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UHPLC-Q Exactive高分辨质谱联用法分析淫羊藿中的化学成分 被引量:4
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作者 曾浏希 黎雄 +3 位作者 王东 李杨 杨洪艳 高路 《沈阳药科大学学报》 CAS CSCD 北大核心 2023年第5期581-592,662,共13页
目的采用UHPLC-Q Exactive四极杆-静电场轨道阱高分辨质谱联用技术鉴定分析淫羊藿药材成分。方法采用Thermo Hypersil GLOD C_(18)(100 mm×2.1 mm,1.9μm)色谱柱,体积分数0.1%甲酸水溶液-乙腈溶液为流动相进行梯度洗脱,流速为0.3 m... 目的采用UHPLC-Q Exactive四极杆-静电场轨道阱高分辨质谱联用技术鉴定分析淫羊藿药材成分。方法采用Thermo Hypersil GLOD C_(18)(100 mm×2.1 mm,1.9μm)色谱柱,体积分数0.1%甲酸水溶液-乙腈溶液为流动相进行梯度洗脱,流速为0.3 mL·min^(-1),柱温为40℃,电喷雾正、负离子模式扫描。结果共分析和鉴定出79个化合物,包括黄酮类、生物碱类、有机酸类和木脂素类化合物,其中16个化合物经与对照品比对鉴定。鉴定的黄酮类包括46个异戊烯基黄酮醇类化合物,异戊烯基黄酮醇类负离子模式二级特征碎片为m/z 367、351、513、353和323。初步鉴定化合物41、54、76、65和69为新的异戊烯基黄酮。结论淫羊藿中异戊烯基黄酮醇类多具有淫羊藿素或8-异戊烯基山奈酚苷元母核结构,该结果为淫羊藿成分的系统分析提供了数据支持。 展开更多
关键词 UHPLC-Q exactive 淫羊藿 淫羊藿素 8-异戊烯基山奈酚 异戊烯基的黄酮醇类
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超高效液相色谱-高分辨质谱测定白酒中氨基甲酸乙酯含量 被引量:20
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作者 熊晓通 胡峰 +4 位作者 尤小龙 尹艳艳 陈明学 程平言 钟方达 《食品科学》 EI CAS CSCD 北大核心 2021年第8期283-287,共5页
利用氨基甲酸乙酯(ehthy carbamate,EC)源内裂解的特殊性质,在超高效液相色谱-高分辨质谱一级全扫描模式下,以EC母离子(m/z 90.05)及其子离子(m/z 62.02)作为定性离子,m/z 62.02作为定量离子,开发酱香型白酒中EC的一级子离子定量法,有... 利用氨基甲酸乙酯(ehthy carbamate,EC)源内裂解的特殊性质,在超高效液相色谱-高分辨质谱一级全扫描模式下,以EC母离子(m/z 90.05)及其子离子(m/z 62.02)作为定性离子,m/z 62.02作为定量离子,开发酱香型白酒中EC的一级子离子定量法,有效解决了一级母离子定量噪音较大、二级子离子定量响应较低的问题。结果表明,在12.2~244μg/L内线性相关系数大于0.999,检出限为0.95μg/L,加标回收率在83.46%~106.79%之间,相对标准偏差为0.67%~3.54%。该方法具有分析速度快、检出限低、准确度高等优点,适用于酱香型白酒中EC的监控。 展开更多
关键词 氨基甲酸乙酯 源内裂解 Q exactive Focus质谱 一级子离子定量 酱香型白酒。
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高考英语模拟练习(上)
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作者 缪庭 《语言教育》 2002年第4期41-42,共2页
第一卷(三部分)第一部分:听力(略)第二部分:英语知识运用(共两节)第一节:单项填空(共15小题) 从A、B、C、D四个选项中,选出可以填入空白处的最佳选项。21.-You mean you know the man? No,Iknow man exactly like him. A.other B.the C... 第一卷(三部分)第一部分:听力(略)第二部分:英语知识运用(共两节)第一节:单项填空(共15小题) 从A、B、C、D四个选项中,选出可以填入空白处的最佳选项。21.-You mean you know the man? No,Iknow man exactly like him. A.other B.the C.不填 D.a22.He is late, is often the case. 展开更多
关键词 高考英语 单项填空 模拟练习 EXACTLY YESTERDAY invite THINK 完形填空 everything electricity
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Recursion-transform approach to compute the resistance of a resistor network with an arbitrary boundary 被引量:22
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作者 谭志中 《Chinese Physics B》 SCIE EI CAS CSCD 2015年第2期94-100,共7页
We consider a profound problem of two-point resistance in the resistor network with a null resistor edge and an arbitrary boundary,which has not been solved before because the Green's function technique and the Lapla... We consider a profound problem of two-point resistance in the resistor network with a null resistor edge and an arbitrary boundary,which has not been solved before because the Green's function technique and the Laplacian matrix approach are invalid in this case.Looking for the exact solutions of resistance is important but difficult in the case of the arbitrary boundary since the boundary is a wall or trap which affects the behavior of a finite network.In this paper,we give a general resistance formula that is composed of a single summation by using the recursion-transform method.Meanwhile,several interesting results are derived by the general formula.Further,the current distribution is given explicitly as a byproduct of the method. 展开更多
关键词 exact solution resistor network matrix equation recursion-transform boundary conditions
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Hawking Radiation from a Non-static Black Hole 被引量:22
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作者 ZHAO Zheng DAI Xianxin 《Chinese Physics Letters》 SCIE CAS CSCD 1991年第10期548-550,共3页
A method exactly determining an event horizon and its temperature in a nonstatic space-time is proposed.Using the generalised Tortoise coordinate,we give exact location of event horison and exact Hawking temperature f... A method exactly determining an event horizon and its temperature in a nonstatic space-time is proposed.Using the generalised Tortoise coordinate,we give exact location of event horison and exact Hawking temperature for a general spherically symmetric evaporating black hole. 展开更多
关键词 HORIZON Hawking EXACT
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Two-point resistance of an m×n resistor network with an arbitrary boundary and its application in RLC network 被引量:13
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作者 谭志中 《Chinese Physics B》 SCIE EI CAS CSCD 2016年第5期95-105,共11页
A rectangular m × n resistor network with an arbitrary boundary is investigated, and a general resistance formula between two nodes on an arbitrary axis is derived by the Recursion-Transform(RT) method, a probl... A rectangular m × n resistor network with an arbitrary boundary is investigated, and a general resistance formula between two nodes on an arbitrary axis is derived by the Recursion-Transform(RT) method, a problem that has never been resolved before, for the Green's function technique and the Laplacian matrix approach are inapplicable to it. To have the exact solution of resistance is important but it is difficult to obtain under the condition of arbitrary boundary. Our result is directly expressed in a single summation and mainly composed of characteristic roots, which contain both finite and infinite cases. Further, the current distribution is given explicitly as a byproduct of the method. Our framework can be effectively applied to RLC networks. As an application to the LC network, we find that our formulation leads to the occurrence of resonances at h_1= 1-cosφ_i-sinφ_icotnφ_i. This somewhat curious result suggests the possibility of practical applications of our formulae to resonant circuits. 展开更多
关键词 rectangular network exact solution RT method complex impedance
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New exact solitary wave solutions to generalized mKdV equation and generalized Zakharov-Kuzentsov equation 被引量:14
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作者 套格图桑 斯仁道尔吉 《Chinese Physics B》 SCIE EI CAS CSCD 2006年第6期1143-1148,共6页
In this paper, based on hyperbolic tanh-function method and homogeneous balance method, and auxiliary equation method, some new exact solitary solutions to the generalized mKdV equation and generalized Zakharov-Kuzent... In this paper, based on hyperbolic tanh-function method and homogeneous balance method, and auxiliary equation method, some new exact solitary solutions to the generalized mKdV equation and generalized Zakharov-Kuzentsov equation are constructed by the method of auxiliary equation with function transformation with aid of symbolic computation system Mathematica. The method is of important significance in seeking new exact solutions to the evolution equation with arbitrary nonlinear term. 展开更多
关键词 generalized mKdV equation generalized Zakharov-Kuzentsov equation nonlinear evolution equation auxiliary equation exact solitary wave solutions
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Exact Solutions of Nonlinear Evolution Equations in Mathematical Physics Using the Modified Simple Equation Method 被引量:10
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作者 E.M.E.Zayed S.A.Hoda Ibrahim 《Chinese Physics Letters》 SCIE CAS CSCD 2012年第6期1-4,共4页
The modified simple equation method is employed to construct the exact solutions involving parameters of nonlinear evolution equations via the (1+1)-dimensional modified KdV equation,and the (1+1)-dimensional reaction... The modified simple equation method is employed to construct the exact solutions involving parameters of nonlinear evolution equations via the (1+1)-dimensional modified KdV equation,and the (1+1)-dimensional reaction-diffusion equation.When these parameters are taken to be special values,the solitary wave solutions are derived from the exact solutions.It is shown that the proposed method provides a more powerful mathematical tool for solving nonlinear evolution equations in mathematical physics. 展开更多
关键词 equation. EXACT EQUATION
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Lie symmetries, perturbation to symmetries and adiabatic invariants of Poincaré equations 被引量:10
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作者 陈向炜 刘翠梅 李彦敏 《Chinese Physics B》 SCIE EI CAS CSCD 2006年第3期470-474,共5页
Based on the invariance of differential equations under infinitesimal transformations, Lie symmetry, laws of conservations, perturbation to the symmetries and adiabatic invariants of Poincaré equations are presen... Based on the invariance of differential equations under infinitesimal transformations, Lie symmetry, laws of conservations, perturbation to the symmetries and adiabatic invariants of Poincaré equations are presented. The concepts of Lie symmetry and higher order adiabatic invariants of Poincaré equations are proposed. The conditions for existence of the exact invariants and adiabatic invariants are proved, and their forms are also given. In addition, an example is presented to illustrate these results. 展开更多
关键词 Poincaré equations perturbation to symmetry exact invariant adiabatic invariant
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A hyperbolic function approach to constructing exact solitary wave solutions of the Hybrid lattice and discrete mKdV lattice 被引量:12
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作者 扎其劳 斯仁道尔吉 《Chinese Physics B》 SCIE EI CAS CSCD 2006年第3期475-477,共3页
Some new exact solitary wave solutions of the Hybrid lattice and discrete mKdV lattice are obtained by using a hyperbolic function approach. This approach can also be applied to other nonlinear differential-difference... Some new exact solitary wave solutions of the Hybrid lattice and discrete mKdV lattice are obtained by using a hyperbolic function approach. This approach can also be applied to other nonlinear differential-difference equations. 展开更多
关键词 hyperbolic function approach nonlinear differential-difference equation exact solitary wave solution
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Soliton excitations and chaotic patterns for the (2+1)-dimensional Boiti-Leon-Pempinelli system 被引量:8
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作者 杨征 马松华 方建平 《Chinese Physics B》 SCIE EI CAS CSCD 2011年第6期107-111,共5页
By improved projective equation approach and a linear variable separation approach, a new family of exact solutions of the (2+1)-dimensional Boiti-Leon-Pempinelli (BLP) system is derived. Based on the derived sol... By improved projective equation approach and a linear variable separation approach, a new family of exact solutions of the (2+1)-dimensional Boiti-Leon-Pempinelli (BLP) system is derived. Based on the derived solitary wave solution, some dromion and solitoff excitations and chaotic behaviours are investigated. 展开更多
关键词 BLP system exact solutions dromion and solitoff excitations chaotic behaviours
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A method for constructing exact solutions and application to Benjamin Ono equation 被引量:12
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作者 王振 李德生 +1 位作者 鲁慧芳 张鸿庆 《Chinese Physics B》 SCIE EI CAS CSCD 2005年第11期2158-2163,共6页
By using an improved projective Riccati equation method, this paper obtains several types of exact travelling wave solutions to the Benjamin Ono equation which include multiple soliton solutions, periodic soliton solu... By using an improved projective Riccati equation method, this paper obtains several types of exact travelling wave solutions to the Benjamin Ono equation which include multiple soliton solutions, periodic soliton solutions and Weierstrass function solutions. Some of them are found for the first time. The method can be applied to other nonlinear evolution equations in mathematical physics. 展开更多
关键词 Benjamin Ono equation nonlinear evolution equation Weierstrass function solutions exact solutions
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On dynamics of elastic rod based on exact Cosserat model 被引量:11
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作者 刘延柱 《Chinese Physics B》 SCIE EI CAS CSCD 2009年第1期1-8,共8页
The analysis of kinematics and dynamics of an elastic rod with circular cross section is studied on the basis of exact Cosserat model under consideration of the tension and shear deformation of the rod. The dynamical ... The analysis of kinematics and dynamics of an elastic rod with circular cross section is studied on the basis of exact Cosserat model under consideration of the tension and shear deformation of the rod. The dynamical equations of a rod with arbitrary initial shape are established in general form. The dynamics of a straight rod under axial tension and torsion is discussed as an example. In discussion of static stability in the space domain the Greenhill criteria of stability and the Euler load are corrected by the influence of tension and shear strain. In analysis of dynamical stability in the time domain it is shown that the Lyapunov and Euler stability conditions of the rod in space domain are the necessary conditions of Lyapunov's stability in the time domain. The longitudinal, torsional and lateral vibrations of a straight rod based on exact model are discussed, and an exact formula of free frequency of lateral vibration is obtained. The free frequency formulas of various simplified models, such as the Rayleigh beam, the Kirchhoff rod, and the Timoshenko beam, can be seen as special cases of the exact formula under different conditions of simplification. 展开更多
关键词 dynamics of elastic rod exact Cosserat model lateral vibration of rod
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Exact Analytic Solutions for a Finite Width Strip with a Single Edge Crack 被引量:7
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作者 FAN Tian-you YANG Xiao-chun LI He-xin 《Chinese Physics Letters》 SCIE CAS CSCD 1999年第1期32-34,共3页
The present study develops a conformal mapping technique and deals with the exact analytic solutions in closed form to the finite width strip with single edge crack.Some exact solutions including a universal suitable ... The present study develops a conformal mapping technique and deals with the exact analytic solutions in closed form to the finite width strip with single edge crack.Some exact solutions including a universal suitable constant are found,which are very useful in science and engineering. 展开更多
关键词 EXACT CONFORMAL ANALYTIC
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Lie symmetrical perturbation and adiabatic invariants of generalized Hojman type for Lagrange systems 被引量:8
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作者 罗绍凯 陈向炜 郭永新 《Chinese Physics B》 SCIE EI CAS CSCD 2007年第11期3176-3181,共6页
Based on the invariance of differential equations under infinitesimal transformations of group, Lie symmetries, exact invariants, perturbation to the symmetries and adiabatic invariants in form of non-Noether for a La... Based on the invariance of differential equations under infinitesimal transformations of group, Lie symmetries, exact invariants, perturbation to the symmetries and adiabatic invariants in form of non-Noether for a Lagrange system are presented. Firstly, the exact invariants of generalized Hojman type led directly by Lie symmetries for a Lagrange system without perturbations are given. Then, on the basis of the concepts of Lie symmetries and higher order adiabatic invariants of a mechanical system, the perturbation of Lie symmetries for the system with the action of small disturbance is investigated, the adiabatic invariants of generalized Hojman type for the system are directly obtained, the conditions for existence of the adiabatic invariants and their forms are proved. Finally an example is presented to illustrate these results. 展开更多
关键词 Lagrange system Lie symmetrical perturbation exact invariant adiabatic invariant of generalized Hojman type
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The Jacobi elliptic function-like exact solutions to two kinds of KdV equations with variable coefficients and KdV equation with forcible term 被引量:10
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作者 套格图桑 斯仁到尔吉 《Chinese Physics B》 SCIE EI CAS CSCD 2006年第12期2809-2818,共10页
By use of an auxiliary equation and through a function transformation, the Jacobi elliptic function wave-like solutions, the degenerated soliton-like solutions and the triangle function wave solutions to two kinds of ... By use of an auxiliary equation and through a function transformation, the Jacobi elliptic function wave-like solutions, the degenerated soliton-like solutions and the triangle function wave solutions to two kinds of Korteweg de Vries (KdV) equations with variable coefficients and a KdV equation with a forcible term are constructed with the help of symbolic computation system Mathematica, where the new solutions are also constructed. 展开更多
关键词 auxiliary equation KdV equation with variable coefficients KdV equation with a forcible term Jacobi elliptic function-like exact solutions
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Zoeppritz-based AVO inversion using an improved Markov chain Monte Carlo method 被引量:8
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作者 Xin-Peng Pan Guang-Zhi Zhang +1 位作者 Jia-Jia Zhang Xing-Yao Yin 《Petroleum Science》 SCIE CAS CSCD 2017年第1期75-83,共9页
The conventional Markov chain Monte Carlo (MCMC) method is limited to the selected shape and size of proposal distribution and is not easy to start when the initial proposal distribution is far away from the target ... The conventional Markov chain Monte Carlo (MCMC) method is limited to the selected shape and size of proposal distribution and is not easy to start when the initial proposal distribution is far away from the target distribution. To overcome these drawbacks of the conventional MCMC method, two useful improvements in MCMC method, adaptive Metropolis (AM) algorithm and delayed rejection (DR) algorithm, are attempted to be combined. The AM algorithm aims at adapting the proposal distribution by using the generated estimators, and the DR algorithm aims at enhancing the efficiency of the improved MCMC method. Based on the improved MCMC method, a Bayesian amplitude versus offset (AVO) inversion method on the basis of the exact Zoeppritz equation has been developed, with which the P- and S-wave velocities and the density can be obtained directly, and the uncertainty of AVO inversion results has been estimated as well. The study based on the logging data and the seismic data demonstrates the feasibility and robustness of the method and shows that all three parameters are well retrieved. So the exact Zoeppritz-based nonlinear inversion method by using the improved MCMC is not only suitable for reservoirs with strong-contrast interfaces and longoffset ranges but also it is more stable, accurate and antinoise. 展开更多
关键词 Adaptive Metropolis (AM) algorithm Delayed rejection (DR) algorithm Bayesian AVOinversion Exact Zoeppritz Nonlinear inversion
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The Power Supply System for HL-2A Tokamak's Magnetic Field 被引量:6
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作者 宣伟民 姚列英 +2 位作者 陈宇红 邵葵 王英翘 《Plasma Science and Technology》 SCIE EI CAS CSCD 2007年第2期211-215,共5页
The highpower pulsed power supply system for the magnetic field of the HL-2A Tokamak is described in this paper. The total output power of its eight magnetic field power supply units of nearly 250 MW. Their highest DC... The highpower pulsed power supply system for the magnetic field of the HL-2A Tokamak is described in this paper. The total output power of its eight magnetic field power supply units of nearly 250 MW. Their highest DC output voltage and current are 3510 V and 45 kA, respectively. All the units are operated in a pulsed mode. The pulse duration is 5 s, and the cyclic period is 15 min. The power supply system consists mainly of pulsed flywheel motor generators, rectifying transformers, thyristor converters, diode rectifiers and switches. The system incorporates many key technologies-supply equalization with two generators and four diode bridges, constant-angle phase triggers with a wide frequency range, current equalization, a status detector for the high current 6-phase converter, and advanced monitoring based on a programmable logic computer and engineering parameter measurement. The experimental results show that the performance of the power supply system satisfies the requirements of HL-2A experiments very well. 展开更多
关键词 high power HL-2A pulsed magnet power supply current equalization exact phase shift
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Dressing Multiphoton Hamiltonian 被引量:5
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作者 ZHOU Peng PENG Jinsheng 《Chinese Physics Letters》 SCIE CAS CSCD 1992年第1期13-16,共4页
The dressed Hamiltonian describing the multiphoton process is presented by means of a canonical transformation.The exact eigenvalues and eigenstates are given for any set of parameters ω_(0),ω and ε.The general evo... The dressed Hamiltonian describing the multiphoton process is presented by means of a canonical transformation.The exact eigenvalues and eigenstates are given for any set of parameters ω_(0),ω and ε.The general evolution of this system is obtained. 展开更多
关键词 HAMILTONIAN EXACT CANONICAL
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Bright and dark soliton solutions for some nonlinear fractional differential equations 被引量:6
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作者 Ozkan Guner Ahmet Bekir 《Chinese Physics B》 SCIE EI CAS CSCD 2016年第3期52-59,共8页
In this work, we propose a new approach, namely ansatz method, for solving fractional differential equations based on a fractional complex transform and apply it to the nonlinear partial space-time fractional modified... In this work, we propose a new approach, namely ansatz method, for solving fractional differential equations based on a fractional complex transform and apply it to the nonlinear partial space-time fractional modified Benjamin-Bona- Mahoney (mBBM) equation, the time fractional mKdV equation and the nonlinear fractional Zoomeron equation which gives rise to some new exact solutions. The physical parameters in the soliton solutions: amplitude, inverse width, free parameters and velocity are obtained as functions of the dependent model coefficients. This method is suitable and more powerful for solving other kinds of nonlinear fractional PDEs arising in mathematical physics. Since the fractional deriva- tives are described in the modified Riemann-Liouville sense. 展开更多
关键词 exact solutions ansatz method space-time fractional modified Benjamin-Bona-Mahoney equa-tion time fractional mKdV equation
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