This study investigates the corrosion-assisted fatigue crack growth rate(FCGR)of 16 mm thick AA 7075-T651 friction stir welded(FSW)joints.Compact tension(CT)specimens were extracted from both the base material and FSW...This study investigates the corrosion-assisted fatigue crack growth rate(FCGR)of 16 mm thick AA 7075-T651 friction stir welded(FSW)joints.Compact tension(CT)specimens were extracted from both the base material and FSW joints to evaluate FCGR under varying corrosion exposure durations(0,7,30,60,and 90 days)at a constant stress ratio of 0.5.Microstructural analysis of the welds was conducted using optical and transmission electron microscopy(TEM).Results indicate that the critical stress intensity factor range(ΔK_(cr))of FSW joints is lower than that of the base material,primarily due to precipitate dissolution in the weld zone during the FSW process,as confirmed by TEM analysis.The fatigue life of FSW joints was significantly lower than that of the base material,but with prolonged exposure to seawater corrosion,the gap in fatigue life narrowed.Specimens exposed to seawater for more than 60days exhibited minimal differences in fatigue life between the base material and the FSW joints.This was attributed to the higher corrosion rate of the base material compared to the weld nugget,resulting in the formation of deeper pits that facilitated crack initiation and accelerated fatigue failure.The findings conclude that extended corrosion exposure leads to similar fatigue life and crack growth behaviour in both the base material and FSW joints.SEM and EDX analysis of AA7075-T651 revealed corrosion pits and rust products in initiation zones,ductile striations in growth regions,and secondary cracks with micro voids in fracture zones.FSW joints exhibited ultra-fine grains,smooth ductile fracture in initiation and growth regions,and brittle fracture in the fracture zones under both corroded and uncorroded conditions.展开更多
This study examines the effects of friction stir welding(FSW)and post-weld heat treatment(PWHT)on the grain boundary character distribution and corrosion resistance of cross sectional(top and bottom)regions of nickel-...This study examines the effects of friction stir welding(FSW)and post-weld heat treatment(PWHT)on the grain boundary character distribution and corrosion resistance of cross sectional(top and bottom)regions of nickel-and molybdenum-free high-nitrogen austenitic stainless steel(HNASS).FSW at 400 rpm and 30 mm/min resulted in finer grains(4.18μm)and higher coincident site lattice(CSL)boundaries(32.3%)at the top of the stir zone(SZ)due to dynamic recrystallization(DRX).PWHT at 900℃for 1 h led to grain coarsening(12.91μm the bottom SZ)but enhanced CSL boundaries from 24.6%to 30.2%,improving grain boundary stability.PWHT reduced the kernel average misorientation(KAM)by 14.9%in the SZ-top layer and 20.4%in the SZ-bottom layer,accompanied by a 25%decrease in hardness in the SZ-top layer and 26.7%in the SZ-bottom layer,indicating strain recovery and reduced dislocation density.Potentiodynamic polarization tests(PDP)showed a 18%increase in pitting potential and a 76%reduction in corrosion rate after PWHT.The improvement in corrosion resistance is attributed to the increase inΣ3 twin boundaries,which enhance grain boundary stability and reduce susceptibility to localized corrosion.These findings highlight the role of PWHT in refining the microstructure and strengthening corrosion resistance,making HNASS a promising material for demanding applications.展开更多
A surface Ti-WC composite was fabricated on CP-Ti by surface friction stirring(SFS)using a pinless WC-Cotool at a processing window of 800−2500 r/min and 8−50 mm/min.At 1600 r/min-50 mm/min,a defect-free compositelaye...A surface Ti-WC composite was fabricated on CP-Ti by surface friction stirring(SFS)using a pinless WC-Cotool at a processing window of 800−2500 r/min and 8−50 mm/min.At 1600 r/min-50 mm/min,a defect-free compositelayer with an average hardness of~HV 1170 is formed.The hardness was increased by WC and TiN reinforcingparticles,dissolved Co atoms in Ti,and the formation of ultrafine grains.WC particles were incorporated into the Tisubstrate owing to the intense frictional interaction/heating at the tool-plate interface(~1000℃),which led to strengthloss and wear of the tool.The Williamson-Hall analysis of the XRD peaks of the SFSed sample confirmed a significantlysmall crystallite size(~100 nm).Wear tests showed that the wear resistance of the composite structure was about 4.5times higher than that of the CP-Ti.Friction analysis revealed a significant reduction in average value and fluctuations ofthe friction coefficient.展开更多
Friction stir welding(FSW) is a promising welding process that can join age hardenable aluminium alloys with high joint efficiency. However,the thermal cycles experienced by the material to be joined during FSW result...Friction stir welding(FSW) is a promising welding process that can join age hardenable aluminium alloys with high joint efficiency. However,the thermal cycles experienced by the material to be joined during FSW resulted in the deterioration of mechanical properties due to the coarsening and dissolution of strengthening precipitates in the thermo-mechanical affected zone(TMAZ) and heat affected zone(HAZ). Under water friction stir welding(UWFSW) is a variant of FSW process which can maintain low heat input as well as constant heat input along the weld line. The heat conduction and dissipation during UWFSW controls the width of TMAZ and HAZ and also improves the joint properties. In this investigation, an attempt has been made to evaluate the mechanical properties and microstructural characteristics of AA2519-T87 aluminium alloy joints made by FSW and UWFSW processes. Finite element analysis has been used to estimate the temperature distribution and width of TMAZ region in both the joints and the results have been compared with experimental results and subsequently correlated with mechanical properties.? 2016 China Ordnance Society. Production and hosting by Elsevier B.V. All rights reserved.展开更多
This paper studies the friction stir spot welding of AA2024-T3/AA7075-T6 Al alloys in the ambient and underwater environments by clarifying the nugget features,microstructure,fracture and mechanical properties of the ...This paper studies the friction stir spot welding of AA2024-T3/AA7075-T6 Al alloys in the ambient and underwater environments by clarifying the nugget features,microstructure,fracture and mechanical properties of the joints.The results show that the water-cooling medium exhibits a significant heat absorption capacity in the AA2024-T3/AA7075-T6 welded joint.Nugget features such as stir zone width,circular imprints,average grain sizes,and angular inter-material hooking are reduced by the watercooling effect in the joints.Narrower whitish(intercalated structures)bands are formed in the underwater joints while Mg2Si and Al2CuMg precipitates are formed in the ambient and the underwater welded joints respectively.An increase in tool rotational speed(600e1400 rpm)and plunge depth(0.1 e0.5 mm)increases the tensile-shear force of the welded AA2024-T3/AA7075-T6 joints in both the ambient and underwater environments.The maximum tensile-shear forces of 5900 N and 6700 N were obtained in the ambient and the underwater welds respectively.展开更多
Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter t...Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter the surface morphology of base metal. Preliminary studies reveal that the coating and layering of aluminium alloys with ceramic particles enhance the ballistic resistance. Furthermore, among aluminium alloys,7075 aluminium alloy exhibits high strength which can be compared to that of steels and has profound applications in the designing of lightweight fortification structures and integrated protection systems. Having limitations such as poor bond integrity, formation of detrimental phases and interfacial reaction between reinforcement and substrate using fusion route to deposit hard particles paves the way to adopt friction stir processing for fabricating surface composites using different sizes of boron carbide particles as reinforcement on armour grade 7075 aluminium alloy as matrix in the present investigation. Wear and ballistic tests were carried out to assess the performance of friction stir processed AA7075 alloy. Significant improvement in wear resistance of friction stir processed surface composites is attributed to the change in wear mechanism from abrasion to adhesion. It has also been observed that the surface metal matrix composites have shown better ballistic resistance compared to the substrate AA7075 alloy. Addition of solid lubricant Mo S2 has reduced the depth of penetration of the projectile to half that of base metal AA7075 alloy. For the first time, the friction stir processing technique was successfully used to improve the wear and ballistic resistances of armour grade high strength AA7075 alloy.展开更多
A systematic approach was presented to develop the empirical model for predicting the ultimate tensile strength of AA5083-H111 aluminum alloy which is widely used in ship building industry by incorporating friction st...A systematic approach was presented to develop the empirical model for predicting the ultimate tensile strength of AA5083-H111 aluminum alloy which is widely used in ship building industry by incorporating friction stir welding(FSW) process parameters such as tool rotational speed,welding speed,and axial force.FSW was carried out considering three-factor five-level central composite rotatable design with full replications technique.Response surface methodology(RSM) was applied to developing linear regression model for establishing the relationship between the FSW process parameters and ultimate tensile strength.Analysis of variance(ANOVA) technique was used to check the adequacy of the developed model.The FSW process parameters were also optimized using response surface methodology(RSM) to maximize the ultimate tensile strength.The joint welded at a tool rotational speed of 1 000 r/min,a welding speed of 69 mm/min and an axial force of 1.33 t exhibits higher tensile strength compared with other joints.展开更多
Bead-on-plate friction stir welds were made on P91 alloy with low and high rotational speeds(100 and 1000 RPM) to study their effects on weld microstructural changes and impression creep behavior. Temperatures experie...Bead-on-plate friction stir welds were made on P91 alloy with low and high rotational speeds(100 and 1000 RPM) to study their effects on weld microstructural changes and impression creep behavior. Temperatures experienced by the stir zone were recorded at the weld tool tip. Different zones of welds were characterized for their microstructural changes, hardness and creep behavior(by impression creep tests). The results were compared with submerged arc fusion weld. Studies revealed that the stir zone temperature with 100 RPM was well below A_(c1) temperature of P91 steel while it was above A_(c3) with 1000 RPM. The results suggest that the microstructural degradation in P91 welds can be controlled by low temperature friction stir welding technique.展开更多
The microstructure and mechanical properties of dissimilar pinless friction stir spot welded joint of2A12aluminum alloy and TC4titanium alloy were evaluated.The results show that the joint of Al/Ti dissimilar alloys c...The microstructure and mechanical properties of dissimilar pinless friction stir spot welded joint of2A12aluminum alloy and TC4titanium alloy were evaluated.The results show that the joint of Al/Ti dissimilar alloys can be successfully attained through pinless friction stir spot welding(FSSW).The joint can be divided into three zones(SZ,TMAZ and HAZ).The microstructure of joint in Al alloy side changes significantly but it basically has no change in Ti alloy side.At the same rotation speed,the maximum load of welded joints gradually rises with the increase in dwell time.At the same dwell time,the maximum load of the welded joint increases with the increase of the rotational speed.In addition,optimal parameters were obtained in this work,and they are rotation speed of1500r/min,plunge speed of30mm/min,plunge depth of0.3mm and dwell time of15s.The fracture mode of welded joints is interfacial shear fracture.The microhardness of the joint on the Al side distributes in a typical“W”type and is symmetry along the weld center,but the distribution of the microhardness on the Ti side has no obvious change.展开更多
文摘This study investigates the corrosion-assisted fatigue crack growth rate(FCGR)of 16 mm thick AA 7075-T651 friction stir welded(FSW)joints.Compact tension(CT)specimens were extracted from both the base material and FSW joints to evaluate FCGR under varying corrosion exposure durations(0,7,30,60,and 90 days)at a constant stress ratio of 0.5.Microstructural analysis of the welds was conducted using optical and transmission electron microscopy(TEM).Results indicate that the critical stress intensity factor range(ΔK_(cr))of FSW joints is lower than that of the base material,primarily due to precipitate dissolution in the weld zone during the FSW process,as confirmed by TEM analysis.The fatigue life of FSW joints was significantly lower than that of the base material,but with prolonged exposure to seawater corrosion,the gap in fatigue life narrowed.Specimens exposed to seawater for more than 60days exhibited minimal differences in fatigue life between the base material and the FSW joints.This was attributed to the higher corrosion rate of the base material compared to the weld nugget,resulting in the formation of deeper pits that facilitated crack initiation and accelerated fatigue failure.The findings conclude that extended corrosion exposure leads to similar fatigue life and crack growth behaviour in both the base material and FSW joints.SEM and EDX analysis of AA7075-T651 revealed corrosion pits and rust products in initiation zones,ductile striations in growth regions,and secondary cracks with micro voids in fracture zones.FSW joints exhibited ultra-fine grains,smooth ductile fracture in initiation and growth regions,and brittle fracture in the fracture zones under both corroded and uncorroded conditions.
文摘This study examines the effects of friction stir welding(FSW)and post-weld heat treatment(PWHT)on the grain boundary character distribution and corrosion resistance of cross sectional(top and bottom)regions of nickel-and molybdenum-free high-nitrogen austenitic stainless steel(HNASS).FSW at 400 rpm and 30 mm/min resulted in finer grains(4.18μm)and higher coincident site lattice(CSL)boundaries(32.3%)at the top of the stir zone(SZ)due to dynamic recrystallization(DRX).PWHT at 900℃for 1 h led to grain coarsening(12.91μm the bottom SZ)but enhanced CSL boundaries from 24.6%to 30.2%,improving grain boundary stability.PWHT reduced the kernel average misorientation(KAM)by 14.9%in the SZ-top layer and 20.4%in the SZ-bottom layer,accompanied by a 25%decrease in hardness in the SZ-top layer and 26.7%in the SZ-bottom layer,indicating strain recovery and reduced dislocation density.Potentiodynamic polarization tests(PDP)showed a 18%increase in pitting potential and a 76%reduction in corrosion rate after PWHT.The improvement in corrosion resistance is attributed to the increase inΣ3 twin boundaries,which enhance grain boundary stability and reduce susceptibility to localized corrosion.These findings highlight the role of PWHT in refining the microstructure and strengthening corrosion resistance,making HNASS a promising material for demanding applications.
文摘A surface Ti-WC composite was fabricated on CP-Ti by surface friction stirring(SFS)using a pinless WC-Cotool at a processing window of 800−2500 r/min and 8−50 mm/min.At 1600 r/min-50 mm/min,a defect-free compositelayer with an average hardness of~HV 1170 is formed.The hardness was increased by WC and TiN reinforcingparticles,dissolved Co atoms in Ti,and the formation of ultrafine grains.WC particles were incorporated into the Tisubstrate owing to the intense frictional interaction/heating at the tool-plate interface(~1000℃),which led to strengthloss and wear of the tool.The Williamson-Hall analysis of the XRD peaks of the SFSed sample confirmed a significantlysmall crystallite size(~100 nm).Wear tests showed that the wear resistance of the composite structure was about 4.5times higher than that of the CP-Ti.Friction analysis revealed a significant reduction in average value and fluctuations ofthe friction coefficient.
基金the financial support of the Directorate of Extramural Research & Intellectual Property Rights (ER&IPR)Defense Research Development Organization (DRDO)New Delhi through a R&D project no. DRDO-ERIPER/ERIP/ER/0903821/M/01/1404 to carry out this investigation
文摘Friction stir welding(FSW) is a promising welding process that can join age hardenable aluminium alloys with high joint efficiency. However,the thermal cycles experienced by the material to be joined during FSW resulted in the deterioration of mechanical properties due to the coarsening and dissolution of strengthening precipitates in the thermo-mechanical affected zone(TMAZ) and heat affected zone(HAZ). Under water friction stir welding(UWFSW) is a variant of FSW process which can maintain low heat input as well as constant heat input along the weld line. The heat conduction and dissipation during UWFSW controls the width of TMAZ and HAZ and also improves the joint properties. In this investigation, an attempt has been made to evaluate the mechanical properties and microstructural characteristics of AA2519-T87 aluminium alloy joints made by FSW and UWFSW processes. Finite element analysis has been used to estimate the temperature distribution and width of TMAZ region in both the joints and the results have been compared with experimental results and subsequently correlated with mechanical properties.? 2016 China Ordnance Society. Production and hosting by Elsevier B.V. All rights reserved.
基金Scientific Research Fund of Hunan Provincial Education Department(No.15C1240)Innovation platform open fund Project(No.16K080).
文摘This paper studies the friction stir spot welding of AA2024-T3/AA7075-T6 Al alloys in the ambient and underwater environments by clarifying the nugget features,microstructure,fracture and mechanical properties of the joints.The results show that the water-cooling medium exhibits a significant heat absorption capacity in the AA2024-T3/AA7075-T6 welded joint.Nugget features such as stir zone width,circular imprints,average grain sizes,and angular inter-material hooking are reduced by the watercooling effect in the joints.Narrower whitish(intercalated structures)bands are formed in the underwater joints while Mg2Si and Al2CuMg precipitates are formed in the ambient and the underwater welded joints respectively.An increase in tool rotational speed(600e1400 rpm)and plunge depth(0.1 e0.5 mm)increases the tensile-shear force of the welded AA2024-T3/AA7075-T6 joints in both the ambient and underwater environments.The maximum tensile-shear forces of 5900 N and 6700 N were obtained in the ambient and the underwater welds respectively.
基金Financial assistance from Armament Research Board, New Delhi, India
文摘Industrial applications of aluminium and its alloys are restricted because of their poor tribological properties. Thermal spraying, laser surfacing, electron beam welding are the most widely used techniques to alter the surface morphology of base metal. Preliminary studies reveal that the coating and layering of aluminium alloys with ceramic particles enhance the ballistic resistance. Furthermore, among aluminium alloys,7075 aluminium alloy exhibits high strength which can be compared to that of steels and has profound applications in the designing of lightweight fortification structures and integrated protection systems. Having limitations such as poor bond integrity, formation of detrimental phases and interfacial reaction between reinforcement and substrate using fusion route to deposit hard particles paves the way to adopt friction stir processing for fabricating surface composites using different sizes of boron carbide particles as reinforcement on armour grade 7075 aluminium alloy as matrix in the present investigation. Wear and ballistic tests were carried out to assess the performance of friction stir processed AA7075 alloy. Significant improvement in wear resistance of friction stir processed surface composites is attributed to the change in wear mechanism from abrasion to adhesion. It has also been observed that the surface metal matrix composites have shown better ballistic resistance compared to the substrate AA7075 alloy. Addition of solid lubricant Mo S2 has reduced the depth of penetration of the projectile to half that of base metal AA7075 alloy. For the first time, the friction stir processing technique was successfully used to improve the wear and ballistic resistances of armour grade high strength AA7075 alloy.
文摘A systematic approach was presented to develop the empirical model for predicting the ultimate tensile strength of AA5083-H111 aluminum alloy which is widely used in ship building industry by incorporating friction stir welding(FSW) process parameters such as tool rotational speed,welding speed,and axial force.FSW was carried out considering three-factor five-level central composite rotatable design with full replications technique.Response surface methodology(RSM) was applied to developing linear regression model for establishing the relationship between the FSW process parameters and ultimate tensile strength.Analysis of variance(ANOVA) technique was used to check the adequacy of the developed model.The FSW process parameters were also optimized using response surface methodology(RSM) to maximize the ultimate tensile strength.The joint welded at a tool rotational speed of 1 000 r/min,a welding speed of 69 mm/min and an axial force of 1.33 t exhibits higher tensile strength compared with other joints.
文摘Bead-on-plate friction stir welds were made on P91 alloy with low and high rotational speeds(100 and 1000 RPM) to study their effects on weld microstructural changes and impression creep behavior. Temperatures experienced by the stir zone were recorded at the weld tool tip. Different zones of welds were characterized for their microstructural changes, hardness and creep behavior(by impression creep tests). The results were compared with submerged arc fusion weld. Studies revealed that the stir zone temperature with 100 RPM was well below A_(c1) temperature of P91 steel while it was above A_(c3) with 1000 RPM. The results suggest that the microstructural degradation in P91 welds can be controlled by low temperature friction stir welding technique.
基金Projects(51405389,51675435)supported by the National Natural Science Foundation of ChinaProject(3102017ZY005)supported by the Fundamental Research Funds for the Central Universities,China+3 种基金Project(SAST2016043)supported by the Fund of SAST,ChinaProject(20161125002)supported by the Aeronautical Science Foundation of ChinaProject(B08040)supported by the 111 Project,ChinaProjects(2016YFB0701203,2016YFB1100104)supported by the National Key Research and Development Program of China
文摘The microstructure and mechanical properties of dissimilar pinless friction stir spot welded joint of2A12aluminum alloy and TC4titanium alloy were evaluated.The results show that the joint of Al/Ti dissimilar alloys can be successfully attained through pinless friction stir spot welding(FSSW).The joint can be divided into three zones(SZ,TMAZ and HAZ).The microstructure of joint in Al alloy side changes significantly but it basically has no change in Ti alloy side.At the same rotation speed,the maximum load of welded joints gradually rises with the increase in dwell time.At the same dwell time,the maximum load of the welded joint increases with the increase of the rotational speed.In addition,optimal parameters were obtained in this work,and they are rotation speed of1500r/min,plunge speed of30mm/min,plunge depth of0.3mm and dwell time of15s.The fracture mode of welded joints is interfacial shear fracture.The microhardness of the joint on the Al side distributes in a typical“W”type and is symmetry along the weld center,but the distribution of the microhardness on the Ti side has no obvious change.
