Aluminum foam is widely used in diverse areas to minimize the weight and maximize the absorption of shock energy in lightweight structures and various bio-materials.It presents a number of advantages,such as low densi...Aluminum foam is widely used in diverse areas to minimize the weight and maximize the absorption of shock energy in lightweight structures and various bio-materials.It presents a number of advantages,such as low density,incombustibility,non-rigidity,excellent energy absorptivity,sound absorptivity and low heat conductivity.The aluminum foam with an air cell structure was placed under the TDCB Mode II tensile load by using Landmark equipment manufactured by MTS to examine the shear failure behavior.The angle of the tapered adhesively-bonded surfaces of specimens was designated as a variable,and three models were developed with the inclined angles differing from one another at 6°,8° and 10°.The specimens with the inclined angles of 6°,8° and 10° have the maximum reaction forces of 168 N,194 N when the forced displacements are 6,5 and 4.2 mm respectively.There are three specimens with the inclined angles of 10°,8° and 6° in the order of maximum reaction force.As the analysis result,the maximum equivalent stresses of 0.813 MPa and 0.895 MPa happened when the forced displacements of 6 mm and 5 mm proceeded at the models of 6° and 8°,respectively.A simulation was carried out on the basis of finite element method and the experimental design.The results of the experiment and the simulation analysis are shown not different from each other significantly.Thus,only a simulation could be confirmed to be performed in substitution of an experiment,which is costly and time-consuming in order to determine the shearing properties of materials made of aluminum foam with artificial data.展开更多
The key parameters of the adhesive layer of a reinforcing patch are of great significance and affect the ability to suppress crack propagation in an Al–Li alloy patch-reinforced structure.This paper proposes a method...The key parameters of the adhesive layer of a reinforcing patch are of great significance and affect the ability to suppress crack propagation in an Al–Li alloy patch-reinforced structure.This paper proposes a method to determine the key parameters of the adhesive layer of adhesively bonded joints in the Al–Li alloy patch-reinforced structure.A zero-thickness cohesive zone model(CZM)was selected to simulate the adhesive layer’s fracture process,and an orthogonal simulation was designed to compare against the test results.A three-dimensional progressive damage model of an Al–Li alloy patch-reinforced structure with single-lap adhesively bonded joints was developed.The simulation’s results closely agree with the test results,demonstrating that this method of determining the key parameters is likely accurate.The results also verify the correctness of the cohesive strength and fracture energy,the two key parameters of the cohesive zone model.The model can accurately predict the strength and fracture process of adhesively bonded joints,and can be used in research to suppress crack propagation in Al–Li alloy patch-reinforced structures.展开更多
The effect of introducing attenuation on Lamb wave dispersion curves is studied in this paper. Attenuation is introduced to a three-layered composite plate by an adhesive bond layer with viscous behavior. No changes a...The effect of introducing attenuation on Lamb wave dispersion curves is studied in this paper. Attenuation is introduced to a three-layered composite plate by an adhesive bond layer with viscous behavior. No changes are required to the transfer matrix formulation for the propagation of elastic waves. By introduction of a complex wavenumber, the model can be used to the propagation of attenuative Lamb waves. Numerical examples for a three-layered aluminium-epoxy-aluminium plate show that attenuation values of each mode in plates are related not only to attenuation, but also to the thickness of the bonded layer, which is in agreement with practical situations.展开更多
In view of the phenomenon that the adhesion strength between the surface of polyacrylonitrile-butadiene-styrene-polycarbonate(ABS-PC)copolymer and the electroless copper plating layer is relatively low.To solve the pr...In view of the phenomenon that the adhesion strength between the surface of polyacrylonitrile-butadiene-styrene-polycarbonate(ABS-PC)copolymer and the electroless copper plating layer is relatively low.To solve the problems of poor surface wettability and low surface roughness of the ABS-PC substrate,the N,N-dimethylformamide(DMF)-ethanol(C_(2)H_(5)OH)-water(H_(2)O)system was employed as the swelling system for the ABS-PC substrate.The effects of the DMF volume fraction in the swelling system and the swelling time on the swelling effect of ABS-PC at 35℃were investigated.KMnO_(4)-H_(2)SO_(4)-H_(2)O system was used as the etching system for ABS-PC substrate under the conditions of the volume ratio of water to sulfuric acid of 1﹕2,with KMnO_(4)content of 30 g/L,etching temperature of 60℃,and etching time of 25 min.The results indicate that dense pores with uniform sized are formed on the surface of the ABS-PC substrate surface after swelling and etching treatments,accompanied by an increase in surface roughness when the swelling temperature is 35℃,the DMF volume fraction in the swelling system is 80%,and the swelling time is 5 min.Furthermore,the content of C element on the surface of the ABS-PC substrate decreased,while that of O element increased,and the surface hydrophilicity is enhanced,which is attributed to two hydrophilic groups,-C=O and-COOH,being generated on the ABS-PC substrate surface,significantly improving the wettability of the ABS-PC substrate surface.Under the combination effects of high surface roughness and strong surface hydrophilicity,the adhesion strength between the ABS-PC substrate surface and the electroless copper plating layer reached to 0.81 kN/m,meeting the adhesion strength requirement of 0.70 kN/m in the industrial production.展开更多
Objective:Endometrial tuberculosis,which commonly affects women of reproductive age,is a significant cause of intrauterine adhesions(IUA),potentially leading to hypomenorrhea,amenorrhea,and infertility.Hysteroscopic a...Objective:Endometrial tuberculosis,which commonly affects women of reproductive age,is a significant cause of intrauterine adhesions(IUA),potentially leading to hypomenorrhea,amenorrhea,and infertility.Hysteroscopic adhesiolysis is the primary treatment for IUA;however,studies specifically addressing its efficacy in tuberculosisinduced IUA remain scarce.This study aims to evaluate the therapeutic outcomes of hysteroscopic adhesiolysis for IUA caused by endometrial tuberculosis.Methods:This retrospective cohort study included patients diagnosed with tuberculosisinduced IUA who underwent hysteroscopic adhesiolysis at the Third Xiangya Hospital of Central South University between May 2014 and October 2022.Clinical data including age,medical history,adhesion severity,surgical treatment,and reproductive outcomes were analyzed.Results:Among 39 patients identified,2 were lost to follow-up.A total of 37 patients were included,with a follow-up duration ranging from 6 months to 9 years.Hypomenorrhea was reported in 24(64.9%)patients,secondary amenorrhea in 10(27.0%)patients,and normal menstruation in 3(8.1%)patients.Most patients presented with primary infertility(59.5%),and only 2(5.4%)had secondary infertility.The median American Fertility Society(AFS)score at initial assessment was 10(range,8−12);8(21.6%)patients had moderate IUA,and 29(78.4%)had severe IUA.A total of 86 surgical procedures were performed across 37 patients,with 27 patients undergoing 2 or more surgeries.Postoperatively,25(67.6%)patients achieved normalization of the uterine cavity,while 12(32.4%)still had a reduced cavity.Only 7(18.9%)patients had a grossly normal endometrium at the final surgery,all of whom had moderate adhesions at the initial procedure.Menstrual flow returned to normal in 12(32.4%)patients,while 25(67.6%)continued to experience hypomenorrhea.Of 29 patients who attempted in vitro fertilization and embryo transfer(IVF-ET),only 6(20.7%)conceived.Among these,4(13.8%)delivered at term via cesarean section;one case was complicated by postpartum hemorrhage due to uterine atony and another by placental adhesion.Conclusion:Endometrial tuberculosis can lead to severe IUA.Hysteroscopic adhesiolysis facilitates cavity restoration and improvement of menstrual conditions,but the overall reproductive outcomes remain suboptimal.展开更多
The role of the adhesive layer in the ballistic performance of ceramic multi-layer armour system is complex and multi-faceted,often with trade-offs between single-and multi-hit performance.However,research focused on ...The role of the adhesive layer in the ballistic performance of ceramic multi-layer armour system is complex and multi-faceted,often with trade-offs between single-and multi-hit performance.However,research focused on untangling the underlying impact of varying adhesive cohesive or adhesion properties is limited and sometimes appears to provide conflicting conclusions.Comparison between the available studies is also often difficult due to variations in armour systems or ballistic testing being conducted.This review scrutinises the available research,identifying six critical properties of an adhesive layer in determining ballistic performance:elastic modulus,fracture strain,acoustic impedance,tensile bond strength,shear bond strength,and thickness.The impact of each of these properties on ballistic performance is discussed in detail,with clear description of the underlying processes involved,allowing clear optimisation goals to be established depending on the ceramic armour specification.展开更多
粘连性肩关节囊炎（adhesive capsulitis of shoulder）是因多种原因致肩盂肱关节囊炎性粘连、僵硬,以肩关节周围疼痛,各方向活动受限和轻度骨质疏松为其临床特点[1],病程长、痛苦大、功能恢复不全,积极治疗可以缩短病程,加速痊愈。笔...粘连性肩关节囊炎（adhesive capsulitis of shoulder）是因多种原因致肩盂肱关节囊炎性粘连、僵硬,以肩关节周围疼痛,各方向活动受限和轻度骨质疏松为其临床特点[1],病程长、痛苦大、功能恢复不全,积极治疗可以缩短病程,加速痊愈。笔者观察了关节腔注射透明质酸钠与手法松解联合治疗粘连性肩关节囊炎的疗效,结果满意,现报告如下。展开更多
Paint removal from steel structure is executed for shipyards of marine and offshore engineering.Due to environmental unfriendliness and unhealthy drawbacks of sand blasting technique, laser ablation technique is propo...Paint removal from steel structure is executed for shipyards of marine and offshore engineering.Due to environmental unfriendliness and unhealthy drawbacks of sand blasting technique, laser ablation technique is proposed as a substituting method.By absorbing high energy of the 1064 nm pulsed laser, the paint is vaporized quickly.The ablated debris is then collected by using a suction pump.Initial metal surface of the steel is exposed when laser beam irradiates perpendicularly and scans over it.The cleaned surface fulfills the requirements of surface preparation standards ISO 8501 of SA2.The adhesion is further characterized with pull-off test after carrying out painting with Jotamastic 87 aluminum paint.The repainting can be embedded onto the laser cleaned surface to bond much more tightly.The excellent adhesion strength of 20 MPa between repainted coating and the substrate is achieved, which is higher than what is required by shipyards applications.展开更多
In the present work,TiAlN coatings were deposited on Ti(C,N)-based cermet substrates by physical vapor deposition method.Emphasis was focused on the influence of grain size of cermet substrates on the microstructure,g...In the present work,TiAlN coatings were deposited on Ti(C,N)-based cermet substrates by physical vapor deposition method.Emphasis was focused on the influence of grain size of cermet substrates on the microstructure,growth behavior,mechanical properties,adhesion strength and wear behavior of the coatings.The results show that finer Ti(C,N)grain size leads to higher nucleation density and lower growth rate of coatings,indicating the crystallite size of the TiAlN coatings decreases with decreasing Ti(C,N)grain size.Nanoindentation tests show that the coatings deposited on cermets of the finest grain size exhibit the highest hardness(H),elastic modulus(E),H/E and H3/E2 of 34.5 GPa,433.2 GPa,0.080 and 0.22,respectively.The adhesion strength between coating and substrate is also enhanced with decreasing Ti(C,N)grain size by scratch test,which corresponds to the grain size and H/E and H3/E2 of the coating.Besides,the lower surface roughness and better mechanical properties of the coating deposited on finer grained cermet contribute to the better wear resistance of the coating.展开更多
Non lubricated slide performance of functional grade copper matrix composite,fabricated using horizontal centrifuge cast technique was investigated using pin-on-disc tribo-tester.Rate of wear and friction coefficient ...Non lubricated slide performance of functional grade copper matrix composite,fabricated using horizontal centrifuge cast technique was investigated using pin-on-disc tribo-tester.Rate of wear and friction coefficient of the inner wall thickness of hollow cylindrical cast specimen was analyzed using Taguchi based L27 orthogonal array,where the percentage of graphite particles were observed higher.Variable process parameters those influenced the rate of wear directly or indirectly were:applied load(15,25 and 35 N),slide velocity(1.5,2.5 and 3.5 m/s)and slide distance(750,1500 and 2250 m).Rate of wear and friction coefficient showed a proportional dependency with applied load and slide distance,whereas showing a decline during intermediate slide velocity.Signal-to-Noise ratio predicted the minimal tribo-condition,on‘smaller-the-better’basis.Analysis of Variance technique quantified the influence of affecting parameters,along with their interactions.Regression analysis was utilized for the validation of the experimental data.Micrographs and scanning electron microscopy exhibited the wear mechanisms and mechanically mixed layer formation during worn surfaces analysis.展开更多
Diamond-coated tools were fabricated using Co-cemented carbide inserts as substrates by the electronically aided hot filament chemical vapor deposition (EACVD). An amount of additive in an acid solution was used to pr...Diamond-coated tools were fabricated using Co-cemented carbide inserts as substrates by the electronically aided hot filament chemical vapor deposition (EACVD). An amount of additive in an acid solution was used to promote the Co etching of the substrate surface. The surface of the WC-Co substrate was decarburized by microwave plasma with Ar-H 2 gas. Effect of the new substrate pretreatment on the adhesion of diamond films was investigated. A boron-doped solution was brushed on the tool surface to diffuse boron into the substrates during diamond deposition. A new process was used to lower the surface roughness of diamond thin films by appropriately controlling deposition parameters. It consists of a composite diamond film chemical vapor deposition procedure including first the deposition of the rough polycrystalline diamond and then the fine-grained diamond. The research results show that the pretreatment including both Co etching in acid solution and Ar-H 2 etching decarburization by microwave plasma is an effective method to enhance adhesive strength. An adequate amount of boron dopant solution can effectively suppress the cobalt diffusion to the surface and avoid the catalytic effect of Co at the high temperature. The composite film CVD process can deposit smooth diamond films with low surface roughness. It is of great significance for improvement of the cutting performances of diamond-coated tools using the above new technology to deposit diamond coatings with the low surface roughness and high adhesive strength on WC-Co substrates.展开更多
The preparation process of electrically conductive filler for anisotropic conductive adhesive was performed and discussed.The spherical filler contains tri-layer structures: resin core,Ni-P intermediate coating layer,...The preparation process of electrically conductive filler for anisotropic conductive adhesive was performed and discussed.The spherical filler contains tri-layer structures: resin core,Ni-P intermediate coating layer,Au outer coating layer.The 4 μm resin spherical cores were synthesized by monodispersion polymerization method.Then they were contributed to electrical conductivity by electrolessly plating Ni-P layer and gold layer.These particles have good corrosion resistance,high stability,and enough mechanical strength.When mixed with thermosetting epoxy resin to produce anisotropic conductive adhesive(ACA),it can realize a good conductive bonding between bumps on dies and pads on substrates.This environmentally friendly conductive material offers numerous advantages over conventional solder technology and is an ideal substitute for the lead-contained solder in electronics packaging.展开更多
Epoxy structural adhesives and composites have been in use for many years for the construction of aerospace vehicles. Henkel provides many epoxy products. Many other resin systems have been evaluated and several, such...Epoxy structural adhesives and composites have been in use for many years for the construction of aerospace vehicles. Henkel provides many epoxy products. Many other resin systems have been evaluated and several, such as imide, phenolic and cyanate ester, have also achieved significant use. Henkel’s newly developed “Epsilon” chemistry demonstrates unique features that benefit application in aerospace structure that use adhesives and composites.展开更多
The adhesion between the mining machine and the deep-sea sediments will significantly affect the driving performance of the mining machine in the deep-sea environment.When the mining machine and the deep-sea sediment ...The adhesion between the mining machine and the deep-sea sediments will significantly affect the driving performance of the mining machine in the deep-sea environment.When the mining machine and the deep-sea sediment interaction simulation was carried out,the accuracy of the particle interaction parameters will directly affect the simulation results.This study proposed a method to systematically calibrate the interaction parameters between deep-sea sediment and grouser through the combination of experiment and simulation.The uniaxial compression test and macro adhesion test and corresponding discrete element numerical simulation were carried out,modifying the contact parameters until the simulation results are close to the experimental results.Then the micro-parameters of the JKR adhesion contact model were back calibrated with the test results,and the contact parameters between soil particle-soil particle and soil particle-metal are calibrated.Besides,the adhesion test shows that the adhesion forces were ranked in the order of 5052<STi80<TA2<TC4 under the same surface roughness,which indicates the aluminum alloy 5052 has the best anti-adhesion performance.The relationship between surface adhesion force and microscopic contact parameters was studied by discrete element numerical simulation,and the result shows that the coefficient of static friction and the coefficient of rolling friction has little effect on adhesion force.While it is mainly affected by the coefficient of restitution and surface energy,the surface adhesion force tends to decrease with the increase of the coefficient of restitution and increase with the growth of surface energy.The obtained parameters of soil particle to soil particle and soil particle to metal affecting the adhesion can contribute to the design optimization for the grouser of mining machines to decrease surface adhesion and enhance its movability and mining efficiency.展开更多
Inspired by the microstructure of gecko’s toe,two kinds of polyvinyl chloride(PVC)gels with different modulus were poured on a silicon mold with micropillars,and then a bio-inspired adhesive with variable modulus was...Inspired by the microstructure of gecko’s toe,two kinds of polyvinyl chloride(PVC)gels with different modulus were poured on a silicon mold with micropillars,and then a bio-inspired adhesive with variable modulus was manufactured in this study.The adhesions of variable modulus and fixed modulus bio-inspired adhesives were tested,respectively,on a smooth glass and a printed circuit board(PCB)with different surface structures.The results show that PVC gel bio-inspired adhesives with variable modulus have many advantages compared with the fixed modulus bioinspired adhesives.The adhesion of variable modulus bio-inspired adhesives on the rough PCB surface increased by 2−5 times,and due to the use of variable modulus of PVC gel,the surface micropillars can maintain high aspect ratio and flexible tips at the same time.Moreover,the use of PVC gel makes it easier to demold during the bio-inspired adhesives preparation.An adhesion-desorption device was made according to the movement of the gecko toes,and the PCB was successfully grasped.展开更多
This paper describes a new technique for the roadway dust control in surface mine. In the method, the emulsified tar liquid with low concentration and the super water-absorbing resin are taken as dust adhesive and spr...This paper describes a new technique for the roadway dust control in surface mine. In the method, the emulsified tar liquid with low concentration and the super water-absorbing resin are taken as dust adhesive and sprayed on the roadway. After doing a large number of in-situ experiments, the technique has shown its excellent characteristics on sticking dust, preventing water evaporation and reducing the combined cost of truck transportation.展开更多
基金Project(2011-0006548)supported by Basic Science Research Program through the National Research Foundation of Korea
文摘Aluminum foam is widely used in diverse areas to minimize the weight and maximize the absorption of shock energy in lightweight structures and various bio-materials.It presents a number of advantages,such as low density,incombustibility,non-rigidity,excellent energy absorptivity,sound absorptivity and low heat conductivity.The aluminum foam with an air cell structure was placed under the TDCB Mode II tensile load by using Landmark equipment manufactured by MTS to examine the shear failure behavior.The angle of the tapered adhesively-bonded surfaces of specimens was designated as a variable,and three models were developed with the inclined angles differing from one another at 6°,8° and 10°.The specimens with the inclined angles of 6°,8° and 10° have the maximum reaction forces of 168 N,194 N when the forced displacements are 6,5 and 4.2 mm respectively.There are three specimens with the inclined angles of 10°,8° and 6° in the order of maximum reaction force.As the analysis result,the maximum equivalent stresses of 0.813 MPa and 0.895 MPa happened when the forced displacements of 6 mm and 5 mm proceeded at the models of 6° and 8°,respectively.A simulation was carried out on the basis of finite element method and the experimental design.The results of the experiment and the simulation analysis are shown not different from each other significantly.Thus,only a simulation could be confirmed to be performed in substitution of an experiment,which is costly and time-consuming in order to determine the shearing properties of materials made of aluminum foam with artificial data.
基金Project(51575535)supported by the National Natural Science Foundation of ChinaProject(2015CX002)supported by the Innovation-driven Plan in Central South University,China+2 种基金Project(zzyjkt2013-09B)supported by the Fund of the State Key Laboratory of High Performance Manufacturing,ChinaProject(2017zzts638)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(2016RS2015)supported by the Scientific and Technological Leading Talent Projects of Hunan Province,China
文摘The key parameters of the adhesive layer of a reinforcing patch are of great significance and affect the ability to suppress crack propagation in an Al–Li alloy patch-reinforced structure.This paper proposes a method to determine the key parameters of the adhesive layer of adhesively bonded joints in the Al–Li alloy patch-reinforced structure.A zero-thickness cohesive zone model(CZM)was selected to simulate the adhesive layer’s fracture process,and an orthogonal simulation was designed to compare against the test results.A three-dimensional progressive damage model of an Al–Li alloy patch-reinforced structure with single-lap adhesively bonded joints was developed.The simulation’s results closely agree with the test results,demonstrating that this method of determining the key parameters is likely accurate.The results also verify the correctness of the cohesive strength and fracture energy,the two key parameters of the cohesive zone model.The model can accurately predict the strength and fracture process of adhesively bonded joints,and can be used in research to suppress crack propagation in Al–Li alloy patch-reinforced structures.
文摘The effect of introducing attenuation on Lamb wave dispersion curves is studied in this paper. Attenuation is introduced to a three-layered composite plate by an adhesive bond layer with viscous behavior. No changes are required to the transfer matrix formulation for the propagation of elastic waves. By introduction of a complex wavenumber, the model can be used to the propagation of attenuative Lamb waves. Numerical examples for a three-layered aluminium-epoxy-aluminium plate show that attenuation values of each mode in plates are related not only to attenuation, but also to the thickness of the bonded layer, which is in agreement with practical situations.
文摘In view of the phenomenon that the adhesion strength between the surface of polyacrylonitrile-butadiene-styrene-polycarbonate(ABS-PC)copolymer and the electroless copper plating layer is relatively low.To solve the problems of poor surface wettability and low surface roughness of the ABS-PC substrate,the N,N-dimethylformamide(DMF)-ethanol(C_(2)H_(5)OH)-water(H_(2)O)system was employed as the swelling system for the ABS-PC substrate.The effects of the DMF volume fraction in the swelling system and the swelling time on the swelling effect of ABS-PC at 35℃were investigated.KMnO_(4)-H_(2)SO_(4)-H_(2)O system was used as the etching system for ABS-PC substrate under the conditions of the volume ratio of water to sulfuric acid of 1﹕2,with KMnO_(4)content of 30 g/L,etching temperature of 60℃,and etching time of 25 min.The results indicate that dense pores with uniform sized are formed on the surface of the ABS-PC substrate surface after swelling and etching treatments,accompanied by an increase in surface roughness when the swelling temperature is 35℃,the DMF volume fraction in the swelling system is 80%,and the swelling time is 5 min.Furthermore,the content of C element on the surface of the ABS-PC substrate decreased,while that of O element increased,and the surface hydrophilicity is enhanced,which is attributed to two hydrophilic groups,-C=O and-COOH,being generated on the ABS-PC substrate surface,significantly improving the wettability of the ABS-PC substrate surface.Under the combination effects of high surface roughness and strong surface hydrophilicity,the adhesion strength between the ABS-PC substrate surface and the electroless copper plating layer reached to 0.81 kN/m,meeting the adhesion strength requirement of 0.70 kN/m in the industrial production.
基金supported by the Wisdom Accumulation and Talent Cultivation Project of Third Xiangya Hosipital of Central South University,China(YX202112).
文摘Objective:Endometrial tuberculosis,which commonly affects women of reproductive age,is a significant cause of intrauterine adhesions(IUA),potentially leading to hypomenorrhea,amenorrhea,and infertility.Hysteroscopic adhesiolysis is the primary treatment for IUA;however,studies specifically addressing its efficacy in tuberculosisinduced IUA remain scarce.This study aims to evaluate the therapeutic outcomes of hysteroscopic adhesiolysis for IUA caused by endometrial tuberculosis.Methods:This retrospective cohort study included patients diagnosed with tuberculosisinduced IUA who underwent hysteroscopic adhesiolysis at the Third Xiangya Hospital of Central South University between May 2014 and October 2022.Clinical data including age,medical history,adhesion severity,surgical treatment,and reproductive outcomes were analyzed.Results:Among 39 patients identified,2 were lost to follow-up.A total of 37 patients were included,with a follow-up duration ranging from 6 months to 9 years.Hypomenorrhea was reported in 24(64.9%)patients,secondary amenorrhea in 10(27.0%)patients,and normal menstruation in 3(8.1%)patients.Most patients presented with primary infertility(59.5%),and only 2(5.4%)had secondary infertility.The median American Fertility Society(AFS)score at initial assessment was 10(range,8−12);8(21.6%)patients had moderate IUA,and 29(78.4%)had severe IUA.A total of 86 surgical procedures were performed across 37 patients,with 27 patients undergoing 2 or more surgeries.Postoperatively,25(67.6%)patients achieved normalization of the uterine cavity,while 12(32.4%)still had a reduced cavity.Only 7(18.9%)patients had a grossly normal endometrium at the final surgery,all of whom had moderate adhesions at the initial procedure.Menstrual flow returned to normal in 12(32.4%)patients,while 25(67.6%)continued to experience hypomenorrhea.Of 29 patients who attempted in vitro fertilization and embryo transfer(IVF-ET),only 6(20.7%)conceived.Among these,4(13.8%)delivered at term via cesarean section;one case was complicated by postpartum hemorrhage due to uterine atony and another by placental adhesion.Conclusion:Endometrial tuberculosis can lead to severe IUA.Hysteroscopic adhesiolysis facilitates cavity restoration and improvement of menstrual conditions,but the overall reproductive outcomes remain suboptimal.
基金funding for this research was provided by Netherlands Ministry of Defence
文摘The role of the adhesive layer in the ballistic performance of ceramic multi-layer armour system is complex and multi-faceted,often with trade-offs between single-and multi-hit performance.However,research focused on untangling the underlying impact of varying adhesive cohesive or adhesion properties is limited and sometimes appears to provide conflicting conclusions.Comparison between the available studies is also often difficult due to variations in armour systems or ballistic testing being conducted.This review scrutinises the available research,identifying six critical properties of an adhesive layer in determining ballistic performance:elastic modulus,fracture strain,acoustic impedance,tensile bond strength,shear bond strength,and thickness.The impact of each of these properties on ballistic performance is discussed in detail,with clear description of the underlying processes involved,allowing clear optimisation goals to be established depending on the ceramic armour specification.
文摘粘连性肩关节囊炎（adhesive capsulitis of shoulder）是因多种原因致肩盂肱关节囊炎性粘连、僵硬,以肩关节周围疼痛,各方向活动受限和轻度骨质疏松为其临床特点[1],病程长、痛苦大、功能恢复不全,积极治疗可以缩短病程,加速痊愈。笔者观察了关节腔注射透明质酸钠与手法松解联合治疗粘连性肩关节囊炎的疗效,结果满意,现报告如下。
基金supported by the National Natural Science Foundation of China (U1609209)National Natural Science Foundation of China (61605162)+2 种基金NSFC-Liaoning Province united foundation (U1608259)National Natural Science Foundation of China (51501219)the financial support from the China Scholarship Council
文摘Paint removal from steel structure is executed for shipyards of marine and offshore engineering.Due to environmental unfriendliness and unhealthy drawbacks of sand blasting technique, laser ablation technique is proposed as a substituting method.By absorbing high energy of the 1064 nm pulsed laser, the paint is vaporized quickly.The ablated debris is then collected by using a suction pump.Initial metal surface of the steel is exposed when laser beam irradiates perpendicularly and scans over it.The cleaned surface fulfills the requirements of surface preparation standards ISO 8501 of SA2.The adhesion is further characterized with pull-off test after carrying out painting with Jotamastic 87 aluminum paint.The repainting can be embedded onto the laser cleaned surface to bond much more tightly.The excellent adhesion strength of 20 MPa between repainted coating and the substrate is achieved, which is higher than what is required by shipyards applications.
基金Projects(51634006,51575368)supported by the National Natural Science Foundation of ChinaProject(2017GZ0041)supported by Science and Technology Support Program of Sichuan Province,China。
文摘In the present work,TiAlN coatings were deposited on Ti(C,N)-based cermet substrates by physical vapor deposition method.Emphasis was focused on the influence of grain size of cermet substrates on the microstructure,growth behavior,mechanical properties,adhesion strength and wear behavior of the coatings.The results show that finer Ti(C,N)grain size leads to higher nucleation density and lower growth rate of coatings,indicating the crystallite size of the TiAlN coatings decreases with decreasing Ti(C,N)grain size.Nanoindentation tests show that the coatings deposited on cermets of the finest grain size exhibit the highest hardness(H),elastic modulus(E),H/E and H3/E2 of 34.5 GPa,433.2 GPa,0.080 and 0.22,respectively.The adhesion strength between coating and substrate is also enhanced with decreasing Ti(C,N)grain size by scratch test,which corresponds to the grain size and H/E and H3/E2 of the coating.Besides,the lower surface roughness and better mechanical properties of the coating deposited on finer grained cermet contribute to the better wear resistance of the coating.
文摘Non lubricated slide performance of functional grade copper matrix composite,fabricated using horizontal centrifuge cast technique was investigated using pin-on-disc tribo-tester.Rate of wear and friction coefficient of the inner wall thickness of hollow cylindrical cast specimen was analyzed using Taguchi based L27 orthogonal array,where the percentage of graphite particles were observed higher.Variable process parameters those influenced the rate of wear directly or indirectly were:applied load(15,25 and 35 N),slide velocity(1.5,2.5 and 3.5 m/s)and slide distance(750,1500 and 2250 m).Rate of wear and friction coefficient showed a proportional dependency with applied load and slide distance,whereas showing a decline during intermediate slide velocity.Signal-to-Noise ratio predicted the minimal tribo-condition,on‘smaller-the-better’basis.Analysis of Variance technique quantified the influence of affecting parameters,along with their interactions.Regression analysis was utilized for the validation of the experimental data.Micrographs and scanning electron microscopy exhibited the wear mechanisms and mechanically mixed layer formation during worn surfaces analysis.
文摘Diamond-coated tools were fabricated using Co-cemented carbide inserts as substrates by the electronically aided hot filament chemical vapor deposition (EACVD). An amount of additive in an acid solution was used to promote the Co etching of the substrate surface. The surface of the WC-Co substrate was decarburized by microwave plasma with Ar-H 2 gas. Effect of the new substrate pretreatment on the adhesion of diamond films was investigated. A boron-doped solution was brushed on the tool surface to diffuse boron into the substrates during diamond deposition. A new process was used to lower the surface roughness of diamond thin films by appropriately controlling deposition parameters. It consists of a composite diamond film chemical vapor deposition procedure including first the deposition of the rough polycrystalline diamond and then the fine-grained diamond. The research results show that the pretreatment including both Co etching in acid solution and Ar-H 2 etching decarburization by microwave plasma is an effective method to enhance adhesive strength. An adequate amount of boron dopant solution can effectively suppress the cobalt diffusion to the surface and avoid the catalytic effect of Co at the high temperature. The composite film CVD process can deposit smooth diamond films with low surface roughness. It is of great significance for improvement of the cutting performances of diamond-coated tools using the above new technology to deposit diamond coatings with the low surface roughness and high adhesive strength on WC-Co substrates.
基金The National Natural Science Foundation of China(No.10474024)NSFC-RGC Joint Research Scheme(No.60318002)+1 种基金Youth Chenguang Project of Science and Technology of Wuhan City of China(No.20065004116-10)StateKey Lab.of Advanced Technology for Materials Synthesis and Processing(Wuhan University of Technology,No.WUT2004 M08)
文摘The preparation process of electrically conductive filler for anisotropic conductive adhesive was performed and discussed.The spherical filler contains tri-layer structures: resin core,Ni-P intermediate coating layer,Au outer coating layer.The 4 μm resin spherical cores were synthesized by monodispersion polymerization method.Then they were contributed to electrical conductivity by electrolessly plating Ni-P layer and gold layer.These particles have good corrosion resistance,high stability,and enough mechanical strength.When mixed with thermosetting epoxy resin to produce anisotropic conductive adhesive(ACA),it can realize a good conductive bonding between bumps on dies and pads on substrates.This environmentally friendly conductive material offers numerous advantages over conventional solder technology and is an ideal substitute for the lead-contained solder in electronics packaging.
文摘Epoxy structural adhesives and composites have been in use for many years for the construction of aerospace vehicles. Henkel provides many epoxy products. Many other resin systems have been evaluated and several, such as imide, phenolic and cyanate ester, have also achieved significant use. Henkel’s newly developed “Epsilon” chemistry demonstrates unique features that benefit application in aerospace structure that use adhesives and composites.
基金Project(12072309)supported by the National Natural Science Foundation of ChinaProject(19B546)supported by the Education Department Foundation of Hunan Province,ChinaProject(2019RS1059)supported by the Hunan Innovative Province Construction Project,China。
文摘The adhesion between the mining machine and the deep-sea sediments will significantly affect the driving performance of the mining machine in the deep-sea environment.When the mining machine and the deep-sea sediment interaction simulation was carried out,the accuracy of the particle interaction parameters will directly affect the simulation results.This study proposed a method to systematically calibrate the interaction parameters between deep-sea sediment and grouser through the combination of experiment and simulation.The uniaxial compression test and macro adhesion test and corresponding discrete element numerical simulation were carried out,modifying the contact parameters until the simulation results are close to the experimental results.Then the micro-parameters of the JKR adhesion contact model were back calibrated with the test results,and the contact parameters between soil particle-soil particle and soil particle-metal are calibrated.Besides,the adhesion test shows that the adhesion forces were ranked in the order of 5052<STi80<TA2<TC4 under the same surface roughness,which indicates the aluminum alloy 5052 has the best anti-adhesion performance.The relationship between surface adhesion force and microscopic contact parameters was studied by discrete element numerical simulation,and the result shows that the coefficient of static friction and the coefficient of rolling friction has little effect on adhesion force.While it is mainly affected by the coefficient of restitution and surface energy,the surface adhesion force tends to decrease with the increase of the coefficient of restitution and increase with the growth of surface energy.The obtained parameters of soil particle to soil particle and soil particle to metal affecting the adhesion can contribute to the design optimization for the grouser of mining machines to decrease surface adhesion and enhance its movability and mining efficiency.
基金Projects(51605220,U1637101)supported by the National Natural Science Foundation of ChinaProject(BK20160793)supported by the Natural Science Foundation of Jiangsu Province,ChinaProject(NS2020029)supported by the Fundamental Research Funds for the Central Universities,China。
文摘Inspired by the microstructure of gecko’s toe,two kinds of polyvinyl chloride(PVC)gels with different modulus were poured on a silicon mold with micropillars,and then a bio-inspired adhesive with variable modulus was manufactured in this study.The adhesions of variable modulus and fixed modulus bio-inspired adhesives were tested,respectively,on a smooth glass and a printed circuit board(PCB)with different surface structures.The results show that PVC gel bio-inspired adhesives with variable modulus have many advantages compared with the fixed modulus bioinspired adhesives.The adhesion of variable modulus bio-inspired adhesives on the rough PCB surface increased by 2−5 times,and due to the use of variable modulus of PVC gel,the surface micropillars can maintain high aspect ratio and flexible tips at the same time.Moreover,the use of PVC gel makes it easier to demold during the bio-inspired adhesives preparation.An adhesion-desorption device was made according to the movement of the gecko toes,and the PCB was successfully grasped.
文摘This paper describes a new technique for the roadway dust control in surface mine. In the method, the emulsified tar liquid with low concentration and the super water-absorbing resin are taken as dust adhesive and sprayed on the roadway. After doing a large number of in-situ experiments, the technique has shown its excellent characteristics on sticking dust, preventing water evaporation and reducing the combined cost of truck transportation.
