This work investigated the microstructure,magnetic properties,and crystallization kinetics of the as-spun and annealed alloy ribbons of(Fe_(40-x)Co_xNi_(40)Si_(6.33)B_(12.66)Cu_1)_(0.97)Nb_(0.03),where x=0,6,7,8,9,pre...This work investigated the microstructure,magnetic properties,and crystallization kinetics of the as-spun and annealed alloy ribbons of(Fe_(40-x)Co_xNi_(40)Si_(6.33)B_(12.66)Cu_1)_(0.97)Nb_(0.03),where x=0,6,7,8,9,prepared using the meltspinning method.The results show that adding a moderate amount of Co can improve the glass forming ability(GFA),the first peak crystallization temperature,and thermal stability of the as-spun alloy ribbons.With x=7,the two-stage crystallization temperature interval△Tx=90 exhibits optimal thermal stability,and the alloy annealed at 673 K for 10 minutes shows the favorable combined magnetic properties,with H_(c)=0.12 A/m,M_(s)=88.7 A·m^(2)/kg,andμ_(e)=13800.The magnetic domain results show that annealing removes numerous pinning points in the magnetic domains of the alloy ribbons,making the domain walls smoother and effectively reducing the pinning effect.展开更多
基金Project supported by the National Natural Science Foundation of China(Grant No.52275567)the Key Research and Development Program of Shanxi Province,China(Grant No.202202050201020)+3 种基金the Doctoral Starting-up Foundation of Taiyuan University of Science and Technology(Grant No.20192016)the Research Project Supported by Shanxi Scholarship Council(Grant No.2017-085)the Graduate Education and Teaching Reform Project of Shanxi Province,China(Grant No.2023JG136)the Special Fund for Science and Technology Innovation Teams of Shanxi Province,China(Grant No.202304051001036)。
文摘This work investigated the microstructure,magnetic properties,and crystallization kinetics of the as-spun and annealed alloy ribbons of(Fe_(40-x)Co_xNi_(40)Si_(6.33)B_(12.66)Cu_1)_(0.97)Nb_(0.03),where x=0,6,7,8,9,prepared using the meltspinning method.The results show that adding a moderate amount of Co can improve the glass forming ability(GFA),the first peak crystallization temperature,and thermal stability of the as-spun alloy ribbons.With x=7,the two-stage crystallization temperature interval△Tx=90 exhibits optimal thermal stability,and the alloy annealed at 673 K for 10 minutes shows the favorable combined magnetic properties,with H_(c)=0.12 A/m,M_(s)=88.7 A·m^(2)/kg,andμ_(e)=13800.The magnetic domain results show that annealing removes numerous pinning points in the magnetic domains of the alloy ribbons,making the domain walls smoother and effectively reducing the pinning effect.