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Extraction optimization of coumarins from radix angelicae pubescentis by HPLC-DAD coupled with uniform design 被引量:1
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作者 郭方遒 黄兰芳 +1 位作者 周火飞 江秋菊 《Journal of Central South University of Technology》 EI 2006年第2期156-159,共4页
Uniform design was used to optimize extraction condition of direct refluence extraction of coumarins from the Chinese traditional medicine of radix angelicae pubescentis(Duhuo); the sum peak area of coumarins separate... Uniform design was used to optimize extraction condition of direct refluence extraction of coumarins from the Chinese traditional medicine of radix angelicae pubescentis(Duhuo); the sum peak area of coumarins separated with high performance liquid chromatography(HPLC) at detection wavelength of 320nm was considered as detection index, two factors of solvent concentration and extraction time were mainly studied at extraction temperature of 85℃ and a volume ratio of solvent to sample of 10∶1. Optimal subclass, quadric polynomial step by step aggression and neural network method were applied to process the experimental results. The results show that the first and second methods give the same factors combination (concentration of ethanol: 95%, extraction time: 3.6 h) and the second method is much better than the first one. The extraction model is consequently developed. 展开更多
关键词 radix angelicae pubescentis(Duhuo) couamrins uniform design high performance liquid chromatagraphy-diode array detectorhplc-dad
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Multi-area detection sensitivity calculation model and detection blind areas influence analysis of photoelectric detection target 被引量:2
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作者 Han-shan Li Xiao-qian Zhang Hui Guan 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2022年第4期547-556,共10页
Multi-element array photoelectric detector is the core devices to form a photoelectric detection target with a large field of view.This photoelectric detection target brings about the problem of uneven detection sensi... Multi-element array photoelectric detector is the core devices to form a photoelectric detection target with a large field of view.This photoelectric detection target brings about the problem of uneven detection sensitivity distribution in the detection screen.To improve the uneven detection sensitivity of this photoelectric detection target,this paper analyzes the distribution law of the uneven detection sensitivity of the photoelectric detection target using the multi-element array photoelectric detector,dissects the main factors affecting the detection sensitivity according to the photoelectric detection principle,establishes the calculation model of detection sensitivity of the photoelectric detection target in the different detection areas and proposes a method to improve the detection sensitivity by compensating the gain of each unit photoelectric detector.The analysis of simulation and experimental results show that the proposed method of photoelectric detection target can effectively improve the output signal amplitude of the projectile under the certain detection distance,in particular,the output signal amplitude of the projectile is significantly increased when the projectile passes through the detection blind area.The experimental results are consistent with the simulation results,which verify the effectiveness of the proposed improvement method. 展开更多
关键词 PROJECTILE Photoelectric detection target Multi-element array photoelectric detector Detection sensitivity Detection screen
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