An algorithm for precisely calculating the inductance of a three-section solenoid is presented, which is based on summing the layer self-inductances and the mutual inductances. A theoretical model with ex plicit expre...An algorithm for precisely calculating the inductance of a three-section solenoid is presented, which is based on summing the layer self-inductances and the mutual inductances. A theoretical model with ex plicit expressions is firstly developed to calculate the self-inductance of a single layer, and then numerical calcu lation of the mutual inductance between two layers is introduced. Using the presented computation method, the inductance of a solenoid designed in the experiment is successfully calculated （4.30 mH）, which has a difference of less than 1% from the experimental data.展开更多
Magnetorheological(MR)materials are a class of smart material,whose the mechanical/rheological state can be controlled under a magnetic field.Magnetorheological materials are typically fluids,gels,or elastomers.In thi...Magnetorheological(MR)materials are a class of smart material,whose the mechanical/rheological state can be controlled under a magnetic field.Magnetorheological materials are typically fluids,gels,or elastomers.In this study,anisotropic and isotropic magneto-rheological elastomer(MRE)samples were fabricated using a silicone rubber matrix with carbonyl iron particles as filler particles.The magnetic field-dependent inductance properties of these samples were studied using inductors specially designed for the analysis.The effect of the filler particle content,fabrication conditions,and inductance properties were characterized using a self-built system in both constant and transient magnetic fields.These factors show a significant effect on the inductance properties of the MRE inductor under an applied magnetic field.The anisotropic MRE inductor was more sensitive than the inductor based on an isotropic MRE.Owing to the presence of a constant magnetic field,the inductance value of the MRE inductor decreased with an increase in the external magnetic field.An attempt in elucidation of the mechanism is reported here.This study may enable the MRE to be widely used in practical applications such as monitoring magnetic field or detecting the filler particle content inside MR materials.展开更多
A transformation of naphthalene-based coalescenced mesophase pitch(NMP)to mesophase microbeads was achieved by heating a mixture of NMP and fullerene(C_(60)).This is different from the conventional process of the liqu...A transformation of naphthalene-based coalescenced mesophase pitch(NMP)to mesophase microbeads was achieved by heating a mixture of NMP and fullerene(C_(60)).This is different from the conventional process of the liquid-phase carbonization of isotropic pitch to the emergence of carbon microbeads in the matrix and finally their growth to form a 100%anisotropic bulk meso-phase,but rather a reverse transformation.The effects of C_(60) loading and reaction temperature on the morphological transformation of mesophase were investigated by polarizing optical and scanning electron microscopies.The physical changes in the NMP induced by C_(60) were characterized by thermogravimetric analysis,Fourier transform infrared spectroscopy,X-ray diffractometry and Raman spectroscopy.The results show that the coalesced NMP can be converted to a spherical type at 300-320℃ with the addition of 5%C_(60),and the size of the mesophase microbeads increases with increasing temperature.Furthermore,a model is established to ex-plain the unique induction effect of C_(60) in the transformation process.This work makes the morphological transformation of MP con-trollable,and provides a new idea for the understanding and research of mesophase pitch.展开更多
Using ultra-fine sample for determination 42 elements by pressurized acid digestion -ICP-MS, the mass of test portion can be reduced to 2 mg yet maintain the representation. And acid used for digestion could be reduce...Using ultra-fine sample for determination 42 elements by pressurized acid digestion -ICP-MS, the mass of test portion can be reduced to 2 mg yet maintain the representation. And acid used for digestion could be reduced to less than 0.5 mL, reaction time also largely reduced.展开更多
Inductively coupled plasma mass spectrometry (ICP-MS) was used to detect trace metal impurities in reagents such as H2O2, HNO3and H2SO4. The limit of detection to metal elements can be down to 2-20 ng/L in H2O2 and HN...Inductively coupled plasma mass spectrometry (ICP-MS) was used to detect trace metal impurities in reagents such as H2O2, HNO3and H2SO4. The limit of detection to metal elements can be down to 2-20 ng/L in H2O2 and HNO3 and 0.1-1.0 ng/L in H2SO4.展开更多
Inductively coupled plasma mass spectrometry (ICP-MS) was applied to determine copper, arsenic, cadmium, lead in athletic food using Sc, Ge, In, Bi as an internal standard. The linear correlation factor for four eleme...Inductively coupled plasma mass spectrometry (ICP-MS) was applied to determine copper, arsenic, cadmium, lead in athletic food using Sc, Ge, In, Bi as an internal standard. The linear correlation factor for four elements are higher than 0.999. Recoveries of spiked samples are in the range of 85.5%-115.5% and precision was fine, RSD is lower than 5.0%. And these are close agreement with the reference values in three standard reference materials of GBW08503, NBS1568, GBW08571. It indicates that the method is simple, rapid, sensitive and accurate, which can meet the demand for copper, arsenic, cadmium, lead analysis in athletic food.展开更多
The isotopic analysis of 232Pu plutonium in 5×10-12 g/g samples using a multi-collector inductively coupled plasma mass spectrometry (MC-ICPMS) is described. IRMM-290b and uranium (UTB750) were used to correct th...The isotopic analysis of 232Pu plutonium in 5×10-12 g/g samples using a multi-collector inductively coupled plasma mass spectrometry (MC-ICPMS) is described. IRMM-290b and uranium (UTB750) were used to correct the metrical data, and the analytical precision is about 0.5%.展开更多
Six massive ores in the Jinchuan deposit were dated by Re-Os technique. The Os concentrations and isotopic ratios were determined by N-TIMS, while Re and Pt concentrations were determined by ICP-MS. The samples gave a...Six massive ores in the Jinchuan deposit were dated by Re-Os technique. The Os concentrations and isotopic ratios were determined by N-TIMS, while Re and Pt concentrations were determined by ICP-MS. The samples gave an isochron age of (852±25) Ma with an initial 187Os/188Os ratio of 0.255 ± 0.014. A 7-point Pt-Os isochrone gives an age of (870±38) Ma with an initial 186Os/188Os ratio of 0.119 84±0.000 27.展开更多
To improve precision of analytical results of pressurized acid digestion-ICP-MS, the first step is to improve the homogeneity by reducing the particle size of sample. Using of ultra-fine sample (-500 mesh) can reduce ...To improve precision of analytical results of pressurized acid digestion-ICP-MS, the first step is to improve the homogeneity by reducing the particle size of sample. Using of ultra-fine sample (-500 mesh) can reduce the mass of the sample and the acid. The satisfactory precision is achieved at 2 mg sampling mass.展开更多
The application of inductively coupled plasma mass spectrometry (ICP-MS) for determination of boron in water and urine samples was described. The detect limit (3σ) was 0.057 μg/L. The precision of the method was les...The application of inductively coupled plasma mass spectrometry (ICP-MS) for determination of boron in water and urine samples was described. The detect limit (3σ) was 0.057 μg/L. The precision of the method was less than 2%. Multi-elements including Cr, Cu, Cd, Ba, Sr, Mn, Co, Tl, Li, Pb, Ca, Fe, K, Na, Mg, P, Si and Zn could be measured simultaneously. The method was successfully used in practice.展开更多
A method of analysis trace element chloride in cleaning products by Inductively Coupled Plasma-Mass Sepctrometry (ICPMS) was studied. It has good precision (RSD<5%). The LOD is 0.06 μg/L (n=7). The recovery is 93....A method of analysis trace element chloride in cleaning products by Inductively Coupled Plasma-Mass Sepctrometry (ICPMS) was studied. It has good precision (RSD<5%). The LOD is 0.06 μg/L (n=7). The recovery is 93.7%-110.0%.展开更多
基于逆磁致伸缩效应,建立钢缆索索力传感器理论模型,分析了施加在缆索材料上的力信号(外力和应变)与磁信号(磁感应强度、磁场强度)之间的耦合关系.针对一种环式结构的索力传感器,对索力测量原理做了详细推导,可通过检测感应线圈的感应...基于逆磁致伸缩效应,建立钢缆索索力传感器理论模型,分析了施加在缆索材料上的力信号(外力和应变)与磁信号(磁感应强度、磁场强度)之间的耦合关系.针对一种环式结构的索力传感器,对索力测量原理做了详细推导,可通过检测感应线圈的感应电压反映材料所受外力.传感器输出感应电压与空气间隙尺寸、外部激励磁场下的材料磁导率、激励磁场变化、加载外力变化等因素有关,重点分析了激励磁场变化和外力变化对传感器输出的影响.当外力是缓变力,可通过检测感应积分电压求得外力;当外力是交变力,直接通过感应电压求得外力;最后通过对磁场变化和外力变化影响分别进行了仿真,结果与理论分析基本一致,表明所建立的索力传感器理论模型可行.
Abstract：
Based on Villari-effect, the theoretic mdel d the cable tension sensor is presented. The relationship between mechanical parameters such as stress, strain and electromagnetic parameters like magnetic field and magnetic induction field are discussed. One loop-shaped stinulative structure of cable tension sensor based on Villari--effect is proposed and cable tension sensor principle is deeply analysed. By measuring inductive voltage in inductive loops, cable tension stress may be measured. Sensor output may be determined by air clearance, magnetic permeability, magnetic field, stress and inductive loops denseness. The sensor output effects resulting from magnetic field and stress ate analysed respectively. When stress changes tardigradely, the cable tension stress may be measured by measuring inductive integral voltage. When stress changes expeditiously, the cable tension stress may be measured by measuring inductive voltage. Sensor sensibility may be determined by stress frequency, inductive loops denseness, magnetic field and nagnetic permeability. In addition, the sensor output effects from magnetic changing and stress changing have been analysed with emulational methods. The results indicate that sensor theory model is feasible.展开更多
In this paper,the determination of six heavy metal ions (arsenic,lead,cadmium,chromium,mercury and nickel) in the Chinese Herb by inductively coupled plasma-mass spectrometry (ICP-MS) was studied.The samples were dige...In this paper,the determination of six heavy metal ions (arsenic,lead,cadmium,chromium,mercury and nickel) in the Chinese Herb by inductively coupled plasma-mass spectrometry (ICP-MS) was studied.The samples were digested by nitric acid and hydrogen peroxide in a microwave oven.The Sc,Y,In,Bi were added as internal standards to eliminate the matrix interferences.The results show that most of the relative standard deviations of these trace elements were below 3.5%,the standard recoveries of these elements were in the range of 91%-107%,and the detection limits were in the range of 0.001-0.006 μg·L-1. This method is accurate,rapid,convenience,and can be applied to the determination of arsenic,lead,cadmium,chromium,mercury and nickel in Chinese Herb with good results.展开更多
Inductively coupled plasma mass spectrometry(ICP-MS) was used to determine the concentration of Pb in atmospheric particulate samples,and the enrichment factor was calculated.The causes of the results were also discus...Inductively coupled plasma mass spectrometry(ICP-MS) was used to determine the concentration of Pb in atmospheric particulate samples,and the enrichment factor was calculated.The causes of the results were also discussed.展开更多
文摘An algorithm for precisely calculating the inductance of a three-section solenoid is presented, which is based on summing the layer self-inductances and the mutual inductances. A theoretical model with ex plicit expressions is firstly developed to calculate the self-inductance of a single layer, and then numerical calcu lation of the mutual inductance between two layers is introduced. Using the presented computation method, the inductance of a solenoid designed in the experiment is successfully calculated （4.30 mH）, which has a difference of less than 1% from the experimental data.
基金Project(cstc2019jcyj-msxm X0005)supported by General Program of Chongqing Natural Science Foundation,ChinaProject(51905062)supported by the National Natural Science Foundation of China。
文摘Magnetorheological(MR)materials are a class of smart material,whose the mechanical/rheological state can be controlled under a magnetic field.Magnetorheological materials are typically fluids,gels,or elastomers.In this study,anisotropic and isotropic magneto-rheological elastomer(MRE)samples were fabricated using a silicone rubber matrix with carbonyl iron particles as filler particles.The magnetic field-dependent inductance properties of these samples were studied using inductors specially designed for the analysis.The effect of the filler particle content,fabrication conditions,and inductance properties were characterized using a self-built system in both constant and transient magnetic fields.These factors show a significant effect on the inductance properties of the MRE inductor under an applied magnetic field.The anisotropic MRE inductor was more sensitive than the inductor based on an isotropic MRE.Owing to the presence of a constant magnetic field,the inductance value of the MRE inductor decreased with an increase in the external magnetic field.An attempt in elucidation of the mechanism is reported here.This study may enable the MRE to be widely used in practical applications such as monitoring magnetic field or detecting the filler particle content inside MR materials.
文摘A transformation of naphthalene-based coalescenced mesophase pitch(NMP)to mesophase microbeads was achieved by heating a mixture of NMP and fullerene(C_(60)).This is different from the conventional process of the liquid-phase carbonization of isotropic pitch to the emergence of carbon microbeads in the matrix and finally their growth to form a 100%anisotropic bulk meso-phase,but rather a reverse transformation.The effects of C_(60) loading and reaction temperature on the morphological transformation of mesophase were investigated by polarizing optical and scanning electron microscopies.The physical changes in the NMP induced by C_(60) were characterized by thermogravimetric analysis,Fourier transform infrared spectroscopy,X-ray diffractometry and Raman spectroscopy.The results show that the coalesced NMP can be converted to a spherical type at 300-320℃ with the addition of 5%C_(60),and the size of the mesophase microbeads increases with increasing temperature.Furthermore,a model is established to ex-plain the unique induction effect of C_(60) in the transformation process.This work makes the morphological transformation of MP con-trollable,and provides a new idea for the understanding and research of mesophase pitch.
文摘Using ultra-fine sample for determination 42 elements by pressurized acid digestion -ICP-MS, the mass of test portion can be reduced to 2 mg yet maintain the representation. And acid used for digestion could be reduced to less than 0.5 mL, reaction time also largely reduced.
文摘Inductively coupled plasma mass spectrometry (ICP-MS) was used to detect trace metal impurities in reagents such as H2O2, HNO3and H2SO4. The limit of detection to metal elements can be down to 2-20 ng/L in H2O2 and HNO3 and 0.1-1.0 ng/L in H2SO4.
文摘Inductively coupled plasma mass spectrometry (ICP-MS) was applied to determine copper, arsenic, cadmium, lead in athletic food using Sc, Ge, In, Bi as an internal standard. The linear correlation factor for four elements are higher than 0.999. Recoveries of spiked samples are in the range of 85.5%-115.5% and precision was fine, RSD is lower than 5.0%. And these are close agreement with the reference values in three standard reference materials of GBW08503, NBS1568, GBW08571. It indicates that the method is simple, rapid, sensitive and accurate, which can meet the demand for copper, arsenic, cadmium, lead analysis in athletic food.
文摘The isotopic analysis of 232Pu plutonium in 5×10-12 g/g samples using a multi-collector inductively coupled plasma mass spectrometry (MC-ICPMS) is described. IRMM-290b and uranium (UTB750) were used to correct the metrical data, and the analytical precision is about 0.5%.
文摘Six massive ores in the Jinchuan deposit were dated by Re-Os technique. The Os concentrations and isotopic ratios were determined by N-TIMS, while Re and Pt concentrations were determined by ICP-MS. The samples gave an isochron age of (852±25) Ma with an initial 187Os/188Os ratio of 0.255 ± 0.014. A 7-point Pt-Os isochrone gives an age of (870±38) Ma with an initial 186Os/188Os ratio of 0.119 84±0.000 27.
文摘To improve precision of analytical results of pressurized acid digestion-ICP-MS, the first step is to improve the homogeneity by reducing the particle size of sample. Using of ultra-fine sample (-500 mesh) can reduce the mass of the sample and the acid. The satisfactory precision is achieved at 2 mg sampling mass.
文摘The application of inductively coupled plasma mass spectrometry (ICP-MS) for determination of boron in water and urine samples was described. The detect limit (3σ) was 0.057 μg/L. The precision of the method was less than 2%. Multi-elements including Cr, Cu, Cd, Ba, Sr, Mn, Co, Tl, Li, Pb, Ca, Fe, K, Na, Mg, P, Si and Zn could be measured simultaneously. The method was successfully used in practice.
文摘A method of analysis trace element chloride in cleaning products by Inductively Coupled Plasma-Mass Sepctrometry (ICPMS) was studied. It has good precision (RSD<5%). The LOD is 0.06 μg/L (n=7). The recovery is 93.7%-110.0%.
文摘基于逆磁致伸缩效应,建立钢缆索索力传感器理论模型,分析了施加在缆索材料上的力信号(外力和应变)与磁信号(磁感应强度、磁场强度)之间的耦合关系.针对一种环式结构的索力传感器,对索力测量原理做了详细推导,可通过检测感应线圈的感应电压反映材料所受外力.传感器输出感应电压与空气间隙尺寸、外部激励磁场下的材料磁导率、激励磁场变化、加载外力变化等因素有关,重点分析了激励磁场变化和外力变化对传感器输出的影响.当外力是缓变力,可通过检测感应积分电压求得外力;当外力是交变力,直接通过感应电压求得外力;最后通过对磁场变化和外力变化影响分别进行了仿真,结果与理论分析基本一致,表明所建立的索力传感器理论模型可行.
Abstract：
Based on Villari-effect, the theoretic mdel d the cable tension sensor is presented. The relationship between mechanical parameters such as stress, strain and electromagnetic parameters like magnetic field and magnetic induction field are discussed. One loop-shaped stinulative structure of cable tension sensor based on Villari--effect is proposed and cable tension sensor principle is deeply analysed. By measuring inductive voltage in inductive loops, cable tension stress may be measured. Sensor output may be determined by air clearance, magnetic permeability, magnetic field, stress and inductive loops denseness. The sensor output effects resulting from magnetic field and stress ate analysed respectively. When stress changes tardigradely, the cable tension stress may be measured by measuring inductive integral voltage. When stress changes expeditiously, the cable tension stress may be measured by measuring inductive voltage. Sensor sensibility may be determined by stress frequency, inductive loops denseness, magnetic field and nagnetic permeability. In addition, the sensor output effects from magnetic changing and stress changing have been analysed with emulational methods. The results indicate that sensor theory model is feasible.
文摘In this paper,the determination of six heavy metal ions (arsenic,lead,cadmium,chromium,mercury and nickel) in the Chinese Herb by inductively coupled plasma-mass spectrometry (ICP-MS) was studied.The samples were digested by nitric acid and hydrogen peroxide in a microwave oven.The Sc,Y,In,Bi were added as internal standards to eliminate the matrix interferences.The results show that most of the relative standard deviations of these trace elements were below 3.5%,the standard recoveries of these elements were in the range of 91%-107%,and the detection limits were in the range of 0.001-0.006 μg·L-1. This method is accurate,rapid,convenience,and can be applied to the determination of arsenic,lead,cadmium,chromium,mercury and nickel in Chinese Herb with good results.
文摘Inductively coupled plasma mass spectrometry(ICP-MS) was used to determine the concentration of Pb in atmospheric particulate samples,and the enrichment factor was calculated.The causes of the results were also discussed.
