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X-射线衍射技术及其在粮油食品中应用 被引量:4
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作者 聂作明 《粮食与油脂》 2003年第1期12-15,共4页
近年来,随着食品工业发展,X-射线衍射分析技术在食品中得到了越来越广泛应用。X-射线衍射分析对淀粉结晶结构与性质的研究已很广泛,它涉及到淀粉相对结晶度指数的测定,淀粉微晶参数的测定以及在不同处理过程中淀粉晶型转换规律的研究等... 近年来,随着食品工业发展,X-射线衍射分析技术在食品中得到了越来越广泛应用。X-射线衍射分析对淀粉结晶结构与性质的研究已很广泛,它涉及到淀粉相对结晶度指数的测定,淀粉微晶参数的测定以及在不同处理过程中淀粉晶型转换规律的研究等,其为‘人造’淀粉生物合成提供一定的理论依据。X-射线衍射技术对脂类的研究涉及到脂类的同质多晶现象,应用X-射线衍射技术对脂类晶型结构进行研究,为脂类在食品中进一步开发和应用展现良好前景。 展开更多
关键词 x-射线衍射技术 粮油食品 应用 结晶度 同质多晶 淀粉结晶
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Friction welding of AA6061 to AISI 4340 using silver interlayer 被引量:9
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作者 SURESH D.MESHRAM G.MADHUSUDHAN REDDY 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2015年第3期292-298,共7页
The present work pertains to the study on joining of AA6061 and AISI 4340 through continuous drive friction welding. The welds were evaluated by metallographic examination, X-ray diffraction, electron probe microanaly... The present work pertains to the study on joining of AA6061 and AISI 4340 through continuous drive friction welding. The welds were evaluated by metallographic examination, X-ray diffraction, electron probe microanalysis, tensile test and microhardness. The study reveals that the presence of an intermetallic compound layer at the bonded interface exhibits poor tensile strength and elongation. Mg in AA6061 near to the interface is found to be favourable for the formation and growth of Fe2Al5 intermetallics. Introduction of silver as an interlayer through electroplating on AISI 4340 resulted in accumulation of Si at weld interface, replacing Mg at AA6061 side, thereby reducing the width of intermetallic compound layer and correspondingly increasing the tensile strength. Presence of silver at the interface results in partial replacement of Fe-Al based intermetallic compounds with Ag-Al based compounds. The presence of these intermetallics was confirmed by X-ray diffraction technique. Since Ag-Al phases are ductile in nature, tensile strength is not deteriorated and the silicon segregation at weld interface on AA6061 in the joints with silver interlayer acts as diffusion barrier for Fe and further avoids formation of Fe-Al based intermetallics. A maximum tensile strength of 240 MPa along with 4.9% elongation was obtained for the silver interlayer dissimilar metal welds. The observed trends in tensile properties and hardness were explained in relation to the microstructure. 展开更多
关键词 AISI 摩擦焊接 金属间化合物层 x-射线衍射技术 焊接界面 博士 夹层
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纳米材料的三维透射电镜表征研究获重要进展
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《化工新型材料》 CAS CSCD 北大核心 2011年第5期136-136,共1页
通常,材料内部的微观结构信息是通过对截面样品的二维观察得到的,这种二维观察不能提供材料内部小品体在三维空间的相对分布和晶界特性等重要的微观结构参数,从而制约了对材料微观结构与宏观性能相互关系的深刻理解和材料性能的改进... 通常,材料内部的微观结构信息是通过对截面样品的二维观察得到的,这种二维观察不能提供材料内部小品体在三维空间的相对分布和晶界特性等重要的微观结构参数,从而制约了对材料微观结构与宏观性能相互关系的深刻理解和材料性能的改进和优化。近年来,在世界范围内,科学家们就开发先进的微观结构三维表征技术进行了不懈的努力探索,三维X-射线衍射技术的成功开发和应用就是一个重要例子。但是这种技术的空间分辨率只能达到lOOnm。 展开更多
关键词 纳米材料 三维空间 表征技术 透射电镜 微观结构参数 x-射线衍射技术 空间分辨率 结构信息
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高纯钽交叉轧制过程中微观结构和织构梯度的演变 被引量:5
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作者 毛宇成 刘施峰 +1 位作者 范海洋 刘庆 《电子显微学报》 CAS CSCD 2017年第1期7-13,共7页
高纯钽板在交叉轧制过程中,通过控制轧制的道次,得到了70%,82%和87%变形量的样品。应用X-射线衍射(XRD)技术测量了轧制样品1/8厚度层,1/4厚度层和中间层的宏观织构,并对样品沿厚度方向上的变形组织与微织构进行电子背散射衍射(EBSD)表... 高纯钽板在交叉轧制过程中,通过控制轧制的道次,得到了70%,82%和87%变形量的样品。应用X-射线衍射(XRD)技术测量了轧制样品1/8厚度层,1/4厚度层和中间层的宏观织构,并对样品沿厚度方向上的变形组织与微织构进行电子背散射衍射(EBSD)表征。结果表明,随着交叉轧制变形量的增加,{111}〈uvw〉和{100}〈uvw〉取向晶粒的取向分裂程度增加,并且{111}取向的晶粒分裂程度高于{100}取向的晶粒。变形量为70%时,高纯钽板沿厚度方向存在强烈的微观组织和织构梯度,中间层具有强烈的{111}〈uvw〉取向晶粒,而1/8厚度层主要为{100}〈uvw〉取向。随着变形量增加,高纯钽板沿厚度方向的微观组织和织构均匀性得到改善。当变形量达到87%时,表面和中心的{100}〈uvw〉和{111}〈uvw〉取向晶粒都为长条状且交互分布在一起,使得钽板沿厚度方向织构梯度得到减弱,同时获得均一的晶粒尺寸。 展开更多
关键词 交叉轧制 x-射线衍射(XRD)技术 电子背散射衍射(EBSD)技术 织构梯度 取向分裂
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Performance of interface between TRC and existing concrete under a chloride dry-wet cycle environment 被引量:4
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作者 LI Yao YIN Shi-ping LV Heng-lin 《Journal of Central South University》 SCIE EI CAS CSCD 2020年第3期876-890,共15页
Textile-reinforced concrete(TRC)is suitable to repair and reinforce concrete structures in harsh environments.The performance of the interface between TRC and existing concrete is an important factor in determining th... Textile-reinforced concrete(TRC)is suitable to repair and reinforce concrete structures in harsh environments.The performance of the interface between TRC and existing concrete is an important factor in determining the strengthening effect of TRC.In this paper,a double-sided shear test was performed to investigate the effects of the chloride dry-wet cycles on the average shear strength and slip at the interface between the TRC and existing concrete,also considering the existing concrete strength,bond length,textile layer and short-cut fiber arrangements.In addition,X-ray diffraction(XRD)technology was used to analyze the microscopic matter at the interface in the corrosive environment.The experimental results indicate that the interface performance between TRC and existing concrete would decrease with continued chloride dry-wet cycles.Compared with the specimen with a single layer of textile reinforcement,the specimens with two layers of textile with added PVA or AR-glass short-cut fibers could further improve the properties of the interface between the TRC layer and existing concrete.For the TRC with a single layer of textile,the average shear strength tended to decrease with increasing bond length.In addition,the strength grade of the existing concrete had a minor effect on the interface properties. 展开更多
关键词 textile-reinforced concrete chloride dry-wet cycles double-sided shear average shear strength interface slip x-ray diffraction technology
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