Thermal diffusion of Si atoms at the interface in Mo/Si multilayers was observed with an imaging type soft X ray emission microscope developed by us. It was possible to observe the diffusion with 0.2nm depth resolutio...Thermal diffusion of Si atoms at the interface in Mo/Si multilayers was observed with an imaging type soft X ray emission microscope developed by us. It was possible to observe the diffusion with 0.2nm depth resolution in the direction normal to the interface by comparing the emission intensity for exactly the same position. The diffusion coefficient of Si atoms in Mo at 600℃ was roughly estimated to be 6.0×10 17 cm 2/s.展开更多
The principle of laser optical feedback microscope was presented and demonstrated. Three methods to advance the vertical resolution of laser optical feedback microscope were experimentally studied. The first one is to...The principle of laser optical feedback microscope was presented and demonstrated. Three methods to advance the vertical resolution of laser optical feedback microscope were experimentally studied. The first one is to detect the two polarized lights’ intensities separately with a Wollaston prism instead of to detect the whole light’s intensity. The second is that both of the two orthogonally polarized lights of a birefringent dual frequency laser are fed back. The third one is that only one of the orthogonally polarized lights is fed back. The experimental results show that the modes competition between orthogonally polarized lights can be used to improve the vertical resolution of laser optical feedback microscope effectively.展开更多
The design and fabrication processes of a novel scanner with minimized coupling motions for a high-speed atomic force microscope （AFM） were addressed. An appropriate design modification was proposed through the anal...The design and fabrication processes of a novel scanner with minimized coupling motions for a high-speed atomic force microscope （AFM） were addressed. An appropriate design modification was proposed through the analyses of the dynamic characteristics of existing linear motion stages using a dynamic analysis program, Recurdyn. Because the scanning speed of each direction may differ, the linear motion stage for a high-speed scanner was designed to have different resonance frequencies for the modes, with one dominant displacement in the desired directions. This objective was achieved by using one-direction flexure mechanisms for each direction and mounting one stage for fast motion on the other stage for slow motion. This unsymmetrical configuration separated the frequencies of two vibration modes with one dominant displacement in each desired direction, and hence suppressed the coupling between motions in two directions. A pair of actuators was used for each axis to decrease the crosstalk between the two motions and give a sufficient force to actuate the slow motion stage, which carried the fast motion stage, A lossy material, such as grease, was inserted into the flexure hinge to suppress vibration problems that occurred when using an input triangular waveforrn. With these design modifications and the vibration suppression method, a novel scanner with a scanning speed greater than 20 Hz is achieved.展开更多
A fiber-optic confocal microscope has been analyzed by Fourier optics.It is found that the detected light intensity has three parts,each of which is depennted on the coupled lens,the detective lens,and the part compri...A fiber-optic confocal microscope has been analyzed by Fourier optics.It is found that the detected light intensity has three parts,each of which is depennted on the coupled lens,the detective lens,and the part comprised of the fiber and the microprobe.The simulated results show that the less the value of the parameter A is,which is dependent on the fiber and microprobe,the higher the axial resolution of the system is. For the case,as A→∞, the axial resolution is zero,which is corresponding to the conventional microscope.as A≤1,the axial resolution changes slightly,and is close to the optimal value,which is corresponding to the perfect confocal microscope.when the reflective loss takes place at the end of fiber,the contrast of axial intensity will decrease.All that will help the design of endoscope with confocal microscope at cellular level.展开更多
It is well known that β-BBO is a new type nonlinear optical crystal discovered in our institute and now β-BBO is widely used in the fields of laser and nonlinear optics. However, there are still some inclusions in ...It is well known that β-BBO is a new type nonlinear optical crystal discovered in our institute and now β-BBO is widely used in the fields of laser and nonlinear optics. However, there are still some inclusions in β-BBO crystal grown by flux method. Using AEM technique, we have studied the shape, composition and structure of inclusions which is very helpful to the explanation of the formation of inclusions.展开更多
调制传递函数(modulation transfer function,MTF)曲线可以客观地评价光学系统的成像性能。基于平面对称光学系统的波像差理论,给出了Kirkpatrick-Baez(KB)显微镜光学系统主要像差的波像差计算表达式,采用自相关法,通过Gauss-Legendre...调制传递函数(modulation transfer function,MTF)曲线可以客观地评价光学系统的成像性能。基于平面对称光学系统的波像差理论,给出了Kirkpatrick-Baez(KB)显微镜光学系统主要像差的波像差计算表达式,采用自相关法,通过Gauss-Legendre数值积分求解并绘制了KB系统的MTF曲线,且与光学分析软件的MTF曲线进行对比。结果表明:应用波像差理论计算调制传递函数不仅可以定量直观地分析KB系统的成像性能,而且能进一步解析光学系统的单项像差分布情况,提供更具针对性的系统优化方案。展开更多
The hydration film on particle surface plays an important role in bubble-particle adhesion in mineral flotation process. The thicknesses of the hydration films on natural hydrophobic coal and hydrophilic mica surfaces...The hydration film on particle surface plays an important role in bubble-particle adhesion in mineral flotation process. The thicknesses of the hydration films on natural hydrophobic coal and hydrophilic mica surfaces were measured directly by atomic force microscopy (AFM) based on the bending mode of the nominal constant compliance regime in AFM force curve in the present study. Surface and solid-liquid interfacial energies were calculated to explain the forming mechanism of the hydration film and atomic force microscopy data. The results show that there are significant differences in the structure and thickness of hydration films on coal and mica surfaces. Hydration film formed on mica surface with the thickness of 22.5 nm. In contrast, the bend was not detected in the nominal constant compliance regime. The van der Waals and polar interactions between both mica and coal and water molecules are characterized by an attractive effect, while the polar attractive free energy between water and mica (-87.36 mN/m) is significantly larger than that between water and coal (-32.89 mN/m), which leads to a thicker and firmer hydration layer on the mica surface. The interfacial interaction free energy of the coal/water/bubble is greater than that of mica. The polar attractive force is large enough to overcome the repulsive van der Waals force and the low energy barrier of film rupture, achieving coal particle bubble adhesion with a total interfacial free energy of-56.30 mN/m.展开更多
With the microscopic phase-field dynamic model, the effects of temperature and concentration on the nucleation incubation time of Ni75AlxV25-x alloy were studied and the relation between the incubation time and precip...With the microscopic phase-field dynamic model, the effects of temperature and concentration on the nucleation incubation time of Ni75AlxV25-x alloy were studied and the relation between the incubation time and precipitation mechanism was investigated by using the atomic occupation probability picture and average order parameter curve. The simulation results demonstrate that there exists the incubation time for different precipitation mechanisms~ such as non-classical nucleation, the mixed style of non-classical nucleation and spinodal decomposition, and spinodal ordering; and the incubation time shortens in turn for the three kinds of mechanisms. With the increase of Al content of Ni75AlxV25-x alloy, the incubation time of Llz phases shortens continuously and that of DOzz phases is prolonged. The effects of temperature on the incubation time of Llz and DOzz phases are accordant, i.e. the incuba- tion time is greatly prolonged with the temperature rising.展开更多
A series of researches were carried out for the soil samples in the Pearl River Delta under the action of consolidation loads,such as the quantitative analyses of the pore scale,shape and size distributions of micro-s...A series of researches were carried out for the soil samples in the Pearl River Delta under the action of consolidation loads,such as the quantitative analyses of the pore scale,shape and size distributions of micro-structure units,with an environmental scanning electron microscope (ESEM),a mercury intrusion analyzer and a mineral diffractometer. The experimental results show that the consolidation pressures remarkably change the pore sizes and distribution characteristics of the silt,thus changing its compressibility and permeability. This can be proved by the fact that,in the earlier stage with a consolidation pressure of p<200 kPa,the pore sizes are greater and the compressibility and permeability coefficients are larger. However,they rapidly decrease with the increase in consolidation pressure. And in the later stage with a consolidation pressure of p>200 kPa,the pore sizes are smaller and the compressibility and permeability coefficients are less. Therefore,the empirical formulas of compression coefficient and permeability coefficient vs consolidation load and average pore diameter are deduced.展开更多
It is important to calibrate micro-parameters for applying partied flow code(PFC)to study mechanical characteristics and failure mechanism of rock materials.Uniform design method is firstly adopted to determine the mi...It is important to calibrate micro-parameters for applying partied flow code(PFC)to study mechanical characteristics and failure mechanism of rock materials.Uniform design method is firstly adopted to determine the microscopic parameters of parallel-bonded particle model for three-dimensional discrete element particle flow code(PFC3D).Variation ranges of microscopic of the microscopic parameters are created by analyzing the effects of microscopic parameters on macroscopic parameters(elastic modulus E,Poisson ratio v,uniaxial compressive strengthσc,and ratio of crack initial stress to uniaxial compressive strengthσci/σc)in order to obtain the actual uniform design talbe.The calculation equations of the microscopic and macroscopic parameters of rock materials can be established by the actual uniform design table and the regression analysis and thus the PFC3D microscopic parameters can be quantitatively determined.The PFC3D simulated results of the intact and pre-cracked rock specimens under uniaxial and triaxial compressions(including the macroscopic mechanical parameters,stress−strain curves and failure process)are in good agreement with experimental results,which can prove the validity of the calculation equations of microscopic and macroscopic parameters.展开更多
The simulations of Cr atom substitution character during the formation of L12 and DO22 phases in Ni-Cr-Al alloy were performed at 873 K based on microscopic phase-field model. It is found that the substitution of Cr i...The simulations of Cr atom substitution character during the formation of L12 and DO22 phases in Ni-Cr-Al alloy were performed at 873 K based on microscopic phase-field model. It is found that the substitution of Cr is affected by Cr and Al contents and limits of occupation probabilities of Cr atom in L12 phase are present. The precipitate is single L12 phase when the component is less than the limit, Cr atoms substitute the Al sublattices in Ll2 phase, and both of atoms Al and Cr occupy the β-sites and complex phases Ni3（Al1-xCrx） are formed; Cr atoms enter Ni sites when Al and Cr contents exceed the limit, and substitute β-sites or both of α- and β-sites. The DO22 phase is formed at the boundary of Ll2 phase.展开更多
文摘Thermal diffusion of Si atoms at the interface in Mo/Si multilayers was observed with an imaging type soft X ray emission microscope developed by us. It was possible to observe the diffusion with 0.2nm depth resolution in the direction normal to the interface by comparing the emission intensity for exactly the same position. The diffusion coefficient of Si atoms in Mo at 600℃ was roughly estimated to be 6.0×10 17 cm 2/s.
文摘The principle of laser optical feedback microscope was presented and demonstrated. Three methods to advance the vertical resolution of laser optical feedback microscope were experimentally studied. The first one is to detect the two polarized lights’ intensities separately with a Wollaston prism instead of to detect the whole light’s intensity. The second is that both of the two orthogonally polarized lights of a birefringent dual frequency laser are fed back. The third one is that only one of the orthogonally polarized lights is fed back. The experimental results show that the modes competition between orthogonally polarized lights can be used to improve the vertical resolution of laser optical feedback microscope effectively.
基金Work(R0A-2007-000-20042-0) partly supported by the Second Stage of Brain Korea 21 Projectspartly by the Korea Science and Engineering Foundation (KOSEF) through the National Research Laboratory Program funded by the Ministry of Science and Technology of Korea
文摘The design and fabrication processes of a novel scanner with minimized coupling motions for a high-speed atomic force microscope （AFM） were addressed. An appropriate design modification was proposed through the analyses of the dynamic characteristics of existing linear motion stages using a dynamic analysis program, Recurdyn. Because the scanning speed of each direction may differ, the linear motion stage for a high-speed scanner was designed to have different resonance frequencies for the modes, with one dominant displacement in the desired directions. This objective was achieved by using one-direction flexure mechanisms for each direction and mounting one stage for fast motion on the other stage for slow motion. This unsymmetrical configuration separated the frequencies of two vibration modes with one dominant displacement in each desired direction, and hence suppressed the coupling between motions in two directions. A pair of actuators was used for each axis to decrease the crosstalk between the two motions and give a sufficient force to actuate the slow motion stage, which carried the fast motion stage, A lossy material, such as grease, was inserted into the flexure hinge to suppress vibration problems that occurred when using an input triangular waveforrn. With these design modifications and the vibration suppression method, a novel scanner with a scanning speed greater than 20 Hz is achieved.
文摘A fiber-optic confocal microscope has been analyzed by Fourier optics.It is found that the detected light intensity has three parts,each of which is depennted on the coupled lens,the detective lens,and the part comprised of the fiber and the microprobe.The simulated results show that the less the value of the parameter A is,which is dependent on the fiber and microprobe,the higher the axial resolution of the system is. For the case,as A→∞, the axial resolution is zero,which is corresponding to the conventional microscope.as A≤1,the axial resolution changes slightly,and is close to the optimal value,which is corresponding to the perfect confocal microscope.when the reflective loss takes place at the end of fiber,the contrast of axial intensity will decrease.All that will help the design of endoscope with confocal microscope at cellular level.
文摘It is well known that β-BBO is a new type nonlinear optical crystal discovered in our institute and now β-BBO is widely used in the fields of laser and nonlinear optics. However, there are still some inclusions in β-BBO crystal grown by flux method. Using AEM technique, we have studied the shape, composition and structure of inclusions which is very helpful to the explanation of the formation of inclusions.
文摘调制传递函数(modulation transfer function,MTF)曲线可以客观地评价光学系统的成像性能。基于平面对称光学系统的波像差理论,给出了Kirkpatrick-Baez(KB)显微镜光学系统主要像差的波像差计算表达式,采用自相关法,通过Gauss-Legendre数值积分求解并绘制了KB系统的MTF曲线,且与光学分析软件的MTF曲线进行对比。结果表明:应用波像差理论计算调制传递函数不仅可以定量直观地分析KB系统的成像性能,而且能进一步解析光学系统的单项像差分布情况,提供更具针对性的系统优化方案。
基金Project(2014BAB01B03)supported by the National Key Technology R&D Program During the 12th Five-Yean Plan of ChinaProject(51774286)supported by the National Natural Science Foundation of ChinaProject(BK20150192)supported by the Natural Science Foundation of Jiaaagsu Province,China
文摘The hydration film on particle surface plays an important role in bubble-particle adhesion in mineral flotation process. The thicknesses of the hydration films on natural hydrophobic coal and hydrophilic mica surfaces were measured directly by atomic force microscopy (AFM) based on the bending mode of the nominal constant compliance regime in AFM force curve in the present study. Surface and solid-liquid interfacial energies were calculated to explain the forming mechanism of the hydration film and atomic force microscopy data. The results show that there are significant differences in the structure and thickness of hydration films on coal and mica surfaces. Hydration film formed on mica surface with the thickness of 22.5 nm. In contrast, the bend was not detected in the nominal constant compliance regime. The van der Waals and polar interactions between both mica and coal and water molecules are characterized by an attractive effect, while the polar attractive free energy between water and mica (-87.36 mN/m) is significantly larger than that between water and coal (-32.89 mN/m), which leads to a thicker and firmer hydration layer on the mica surface. The interfacial interaction free energy of the coal/water/bubble is greater than that of mica. The polar attractive force is large enough to overcome the repulsive van der Waals force and the low energy barrier of film rupture, achieving coal particle bubble adhesion with a total interfacial free energy of-56.30 mN/m.
文摘With the microscopic phase-field dynamic model, the effects of temperature and concentration on the nucleation incubation time of Ni75AlxV25-x alloy were studied and the relation between the incubation time and precipitation mechanism was investigated by using the atomic occupation probability picture and average order parameter curve. The simulation results demonstrate that there exists the incubation time for different precipitation mechanisms~ such as non-classical nucleation, the mixed style of non-classical nucleation and spinodal decomposition, and spinodal ordering; and the incubation time shortens in turn for the three kinds of mechanisms. With the increase of Al content of Ni75AlxV25-x alloy, the incubation time of Llz phases shortens continuously and that of DOzz phases is prolonged. The effects of temperature on the incubation time of Llz and DOzz phases are accordant, i.e. the incuba- tion time is greatly prolonged with the temperature rising.
基金Project(2008ZA11) supported by State Key Laboratory of Subtropical Building Science in South China University of Technology, ChinaProject(20080430815) supported by China Postdoctoral Science Foundation
文摘A series of researches were carried out for the soil samples in the Pearl River Delta under the action of consolidation loads,such as the quantitative analyses of the pore scale,shape and size distributions of micro-structure units,with an environmental scanning electron microscope (ESEM),a mercury intrusion analyzer and a mineral diffractometer. The experimental results show that the consolidation pressures remarkably change the pore sizes and distribution characteristics of the silt,thus changing its compressibility and permeability. This can be proved by the fact that,in the earlier stage with a consolidation pressure of p<200 kPa,the pore sizes are greater and the compressibility and permeability coefficients are larger. However,they rapidly decrease with the increase in consolidation pressure. And in the later stage with a consolidation pressure of p>200 kPa,the pore sizes are smaller and the compressibility and permeability coefficients are less. Therefore,the empirical formulas of compression coefficient and permeability coefficient vs consolidation load and average pore diameter are deduced.
基金Projects(51474251,51874351)supported by the National Natural Science Foundation,China。
文摘It is important to calibrate micro-parameters for applying partied flow code(PFC)to study mechanical characteristics and failure mechanism of rock materials.Uniform design method is firstly adopted to determine the microscopic parameters of parallel-bonded particle model for three-dimensional discrete element particle flow code(PFC3D).Variation ranges of microscopic of the microscopic parameters are created by analyzing the effects of microscopic parameters on macroscopic parameters(elastic modulus E,Poisson ratio v,uniaxial compressive strengthσc,and ratio of crack initial stress to uniaxial compressive strengthσci/σc)in order to obtain the actual uniform design talbe.The calculation equations of the microscopic and macroscopic parameters of rock materials can be established by the actual uniform design table and the regression analysis and thus the PFC3D microscopic parameters can be quantitatively determined.The PFC3D simulated results of the intact and pre-cracked rock specimens under uniaxial and triaxial compressions(including the macroscopic mechanical parameters,stress−strain curves and failure process)are in good agreement with experimental results,which can prove the validity of the calculation equations of microscopic and macroscopic parameters.
基金Project(50071046) supported by the National Natural Science Foundation of China
文摘The simulations of Cr atom substitution character during the formation of L12 and DO22 phases in Ni-Cr-Al alloy were performed at 873 K based on microscopic phase-field model. It is found that the substitution of Cr is affected by Cr and Al contents and limits of occupation probabilities of Cr atom in L12 phase are present. The precipitate is single L12 phase when the component is less than the limit, Cr atoms substitute the Al sublattices in Ll2 phase, and both of atoms Al and Cr occupy the β-sites and complex phases Ni3（Al1-xCrx） are formed; Cr atoms enter Ni sites when Al and Cr contents exceed the limit, and substitute β-sites or both of α- and β-sites. The DO22 phase is formed at the boundary of Ll2 phase.
