantly improving measurement accuracy.Additionally,a gas migration model for deep coal mines was developed to elucidate gas migration characteristics under pressure-preserved coring conditions.The model offers valuable insights for optimizing coring parameters,demonstrating that both minimizing the coring hole diameter and reducing the pressure difference between the coring-point pressure and the original pore pressure can effectively improve the precision of gas content measurements.Coring tests conducted at an experimental base validated the performance of the corer and its effectiveness in sample collection.Furthermore,successful horizontal coring tests conducted in an underground coal mine roadway demonstrated that the measured gas content using pressure-preserved coring was 34%higher than that obtained through open sampling methods. 展开更多
关键词 Pressure-and gas-preserved coring Deep coal mines coring Gas migration model In-situ gas content
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Findings from a social media listening study on Chinese patients with Alzheimer's disease:a content analysis
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作者 Nan Zhi Yongtian Zhang +7 位作者 Wenwei Cao Jinwen Xiao Jianping Li Haixia Li Xinyi Xie Rujing Ren Jieli Geng Gang Wang 《General Psychiatry》 2025年第1期55-62,共8页
Background Social media listening is a new approach for gathering insights from social media platforms about users experiences.This approach has not been applied to analyse discussions about Alzheimer's disease(AD... Background Social media listening is a new approach for gathering insights from social media platforms about users experiences.This approach has not been applied to analyse discussions about Alzheimer's disease(AD)in China.Aims We aimed to leverage multisource Chinese data to gain deeper insights into the current state of the daily management of Chinese patients with AD and the burdens faced by their caregivers.Methods We searched ninemainstreampublic onlineplatforms in China fromSeptember2010 to March 2024.Natural language processing tools were used to identify patients and caregivers,and categorise patients by disease stage forfurther analysis.We analysed the current state of patient daily management,including diagnosis and treatment,choice oftreatment scenarios,patient safetyand caregiverconcerns.Results Atotal of 1211patientswithAD(66% female,82% aged 60-90)and 756caregiversfor patients with AD were identified from 107556 online sources.Most patients were derived from online consultation platforms(43%),followed by bulletin board system platforms(24%).Among the patients categorised into specific disease stages(n=382),42% were in the moderate stage.The most frequent diagnostic tools included medical history(97%)and symptoms(84%).Treatment options for patients with AD primarily included cholinesterase inhibitors,N-methyl-D-aspartate receptor antagonists and antipsychotics.Both quantitative and qualitative analysis of patients whoexperiencedwandering(n=92)indicated a higher incidence of wandering during the moderate stage of the disease.Most caregivers were family members,with their primary concerns focusing on disease management and treatment(90%),followed by daily life care(37%)and psychosocial support(25%).Conclusions Online platform data provide a broad spectrum of real-world insights into individuals affected byAD in China.This study enhances our understanding of the experiences of patients with AD and their caregivers,providing guidance for developing personalised interventions,providing advicefor caregivers and improving care for patients with AD. 展开更多
关键词 gathering insights social media platforms content analysis alzheimers disease ad ninemainstreampublic onlineplatforms Alzheimers disease analyse discussions CAREGIVERS social media listening
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Li^(+)浓度对化学增强锂铝硅玻璃性能的影响
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作者 田昊东 徐驰 +2 位作者 胥爽 李现梓 祖成奎 《材料导报》 EI CAS CSCD 北大核心 2024年第S01期137-142,共6页
采用一步法化学增强工艺,研究了熔盐中Li^(+)的富集对不同厚度锂铝硅玻璃表面压应力、应力层深度、弯曲强度、硬度等性能的影响,选择Na_(3)PO_(4)作为熔盐除杂剂并对净化效果进行了评定。研究表明:熔盐中Li^(+)浓度增加至4800×10^(... 采用一步法化学增强工艺,研究了熔盐中Li^(+)的富集对不同厚度锂铝硅玻璃表面压应力、应力层深度、弯曲强度、硬度等性能的影响,选择Na_(3)PO_(4)作为熔盐除杂剂并对净化效果进行了评定。研究表明:熔盐中Li^(+)浓度增加至4800×10^(-6),3 mm化学增强锂铝硅玻璃的表面压应力、弯曲强度、硬度下降16.8%、16.8%、10.6%;8 mm化学增强锂铝硅玻璃的表面压应力、弯曲强度、硬度下降17.6%、14.7%、9.8%。熔盐中Li^(+)浓度的变化未对化学增强锂铝硅玻璃应力层深度产生明显影响。Na_(3)PO_(4)具有较好的除杂效果,化学增强锂铝硅玻璃的表面压应力、弯曲强度、硬度得到了明显的恢复,为保证化学增强锂铝硅玻璃在可见光波段具有较高的透光率,除杂剂Na_(3)PO_(4)的掺量不宜超过1%(质量分数)。 展开更多
关键词 锂铝硅玻璃 化学增强 离子交换 Li^(+)浓度 熔盐净化 半无限扩散模型
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Li^(+)增强NaGd(WO_(4))_(2)∶Yb^(3+)/Er^(3+)荧光粉的上转换发光和温度传感性能
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作者 吴超飞 田孜雨 +5 位作者 刘一凡 王恒越 穆浩楠 徐若瑜 贺乔 于晓晨 《微纳电子技术》 CAS 2024年第10期81-90,共10页
采用水热法制备了NaGd(WO_(4))_(2)∶0.05Yb^(3+)/0.005Er^(3+)/xLi^(+)(x=0,0.01,0.02,0.03,0.05)荧光粉。通过X射线衍射仪(XRD)、扫描电子显微镜(SEM)和光致发光(PL)谱等手段分析了样品的晶体结构、形貌和上转换发光性能。结果表明,L... 采用水热法制备了NaGd(WO_(4))_(2)∶0.05Yb^(3+)/0.005Er^(3+)/xLi^(+)(x=0,0.01,0.02,0.03,0.05)荧光粉。通过X射线衍射仪(XRD)、扫描电子显微镜(SEM)和光致发光(PL)谱等手段分析了样品的晶体结构、形貌和上转换发光性能。结果表明,Li的掺杂并未改变NaGd(WO_(4))_(2)∶Yb^(3+)/Er^(3+)荧光粉的四方相晶体结构,但在波长980nm激光二极管(LD)激发下,样品的上转换发光强度发生明显改变。随着x的增加,Er^(3+)的绿光和红光发光强度均呈现先升高后降低的趋势,当x=0.03时,发光强度达到最大值。上转换发光强度与泵浦功率的依赖关系表明,绿光和红光发射都属于双光子吸收过程。此外,采用基于Er^(3+)热耦合能级的荧光强度比(FIR)测温技术,研究了+NaGd(WO_(4))_(2)∶0.05Yb^(3+)/0.005Er^(3+)/0.03Li^(+)荧光粉在298~573K温度范围内的温度传感性能。该结果表明NaGd(WO_(4))_(2)∶0.05Yb^(3+)/0.005Er^(3+)/0.03Li^(+)荧光粉相对灵敏度(SR)在298K时达到最大值0.0119K^(-1),表明其在光学温度传感领域具有潜在的应用价值。 展开更多
关键词 上转换发光 Li^(+)掺杂 稀土 荧光强度比(FIR) 温度传感
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Incorporating empirical knowledge into data-driven variable selection for quantitative analysis of coal ash content by laser-induced breakdown spectroscopy 被引量:1
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作者 吕一涵 宋惟然 +1 位作者 侯宗余 王哲 《Plasma Science and Technology》 SCIE EI CAS CSCD 2024年第7期148-156,共9页
Laser-induced breakdown spectroscopy(LIBS)has become a widely used atomic spectroscopic technique for rapid coal analysis.However,the vast amount of spectral information in LIBS contains signal uncertainty,which can a... Laser-induced breakdown spectroscopy(LIBS)has become a widely used atomic spectroscopic technique for rapid coal analysis.However,the vast amount of spectral information in LIBS contains signal uncertainty,which can affect its quantification performance.In this work,we propose a hybrid variable selection method to improve the performance of LIBS quantification.Important variables are first identified using Pearson's correlation coefficient,mutual information,least absolute shrinkage and selection operator(LASSO)and random forest,and then filtered and combined with empirical variables related to fingerprint elements of coal ash content.Subsequently,these variables are fed into a partial least squares regression(PLSR).Additionally,in some models,certain variables unrelated to ash content are removed manually to study the impact of variable deselection on model performance.The proposed hybrid strategy was tested on three LIBS datasets for quantitative analysis of coal ash content and compared with the corresponding data-driven baseline method.It is significantly better than the variable selection only method based on empirical knowledge and in most cases outperforms the baseline method.The results showed that on all three datasets the hybrid strategy for variable selection combining empirical knowledge and data-driven algorithms achieved the lowest root mean square error of prediction(RMSEP)values of 1.605,3.478 and 1.647,respectively,which were significantly lower than those obtained from multiple linear regression using only 12 empirical variables,which are 1.959,3.718 and 2.181,respectively.The LASSO-PLSR model with empirical support and 20 selected variables exhibited a significantly improved performance after variable deselection,with RMSEP values dropping from 1.635,3.962 and 1.647 to 1.483,3.086 and 1.567,respectively.Such results demonstrate that using empirical knowledge as a support for datadriven variable selection can be a viable approach to improve the accuracy and reliability of LIBS quantification. 展开更多
关键词 laser-induced breakdown spectroscopy(LIBS) coal ash content quantitative analysis variable selection empirical knowledge partial least squares regression(PLSR)
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Quantitative characterizations of anisotropic dynamic properties in organic-rich shale with different kerogen content
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作者 Jian-Yong Xie Yan-Ping Fang +4 位作者 Xing-Hua Wu Jian'er Zhao Jun-Cheng Dai Jun-Xing Cao Ji-Xin Deng 《Petroleum Science》 SCIE EI CAS CSCD 2024年第2期855-865,共11页
Understanding the quantitative responses of anisotropic dynamic properties in organic-rich shale with different kerogen content(KC)is of great significance in hydrocarbon exploration and development.Conducting control... Understanding the quantitative responses of anisotropic dynamic properties in organic-rich shale with different kerogen content(KC)is of great significance in hydrocarbon exploration and development.Conducting controlled experiments with a single variable is challenging for natural shales due to their high variations in components,diagenesis conditions,or pore fluid.We employed the hot-pressing technique to construct 11 well-controlled artificial shale with varying KC.These artificial shale samples were successive machined into prismatic shape for ultrasonic measurements along different directions.Observations revealed bedding perpendicular P-wave velocities are more sensitive to the increasing KC than bedding paralleling velocities due to the preferential alignments of kerogen.All elastic stiffnesses except C_(13)are generally decreasing with the increasing KC,the variation of C_(1) and C_(33)on kerogen content are more sensitive than those of C_(44)and C_(66).Apparent dynamic mechanical parameters(v and E)were found to have linear correlation with the true ones from complete anisotropic equations independent of KC,which hold value towards the interpretation of well logs consistently across formations,Anisotropic mechanical parameters(ΔE and brittlenessΔB)tend to decrease with the reducing KC,withΔB showing great sensitivity to KC variations.In the range of low KC(<10%),the V_(P)/V_(S) ratio demonstrated a linearly negative correlation with KC,and the V_(P)/V_(S) ratio magnitude of less than 1.75may serve as a significant characterization for highly organic-rich(>10%)shale,compilation of data from natural organic rich-shales globally verified the similar systematic relationships that can be empirically used to predict the fraction of KC in shales. 展开更多
关键词 Elastic properties Organic shale ANISOTROPY Kerogen content Physical modeling
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Experimental and numerical analyses of the effect of fibre content on the close-in blast performance of a UHPFRC beam
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作者 Junbo Yan Qiyue Zhang +4 位作者 Yan Liu Yingliang Xu Zhenqing Shi Fan Bai Fenglei Huang 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第1期242-261,共20页
Limited research has been conducted on the influences of fiber content on close-in blasting characteristics for ultrahigh-performance fiber-reinforced concrete(UHPFRC)beams.This paper aims to address this knowledge ga... Limited research has been conducted on the influences of fiber content on close-in blasting characteristics for ultrahigh-performance fiber-reinforced concrete(UHPFRC)beams.This paper aims to address this knowledge gap through experimental and mesoscale numerical methods.Experiments were conducted on ten UHPFRC beams built with varying steel fiber volumetric fractions subjected to close-in explosive conditions.Additionally,this study considered other parameters,such as the longitudinal reinforcement type and ratio.In the case of UHPFRC beams featuring normal-strength longitudinal reinforcement of diametersΦ12,Φ16,andΦ20,a reduction in maximum displacement by magnitudes of19.6%,19.5%,and 17.4%was observed,respectively,as the volumetric fractions of fiber increased from1.0%to 2.5%.In addition,increasing the longitudinal reinforcement ratio and using high-strength steel longitudinal reinforcement both significantly reduced the deformation characteristics and increase the blasting resistances of UHPFRC beams.However,the effects on the local crushing and spalling damage were not significant.A mesoscale finite element model,which considers the impacts of fiber parameters on UHPFRC beam behaviors,was also established and well correlated with the test findings.Nevertheless,parametric analyses were further conducted to examine the impacts of the steel fiber content and length and the hybrid effects of various types of microfibers and steel fibers on the blasting performance of UHPFRC beams. 展开更多
关键词 Blast performance Close-in blast Fiber content Mesoscale approach UHPFRC beams
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Main controlling factor and mechanism of gas-in-place content of the Lower Cambrian shale from different sedimentary facies in the western Hubei area, South China
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作者 Gang Li Xian-Ming Xiao +3 位作者 Bo-Wei Cheng Chen-Gang Lu Yue Feng Dong-Sheng Li 《Petroleum Science》 SCIE EI CAS CSCD 2024年第3期1488-1507,共20页
The Lower Cambrian shale gas in the western Hubei area,South China has a great resource prospect,but the gas-in-place(GIP)content in different sedimentary facies varies widely,and the relevant mechanism has been not w... The Lower Cambrian shale gas in the western Hubei area,South China has a great resource prospect,but the gas-in-place(GIP)content in different sedimentary facies varies widely,and the relevant mechanism has been not well understood.In the present study,two sets of the Lower Cambrian shale samples from the Wells YD4 and YD5 in the western Hubei area,representing the deep-water shelf facies and shallowwater platform facies,respectively,were investigated on the differences of pore types,pore structure and methane adsorption capacity between them,and the main controlling factor and mechanism of their methane adsorption capacities and GIP contents were discussed.The results show that the organic matter(OM)pores in the YD4 shale samples are dominant,while the inorganic mineral(IM)pores in the YD5 shale samples are primary,with underdeveloped OM pores.The pore specific surface area(SSA)and pore volume(PV)of the YD4 shale samples are mainly from micropores and mesopores,respectively,while those of the YD5 shale samples are mainly from micropores and macropores,respectively.The methane adsorption capacity of the YD4 shale samples is significantly higher than that of the YD5 shale samples,with a maximum absolute adsorption capacity of 3.13 cm^(3)/g and 1.31 cm^(3)/g in average,respectively.Compared with the shallow-water platform shale,the deep-water shelf shale has a higher TOC content,a better kerogen type and more developed OM pores,which is the main mechanism for its higher adsorption capacity.The GIP content models based on two samples with a similar TOC content selected respectively from the Wells YD4 and YD5 further indicate that the GIP content of the deep-water shelf shale is mainly 34 m^(3)/t within a depth range of 1000—4000 m,with shale gas exploration and development potential,while the shallow-water platform shale has normally a GIP content of<1 m^(3)/t,with little shale gas potential.Considering the geological and geochemical conditions of shale gas formation and preservation,the deep-water shelf facies is the most favorable target for the Lower Cambrian shale gas exploration and development in the western Hubei area,South China. 展开更多
关键词 Lower Cambrian shale Deep-water shelf facies Shallow-waterplat form facies Pore structure Methane adsorption Gas-in-place content Controlling factor
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Influence of wind-blown sand content on the mechanical quality state of ballast bed in sandy railways
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作者 Yihao Chi Hong Xiao +3 位作者 Zhihai Zhang Yang Wang Zhongxia Qian Weize Zhao 《Railway Engineering Science》 EI 2024年第4期533-550,共18页
During the operation of sandy railways, the challenge posed by wind-blown sand is a persistent issue. An in-depth study on the influence of wind-blown sand content on the macroscopic and microscopic mechanical propert... During the operation of sandy railways, the challenge posed by wind-blown sand is a persistent issue. An in-depth study on the influence of wind-blown sand content on the macroscopic and microscopic mechanical properties of the ballast bed is of great significance for understanding the potential problems of sandy railways and proposing reasonable and adequate maintenance and repair strategies. Building upon existing research, this study proposes a new assessment indicator for sand content. Utilizing the discrete element method(DEM) and fully considering the complex interactions between ballast and sand particles, three-dimensional(3D) multi-scale analysis models of sandy ballast beds with different wind-blown sand contents are established and validated through field experiments. The effects of varying wind-blown sand content on the microscopic contact distribution and macroscopic mechanical behavior(such as resistance and support stiffness) of ballast beds are carefully analyzed. The results show that with the increase in sand content, the average contact force and coordination number between ballast particles gradually decrease, and the disparity in contact forces between different layers of the ballast bed diminishes. The longitudinal and lateral resistance of the ballast bed initially decreases and then increases, with a critical point at 10% sand content. At 15% sand content, the lateral resistance is mainly shared by the ballast shoulder. The longitudinal resistance sharing ratio is always the largest on the sleeper side, followed by that at the sleeper bottom, and the smallest on the ballast shoulder. When the sand content exceeds 10%, the contribution of sand particles to stiffness significantly increases, leading to an accelerated growth rate of the overall support stiffness of the ballast bed, which is highly detrimental to the long-term service performance of the ballast bed. In conclusion, it is recommended that maintenance and repair operations should be promptly conducted when the sand content of the ballast bed reaches or exceeds 10%. 展开更多
关键词 Sandy railway Wind-blown sand content Discrete element method(DEM) Macroscopic and microscopic mechanical properties Maintenance and repair strategies
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玉米秸秆压缩特性试验研究
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作者 郭思佳 刘新柱 +6 位作者 刘春山 刘向东 邢蕾 栾积毅 韩平 王海祥 李剑英 《农机化研究》 北大核心 2025年第2期153-158,共6页
为了更好地利用玉米秸秆这种生物质材料,同时为设计和优化秸秆收获、打捆、切割等装置结构提供一定的技术参数,对寒地玉米秸秆进行了压缩试验。设计了三因素三水平的正交试验,并结合自制试验装置,利用万能试验机、数显鼓风干燥箱等设备... 为了更好地利用玉米秸秆这种生物质材料,同时为设计和优化秸秆收获、打捆、切割等装置结构提供一定的技术参数,对寒地玉米秸秆进行了压缩试验。设计了三因素三水平的正交试验,并结合自制试验装置,利用万能试验机、数显鼓风干燥箱等设备对玉米秸秆进行了有节段的径向和轴向压缩试验,测得了基于不同部位、不同速度、不同含水率三因素在不同水平组合下的破坏力的大小,获得因素的显著性影响程度及最优水平组合。试验结果表明:玉米秸秆轴向压缩破坏力为0.726~3.271 kN,R值为0.586~1.527,F值为7.093~38.742;玉米秸秆径向压缩破坏力为0.370~2.297 kN,R值为0.382~0.921,F值为9.096~22.183。分析得出:各因素对试验指标影响极显著的是秸秆部位,加载速度和含水率次之;最优水平组合为秸秆部位为上、加载速度为10 mm/min、含水率为最低,且径向压缩所需破坏力小于轴向压缩所需破坏力。 展开更多
关键词 玉米秸秆 压缩 含水率
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复杂电磁环境下的电离层总电子含量反演方法
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作者 石善斌 董翔 +2 位作者 黄胜 朱鹏飞 朱庆林 《电波科学学报》 北大核心 2025年第1期113-123,共11页
利用全球导航卫星系统(Global Navigation Satellite System,GNSS)双频差分信号进行电离层电子含量反演是一种常用的电离层探测手段,但GNSS信号在强电磁干扰环境下,被淹没于电磁噪声中而无法被提取,影响电离层总电子含量(total electron... 利用全球导航卫星系统(Global Navigation Satellite System,GNSS)双频差分信号进行电离层电子含量反演是一种常用的电离层探测手段,但GNSS信号在强电磁干扰环境下,被淹没于电磁噪声中而无法被提取,影响电离层总电子含量(total electron content,TEC)反演系统的可靠性。采用传统调零抗干扰阵列天线方案能解决干扰源剥离的问题,但调零信号的天线相位中心不稳定导致高精度的相位平滑伪距和精密单点定位(precise point positioning,PPP)算法无法收敛。针对强干扰环境下的电离层监测需求,本文提出一种抗干扰TEC数据反演手段,通过对阵列天线通道幅相一致性进行校正,保证相位中心的稳定性,从而推算出准确的电离层TEC信息,提高了系统的可靠性和抗干扰能力。 展开更多
关键词 总电子含量(TEC) 倾斜总电子含量(STEC) 垂直总电子含量(VTEC) 全球导航卫星系统(GNSS) 双频差分 抗干扰
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基于三相孔隙介质模型的地震动传播特性研究
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作者 杨艳霜 闫磊 +4 位作者 张占荣 刘永莉 崔臻 彭剑承 亢兆鹏 《岩土力学》 北大核心 2025年第4期1109-1121,共13页
研究地震动在软土层中的传播特性对建筑物抗震设防具有重要现实意义。根据地震动在离心振动台试验中的衰减特性,将获取的土样重塑成35%、45%、55%含水率的土样并进行常规物理试验。通过宏细观参数对比来设定模型中颗粒之间的团簇形态和... 研究地震动在软土层中的传播特性对建筑物抗震设防具有重要现实意义。根据地震动在离心振动台试验中的衰减特性,将获取的土样重塑成35%、45%、55%含水率的土样并进行常规物理试验。通过宏细观参数对比来设定模型中颗粒之间的团簇形态和颗粒之间黏结的切法向刚度、摩擦系数、泊松比、阻尼比等参数,并引入质量阻尼β_(n)和刚度阻尼k_(n)来限制颗粒的运动状态,调节颗粒运动中的碰撞。依据不同含水率常规物理试验结果修正三相孔隙介质地层模型的细观参量,以研究在地震荷载下不同含水率的软土对峰值加速度传播衰减效应的影响。研究结果表明,在不同地震动条件下,峰值加速度在30m深度段,软硬分层土质中呈现出先缓慢衰减后急剧衰减再回弹上升的变化规律。随着含水率增加,深度30~8m地层内峰值加速度衰减倍率在2.33~2.70区间内增加;而深度8~0m地层对应放大倍率则在1.60~1.23区间内减小。反应谱周期0.2~1.1s对应中低频率范围,加速度值呈现增加趋势,在周期1.1~2.0s内对应的是高频率范围,加速度值普遍呈现减小趋势,这与高频衰减效应一致。通过数值模拟与理论分析对比验证,初步探明了不同含水率条件下地震动在近地表的传播放大规律,为评估地震灾害风险及提升地震防护提供了理论依据。 展开更多
关键词 地震波 放大效应 离散元 峰值加速度 含水率
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精制敌百虫粉鉴别及含量测定方法优化
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作者 陈向丹 文静静 +4 位作者 周平 谈暠媛 董书香 丁阳 王峻 《现代畜牧科技》 2025年第2期36-38,共3页
该研究建立了精制敌百虫粉中敌百虫含量的反相高效液相色谱法(HPLC)测定方法。采用十八硅烷键合硅胶色谱柱,检测波长200 nm,流动相为水(用85%磷酸溶液调节pH值至3.0)-乙腈(85∶15),流速1.0 mL/min。结果表明,敌百虫在0.30~9.00 mg/mL浓... 该研究建立了精制敌百虫粉中敌百虫含量的反相高效液相色谱法(HPLC)测定方法。采用十八硅烷键合硅胶色谱柱,检测波长200 nm,流动相为水(用85%磷酸溶液调节pH值至3.0)-乙腈(85∶15),流速1.0 mL/min。结果表明,敌百虫在0.30~9.00 mg/mL浓度范围内含量与峰面积呈良好的线性关系,相关系数为0.999 8,平均回收率100.1%,RSD为1.6%。该方法简便、准确、快速、重现性好,可用于该制剂的鉴别及含量测定。 展开更多
关键词 敌百虫 高效液相色谱法 鉴别 含量
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超微粉碎与普通粉碎对裂褶菌粉体理化特性及营养成分含量的影响
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作者 罗晓莉 杨宁 +3 位作者 周锫 曹晶晶 张沙沙 孙达锋 《食品工业科技》 北大核心 2025年第8期104-110,共7页
为探究不同粉碎处理对裂褶菌粉体理化特性及营养成分含量的影响,本研究分别采用超微粉碎和普通粉碎两种粉碎方法,制备了不同粉碎强度的裂褶菌粉(CG-60、CG-100、CG-150、SG-20、SG-40),并对粉体的色泽、流动性、填充性、水合性质等理化... 为探究不同粉碎处理对裂褶菌粉体理化特性及营养成分含量的影响,本研究分别采用超微粉碎和普通粉碎两种粉碎方法,制备了不同粉碎强度的裂褶菌粉(CG-60、CG-100、CG-150、SG-20、SG-40),并对粉体的色泽、流动性、填充性、水合性质等理化特性和粗蛋白、粗多糖、膳食纤维等营养成分含量进行了测定和比较分析。结果表明:超微粉碎使裂褶菌粉体的振实密度降低,滑角、休止角增加,虽流动性、填充性变差,但粉体色泽更为白亮。与普通粉碎的CG-60相比,经超微粉碎的SG-40的膨胀力、持水力、持油力分别提高了77.27%、6.74%、11.63%,水溶性指数达到CG-60样品的4倍以上,水合性质得到显著改善(P<0.05),粗蛋白、粗多糖、可溶性膳食纤维等营养成分含量分别达到13.10、10.47、4.27 g/100 g,与普通粉碎粉体相比均显著增加(P<0.05)。综上所述,超微粉碎处理可改善裂褶菌粉体的水合性质,提高营养成分的溶出,粉体质地更为细腻、颜色更为白亮,但在一定程度上降低了裂褶菌粉的流动性和填充性。 展开更多
关键词 超微粉碎 普通粉碎 裂褶菌 粉体特性 营养成分
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花生籽仁蔗糖含量近红外光谱快速测定方法研究
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作者 赵星 张嘉楠 +5 位作者 张一鸣 金欣欣 苏俏 宋亚辉 李玉荣 王瑾 《中国油料作物学报》 北大核心 2025年第1期226-233,共8页
本研究以重组自交系群体为材料,建立检测范围宽、适用于优良单株筛选的蔗糖含量近红外光谱快速测定方法。采用高效液相色谱-示差折光技术测定325份材料的蔗糖含量,并利用波通DA7200型近红外分析仪采集近红外光谱,采用偏最小二乘法,构建... 本研究以重组自交系群体为材料,建立检测范围宽、适用于优良单株筛选的蔗糖含量近红外光谱快速测定方法。采用高效液相色谱-示差折光技术测定325份材料的蔗糖含量,并利用波通DA7200型近红外分析仪采集近红外光谱,采用偏最小二乘法,构建基于18~23粒花生籽仁的蔗糖含量近红外预测模型。结果表明,模型对花生籽仁蔗糖含量的预测范围可达2.07%~12.37%,决定系数为0.9054,均方根误差为0.6774。利用20份材料对模型进行外部验证,独立测试集决定系数为0.9478。该模型对花生籽仁蔗糖含量的预测准确,可实现杂交早期世代单株蔗糖含量的快速、无损测定,提升高蔗糖含量花生品种的育种效率。 展开更多
关键词 花生籽仁 蔗糖含量 HPLC-RID 近红外预测模型
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茶叶中22种元素含量分析
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作者 秦鹏 张苗 +1 位作者 陈建文 王伟光 《食品安全导刊》 2025年第4期76-79,共4页
目的:分析评价茶叶中限量元素的安全风险与所含相关元素的地理特征,为日照市场上供应茶叶中相关元素含量提供本底资料。方法:2023年10—12月随机采集120份茶叶样品,分别检测茶叶中铅、镉、汞、砷、铬、铝、锰、铜、钡、钒、硒、锑、镍... 目的:分析评价茶叶中限量元素的安全风险与所含相关元素的地理特征,为日照市场上供应茶叶中相关元素含量提供本底资料。方法:2023年10—12月随机采集120份茶叶样品,分别检测茶叶中铅、镉、汞、砷、铬、铝、锰、铜、钡、钒、硒、锑、镍、锡、锂、硼、锌、铁、锶、钼、钴和铷等22种元素含量。结果:120份茶叶样品所检的22种元素中有限量要求的铅、镉、汞、砷、铬和铜均未超出限量要求,日照茶叶与外地茶叶中镉、锰、钡、钒、镍、锂、铁、锶、钴和铷元素在数值上的差异有统计学意义,日照红茶与日照绿茶中所检22种元素含量在数值上的差异均无统计学意义。结论:日照辖区内市场上所销售的茶叶就所限制元素的限量要求而言,不存在食品安全风险。 展开更多
关键词 茶叶 元素 含量
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政策扩散量化研究方法述评
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作者 梁晓贺 周爱莲 张毅 《现代情报》 北大核心 2025年第2期87-96,共10页
[目的/意义]政策扩散量化分析是政策文献量化分析在政策扩散领域的应用研究,是一种跨学科的研究方向。本文从理论、方法和应用3个维度,系统梳理了政策扩散量化研究的最新进展,可以指导密集性政策文本扩散分析实践。[方法/过程]文章阐释... [目的/意义]政策扩散量化分析是政策文献量化分析在政策扩散领域的应用研究,是一种跨学科的研究方向。本文从理论、方法和应用3个维度,系统梳理了政策扩散量化研究的最新进展,可以指导密集性政策文本扩散分析实践。[方法/过程]文章阐释政策扩散量化的概念内涵、数据特点、研究框架以及应用范围。在方法层面,分为政策扩散计量分析和政策扩散文本挖掘方法两类;在应用层面,主要有政策扩散影响研究、扩散模式研究和扩散结构评估研究。[结果/结论]政策扩散量化研究发展迅速,多集中在跨学科领域的迁移与应用,未来还需在专属研究工具开发、融通方法创新与数据类型拓展上下功夫。 展开更多
关键词 政策扩散 量化研究 引用关系 方法述评 内容关联
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空气煎炸对薯条丙烯酰胺及其中间产物形成的影响
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作者 李晶 张豪 +4 位作者 鲍涛 赵念思 夏书芹 侯娅琪 张敏 《食品与发酵工业》 北大核心 2025年第6期264-271,共8页
空气煎炸可以实现薯条无油煎炸的烹饪效果,但目前尚未明晰空气煎炸过程中高温热风烹饪参数对丙烯酰胺等潜在危害因子生成的影响。该文研究了空气煎炸温度和时间对薯条中丙烯酰胺形成的影响,借助液-质联用对关键中间产物5-羟甲基糠醛和α... 空气煎炸可以实现薯条无油煎炸的烹饪效果,但目前尚未明晰空气煎炸过程中高温热风烹饪参数对丙烯酰胺等潜在危害因子生成的影响。该文研究了空气煎炸温度和时间对薯条中丙烯酰胺形成的影响,借助液-质联用对关键中间产物5-羟甲基糠醛和α-二羰基化合物的积累进行追踪,并考察了水分含量的变化规律,探索了空气煎炸过程中丙烯酰胺形成的机制。结果表明,丙烯酰胺的含量随空气煎炸温度的提高而增加,且随着加热时间的延长呈先升后降的趋势;丙烯酰胺的生成与5-羟甲基糠醛和水分含量呈极显著相关,相关系数分别为0.846(P<0.01)和-0.891(P<0.01),而5-羟甲基糠醛的生成也与3-脱氧葡糖醛酮的含量呈显著正相关(r=0.631,P<0.05)。因此可以通过抑制5-羟甲基糠醛等中间产物的生成以及减少烹饪的水分损失等,来抑制空气煎炸薯条中丙烯酰胺的生成。 展开更多
关键词 空气煎炸 丙烯酰胺 5-羟甲基糠醛 α-二羰基化合物 水分含量
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低含沙水流低速冲蚀混凝土特性试验研究
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作者 顾磊 戴福旭 +2 位作者 李洪彬 王顺 刘勇 《振动与冲击》 北大核心 2025年第4期238-243,252,共7页
低含沙水流低速冲蚀是水工混凝土结构长期服役面临的普遍而又极易忽略的问题。为研究其磨蚀的关键影响因素与规律,设计了一种低含沙低速射流冲刷试验装置,对6种不同配比的混凝土试样开展了4组共计23次长时间冲蚀试验,并且基于试样质量... 低含沙水流低速冲蚀是水工混凝土结构长期服役面临的普遍而又极易忽略的问题。为研究其磨蚀的关键影响因素与规律,设计了一种低含沙低速射流冲刷试验装置,对6种不同配比的混凝土试样开展了4组共计23次长时间冲蚀试验,并且基于试样质量磨损量的精确测量,分析了射流特征参数及混凝土关键掺量对混凝土磨损的影响。试验结果表明,低含沙水流低速冲蚀混凝土的作用可分为法向冲蚀和切向磨削两种作用,速度、面积相同时法向冲蚀的磨损效果高于切向磨削。随着冲刷时间发展,混凝土小时磨损量逐渐降低后趋于某一稳定值。在试验条件范围内,小时磨损量随着射流冲刷速度和含沙量的提高而有所增大,在大冲刷角度时具有较高的小时磨损量。适当增加硅粉及纤维掺量有助于提高混凝土的抗冲蚀性能。并最终建立了最优配比混凝土的含沙水流冲蚀预测模型,以期为混凝土的使用寿命评估和性能提升提供依据。 展开更多
关键词 混凝土 小时磨损量 低含沙射流 低速冲蚀 试验
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纤维特性对磷酸镁基免蒸压加气混凝土性能的影响
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作者 陈畅 丁学成 +1 位作者 酒少武 陈延信 《材料导报》 北大核心 2025年第10期94-100,共7页
免蒸压加气混凝土(NAAC)存在强度低和易开裂的问题。本工作采用磷酸镁水泥(MPC)作为基体制备磷酸镁基免蒸压加气混凝土(MPC-NAAC),通过添加聚丙烯纤维和玻璃纤维对其进行增强,系统研究了纤维长度和掺量对其物理、力学和耐水性能的影响;... 免蒸压加气混凝土(NAAC)存在强度低和易开裂的问题。本工作采用磷酸镁水泥(MPC)作为基体制备磷酸镁基免蒸压加气混凝土(MPC-NAAC),通过添加聚丙烯纤维和玻璃纤维对其进行增强,系统研究了纤维长度和掺量对其物理、力学和耐水性能的影响;并采用X射线衍射仪和扫描电镜分析其微观结构,揭示了纤维的增强机理。研究结果表明:纤维可以在降低MPC-NAAC干密度的同时提高其抗压和抗折强度,聚丙烯纤维和玻璃纤维的最佳长度均为9 mm,最佳掺量均为0.1%。此时,聚丙烯纤维增强的MPC-NAAC抗压和抗折强度较对照组分别提高了5.95%和16.46%;玻璃纤维增强的MPC-NAAC抗压和抗折强度较对照组分别提高了12.70%和11.39%。此外,纤维与基体之间的作用是物理作用,聚丙烯纤维表现出拔出破坏机制,玻璃纤维表现出断裂破坏机制。 展开更多
关键词 磷酸镁水泥 纤维长度 纤维掺量 力学性能 微观结构
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