Solanesyl bromide(Ⅱ) was reacted with diethanolamine to give solanesyl diethanolamine(Ⅲ) which was acylated with 3,4,5 trimethoxybenzoyl chloride, acetic anhydride, benzoyl chloride and cinnamyl chloride to give N,N...Solanesyl bromide(Ⅱ) was reacted with diethanolamine to give solanesyl diethanolamine(Ⅲ) which was acylated with 3,4,5 trimethoxybenzoyl chloride, acetic anhydride, benzoyl chloride and cinnamyl chloride to give N,N di[(3,4,5 trimethoxybenzoyloxy)ethyl]solanesylamine(Ⅳ), N,N di[(acetyloxy)ethyl] solanesylamine(Ⅴ), N,N di[(benzoyloxy)ethyl]solanesylamine(Ⅵ), N,N di[(cinnyloxy)ethyl]solanesylamine(Ⅶ) respectively. The structures of compounds Ⅲ～Ⅶ were confirmed by IR, 1H NMR, MS and elemental analysis.展开更多
文摘Solanesyl bromide(Ⅱ) was reacted with diethanolamine to give solanesyl diethanolamine(Ⅲ) which was acylated with 3,4,5 trimethoxybenzoyl chloride, acetic anhydride, benzoyl chloride and cinnamyl chloride to give N,N di[(3,4,5 trimethoxybenzoyloxy)ethyl]solanesylamine(Ⅳ), N,N di[(acetyloxy)ethyl] solanesylamine(Ⅴ), N,N di[(benzoyloxy)ethyl]solanesylamine(Ⅵ), N,N di[(cinnyloxy)ethyl]solanesylamine(Ⅶ) respectively. The structures of compounds Ⅲ～Ⅶ were confirmed by IR, 1H NMR, MS and elemental analysis.
