AlN particulate reinforced 6061 aluminum alloy composite was fabricated by powder metallurgy method and hot rolled after extrusion. Tensile strength and elongation at elevated temperature were measured by tensile test...AlN particulate reinforced 6061 aluminum alloy composite was fabricated by powder metallurgy method and hot rolled after extrusion. Tensile strength and elongation at elevated temperature were measured by tensile test at initial strain rates between 10 -2 s -1 and 10 0 s -1 . The AlNp/6061Al composite exhibits an m value of 0.42 and a maximum elongation of 450% at 863?K. Differential scanning calorimeter was used to ascertain the possibility of any partial melting in the vicinity of optimum superplastic temperature. Partial melting resulting from solute segregation at interfaces has much influence on superplasticity of the composite. It is postulated that AlNp/matrix interface sliding occurs along with grain boundary in superplastic deformation.展开更多
The superplasticity of Al-6Mg-0.4Mn-0.25Sc-0.12Zr and Al-6Mg-0.4Mn-0.25Er-0.12Zr(mass fraction,%)alloys sheet was investigated,and the effect of Sc and Er was discussed.The results show that the superplastic ductiliti...The superplasticity of Al-6Mg-0.4Mn-0.25Sc-0.12Zr and Al-6Mg-0.4Mn-0.25Er-0.12Zr(mass fraction,%)alloys sheet was investigated,and the effect of Sc and Er was discussed.The results show that the superplastic ductilities of Al-Mg-Mn-Sc-Zr alloy was higher than that of Al-Mg-Mn-Er-Zr alloy at a wide temperature range of 400-540°C and high strain rate range of1.67×10-4-1.67×10-1 s-1.A maximum elongation 673%is obtained at 520°C and 1.67×10-3 s-1 in the Sc-containing alloy;while the Er-containing alloy only gets a maximum elongation 253%at 520°C and 1.67×10-3 s-1.Moreover,the average stress exponent of Sc-containing alloy is about 2.84,which is smaller than that of Er-containing alloy(3.64).Besides,the activation energies of the Sc-containing and Er-containing alloy are 84.8 k J/mol and 87.2 k J/mol,respectively.It is indicated that grain boundary sliding is the dominant mechanism during tensile deformation.According to microstructure examination,the better superplasticity of Sc-containing alloy may be attributed to the presence of Al3_(Sc,Zr)dispersoids,which can inhibit recrystallization and grain growth effectively.展开更多
Based on current theories of diffusion and creep cavity closure at high temperature, a theoretical analysis of phase transformation diffusion bonding for T8/T8 eutectoid steel is carried out. The diffusion bonding is ...Based on current theories of diffusion and creep cavity closure at high temperature, a theoretical analysis of phase transformation diffusion bonding for T8/T8 eutectoid steel is carried out. The diffusion bonding is mainly described as two-stage process: Ⅰ The interfacial cavity with shape change from diamond to cylinder.Ⅱ The radius of the cylindrical cavity are reduced and eliminated gradually. A new theoretical model is established for the process of transformation superplastic diffusion bonding (TSDB) on the basis of a theoretical model for isothermal superplastic diffusion. The model can predict the bonding quality which is affected by technological parameters, such as limit cycling temperature, the compressive stress, the numbers of thermal cycles and temperature cycling through the phase transformation in the thermal cycling and so on. Results show that the maximum temperature, the compressive stress, the numbers of thermal cycles and the rate of temperature changing speed in the thermal cycling have an important influence on TSDB process. Meanwhile, reasonable technological parameters chosen from theoretical analysis is in good agreement with those obtained from experimental results.展开更多
True stress-true strain curve,microstructure and texture information were obtained to investigate the superplastic deformation behavior of 1420 Al-Li alloy sheets with initial elongated grains.From the true stress-tru...True stress-true strain curve,microstructure and texture information were obtained to investigate the superplastic deformation behavior of 1420 Al-Li alloy sheets with initial elongated grains.From the true stress-true curve,the stress increases with the increase of strain to 0.15,then dramatically decreases with the increase of strain to 0.80,and finally keeps almost a horizontal line.Meanwhile,initial elongated grains are gradually changed into equiaxed grains and the initial strong Brass {0 1 1} <2 1 1> and S {1 2 3} <6 3 4> orientations are turned into nearly random orientation with increasing strain.All these results suggest that dislocation activity is the dominant mechanism during the first stage,then dynamic recrystallization occurs,and grain rotation is expected as an accommodation for grain boundary sliding(GBS).At larger strains,grain boundary migration(GBM) becomes necessary to accommodate GBS.展开更多
文摘AlN particulate reinforced 6061 aluminum alloy composite was fabricated by powder metallurgy method and hot rolled after extrusion. Tensile strength and elongation at elevated temperature were measured by tensile test at initial strain rates between 10 -2 s -1 and 10 0 s -1 . The AlNp/6061Al composite exhibits an m value of 0.42 and a maximum elongation of 450% at 863?K. Differential scanning calorimeter was used to ascertain the possibility of any partial melting in the vicinity of optimum superplastic temperature. Partial melting resulting from solute segregation at interfaces has much influence on superplasticity of the composite. It is postulated that AlNp/matrix interface sliding occurs along with grain boundary in superplastic deformation.
基金Project(2014M552149) supported by the China Postdoctoral Science FoundationProject(CX2016B041) supported by the Hunan Provincial Innovation Foundation For Postgraduate,ChinaProject(CSUZC201614) supported by the Open-End Fund for the Valuable and Precision Instruments of Central South University,China
文摘The superplasticity of Al-6Mg-0.4Mn-0.25Sc-0.12Zr and Al-6Mg-0.4Mn-0.25Er-0.12Zr(mass fraction,%)alloys sheet was investigated,and the effect of Sc and Er was discussed.The results show that the superplastic ductilities of Al-Mg-Mn-Sc-Zr alloy was higher than that of Al-Mg-Mn-Er-Zr alloy at a wide temperature range of 400-540°C and high strain rate range of1.67×10-4-1.67×10-1 s-1.A maximum elongation 673%is obtained at 520°C and 1.67×10-3 s-1 in the Sc-containing alloy;while the Er-containing alloy only gets a maximum elongation 253%at 520°C and 1.67×10-3 s-1.Moreover,the average stress exponent of Sc-containing alloy is about 2.84,which is smaller than that of Er-containing alloy(3.64).Besides,the activation energies of the Sc-containing and Er-containing alloy are 84.8 k J/mol and 87.2 k J/mol,respectively.It is indicated that grain boundary sliding is the dominant mechanism during tensile deformation.According to microstructure examination,the better superplasticity of Sc-containing alloy may be attributed to the presence of Al3_(Sc,Zr)dispersoids,which can inhibit recrystallization and grain growth effectively.
文摘Based on current theories of diffusion and creep cavity closure at high temperature, a theoretical analysis of phase transformation diffusion bonding for T8/T8 eutectoid steel is carried out. The diffusion bonding is mainly described as two-stage process: Ⅰ The interfacial cavity with shape change from diamond to cylinder.Ⅱ The radius of the cylindrical cavity are reduced and eliminated gradually. A new theoretical model is established for the process of transformation superplastic diffusion bonding (TSDB) on the basis of a theoretical model for isothermal superplastic diffusion. The model can predict the bonding quality which is affected by technological parameters, such as limit cycling temperature, the compressive stress, the numbers of thermal cycles and temperature cycling through the phase transformation in the thermal cycling and so on. Results show that the maximum temperature, the compressive stress, the numbers of thermal cycles and the rate of temperature changing speed in the thermal cycling have an important influence on TSDB process. Meanwhile, reasonable technological parameters chosen from theoretical analysis is in good agreement with those obtained from experimental results.
基金Project(2006DFA53250) supported by the International Science and Technology Cooperation Program of ChinaProject(2005CB623706) supported by the National Basic Research Program of China
文摘True stress-true strain curve,microstructure and texture information were obtained to investigate the superplastic deformation behavior of 1420 Al-Li alloy sheets with initial elongated grains.From the true stress-true curve,the stress increases with the increase of strain to 0.15,then dramatically decreases with the increase of strain to 0.80,and finally keeps almost a horizontal line.Meanwhile,initial elongated grains are gradually changed into equiaxed grains and the initial strong Brass {0 1 1} <2 1 1> and S {1 2 3} <6 3 4> orientations are turned into nearly random orientation with increasing strain.All these results suggest that dislocation activity is the dominant mechanism during the first stage,then dynamic recrystallization occurs,and grain rotation is expected as an accommodation for grain boundary sliding(GBS).At larger strains,grain boundary migration(GBM) becomes necessary to accommodate GBS.
