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Geometric dilution of precision for GPS single-point positioning based on four satellites 被引量:5
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作者 Wang Huihui Zhan Xingqun Zhang Yanhua 《Journal of Systems Engineering and Electronics》 SCIE EI CSCD 2008年第5期1058-1062,F0003,共6页
To improve the positioning accuracy in GPS point positioning, the geometric dilution of precision (GDOP) including HDOP, VDOP, TDOP, PDOP is commonly considered. The properties of the DOP for the GPS satellite navig... To improve the positioning accuracy in GPS point positioning, the geometric dilution of precision (GDOP) including HDOP, VDOP, TDOP, PDOP is commonly considered. The properties of the DOP for the GPS satellite navigation system are studied and the coordinate system is improved in order to decrease the amount of variables. In the end, by simulation and discussing the results, the corresponding conclusions are presented. 展开更多
关键词 GPS dilution of precision GDOP NAVIGATION simulation.
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Effects of Diet Dilution during the Finishing Period on the Performance and Carcass Characteristics of Broiler Chickens
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作者 SHI Bao-ming SHAN An-shan CHAN Long 《Journal of Northeast Agricultural University(English Edition)》 CAS 2005年第2期122-125,共4页
An experiment was conducted to study the response of broiler to diet dilution during the finishing period. Sixty 29-day-old commercial Avian male broiler chicks were assigned to two groups randomly, with 30 broilers e... An experiment was conducted to study the response of broiler to diet dilution during the finishing period. Sixty 29-day-old commercial Avian male broiler chicks were assigned to two groups randomly, with 30 broilers each. Birds were offered a conventional finishing diet or with 10% dilution diet with ground rice hulls from 29 to 49 days of age. The result showed that there were no significant differences between the effects of diet dilution and the control on final body weight, growth rate and feed conversion efficiency. Diet dilution led to a reduction in abdominal fat weight, whereas carcass and breast muscle weight were not affected. 展开更多
关键词 BROILER diet dilution finishing period carcass characteristics
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同位素稀释-HRGC-LRMS法测定环境样品中二噁英类多氯联苯 被引量:8
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作者 刘劲松 谭香萍 +3 位作者 庞晓露 高亮 钟光剑 许行义 《分析测试学报》 CAS CSCD 北大核心 2004年第z1期177-180,共4页
  多氯联苯(PCBs)是一类具有209种同类物的高毒性、难降解、强脂溶性和生物累积性的持久性有机污染物,自从1996年Jensen首次在鹰和鲱鱼中发现PCBs后[1,2],现在已在世界各地不同的环境介质中都发现有PCBs的存在[3].……
关键词 Isotope dilution HRGC - LRMS Dioxin-like PCBs Environmental sample
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高效液相色谱法-同位素稀释质谱联用法对奶粉中维生素A含量的检测 被引量:5
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作者 黄挺 张伟 +2 位作者 刘军 田颖 杨改霞 《分析测试学报》 CAS CSCD 北大核心 2008年第S1期195-196,共2页
A method for the determination of vitamin A in milk powder was developed by high performance liquid chromatography-isotope dilution mass spectrometry(HPLC-ID MS) and using deuterium-labeled vitamin A as an internal st... A method for the determination of vitamin A in milk powder was developed by high performance liquid chromatography-isotope dilution mass spectrometry(HPLC-ID MS) and using deuterium-labeled vitamin A as an internal standard.RSD of the method was 2.85%.This method was applied in the determination of standard reference material SRM 1849 with satisfactory results. 展开更多
关键词 liquid chromatography ISOTOPE dilution mass SPECTROMETRY milk powder VITAMIN A
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液相色谱同位素稀释质谱对寡核苷酸含量的测定研究 被引量:4
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作者 高运华 武利庆 +2 位作者 王晶 张玲 刘张岚 《分析测试学报》 CAS CSCD 北大核心 2008年第S1期33-36,共4页
The mass of oligonucleotides was quantitated by liquid chromatography-isotope dilution mass spectrometry.The uncertainty was calculated.This could provide information for the further quantitative measurement and utili... The mass of oligonucleotides was quantitated by liquid chromatography-isotope dilution mass spectrometry.The uncertainty was calculated.This could provide information for the further quantitative measurement and utilization of DNA. 展开更多
关键词 QUANTITATION OLIGONUCLEOTIDES liquid chromatography-isotope dilution mass SPECTROMETRY
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LC-MS/MS同位素稀释法测定食品中地西泮和氯丙嗪残留量 被引量:3
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作者 朱坚 邓晓军 +1 位作者 郭德华 李波 《分析测试学报》 CAS CSCD 北大核心 2007年第z1期239-241,共3页
This article concentrates on the method of the determination of diazepam and chlorpromazine residue in meat and kidney,by using HPLC-MS/MS.The D6-chlorpromazine was added to sample as an internal standard.Then extract... This article concentrates on the method of the determination of diazepam and chlorpromazine residue in meat and kidney,by using HPLC-MS/MS.The D6-chlorpromazine was added to sample as an internal standard.Then extracted the sample with acetonitrile,cleaned up the extract through Oasis HLB cartridge.Determination and confirmation is made by means of liquid chromatography-tandem mass spectrometry,using internal standard method.The limit of quantitation of chlorpromazine and diazepam are all 1.0 μg/kg. 展开更多
关键词 LC-MS/MS Isotope dilution DIAZEPAM CHLORPROMAZINE
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我国某城市市售食品中PCDD/Fs污染水平和人群二噁英膳食暴露量研究 被引量:1
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作者 张建清 蒋友胜 +10 位作者 周健 方道奎 姜杰 刘桂华 张红宇 谢建滨 黄薇 张锦州 李慧 王舟 潘柳波 《分析测试学报》 CAS CSCD 北大核心 2007年第z1期228-230,共3页
The status of PCDDs and PCDFs content in retail foods from a certain area by Isotope Dilution HRGC-HRMS was surveyed and the local population PCDD/Fs exposure from diverse foods and health risk was evaluated.PCDD/Fs w... The status of PCDDs and PCDFs content in retail foods from a certain area by Isotope Dilution HRGC-HRMS was surveyed and the local population PCDD/Fs exposure from diverse foods and health risk was evaluated.PCDD/Fs was extracted from samples by Soxhlet extraction,concentrated and purified by FMS column chromatograph,carbon column enrichment.Confirmation and quantitative analysis at pg/g level of PCDD/Fs was performed by HRGC/HRMS using multiple ion detection mode(MID).TEQ concentration was calculated by WHO-TEF multiplying by concentration of seventeen PCDD/Fs congener.Median of PCDD/Fs concentration for fish,livestock,poultry,egg,vegetable oil,milk,vegetable totally 100 samples for ten diverse foods didn’t exceed the limit standards by EU.The level of PCDD/Fs for different food in the certain area was lower or comparable to the data reported by developed country in the world.The total weekly intake and monthly intake for local population or national population was 3.44,14.8 WHO-TEQ/kg BW and 1.5,6.42 pg WHO-TEQ/kg BW respectively,the value was lower than the Tolerable Weekly Intake of 14 pg WHO TEQ/kg BW for PCDDs,PCDFs and dioxin-like PCBs established by EU Scientific Committee for Food.The dietary PCDD/Fs intake for local people was higher than national population.And animal food was the dominant contributor to the total dietary intake,which accounted for more than 70 percent.These levels of consumption of diverse food containing typical levels of PCDD/Fs doesn’t present a risk to the health of the local population.But integrative dietary intake could be evaluated including of PCBs intake for population in the future. 展开更多
关键词 Gas chromatography-high resolution mass spectrometry(HRGC-HRMS) Isotope dilution Retailed foods PCDD/Fs contamination Human dietary intake
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同位素稀释-ICPMS法测定地质标准物质中铂族元素 被引量:2
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作者 胡明月 何红蓼 《质谱学报》 EI CAS CSCD 2005年第z1期9-10,共2页
Platinum group elements (PGEs) includes platinum, palladium, iridium, osmium, rhodium and ruthenium. It has very high economic and scientific value in the field of geoscience and environmental science. But the analysi... Platinum group elements (PGEs) includes platinum, palladium, iridium, osmium, rhodium and ruthenium. It has very high economic and scientific value in the field of geoscience and environmental science. But the analysis data referred by the different lab are very disperse because of the difficulty of the determination of PGEs. It makes very difficult to fix the value of the PGEs in the standard reference materials. In the article, the values of the PGEs in the standard reference materials of ocean sediment are determined by isotope dilution technique and dependable values of these elements are provided. 展开更多
关键词 ISOTOPE dilution technique PLATINUM group elements ocean SEDIMENT
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国际比对CCQM-P77a血清中氢化可的松测定 被引量:1
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作者 戴新华 徐锐锋 +1 位作者 王卫华 张春梅 《分析测试学报》 CAS CSCD 北大核心 2007年第z1期55-57,60,共4页
The concept of metrological traceability in laboratory medicine has increasingly received considerable recognition worldwide.The Consultative Committee for Amount of Substance (CCQM) which concerned international comp... The concept of metrological traceability in laboratory medicine has increasingly received considerable recognition worldwide.The Consultative Committee for Amount of Substance (CCQM) which concerned international comparisons and establishment of international equivalence between national laboratories had organized international comparison CCQM-P77a: determination of serum cortisol in 2006.National Institute of Metrology (NIM) took part in the comparison as the representative of China and received good performance according to the results published by CCQM. 展开更多
关键词 International comparison CORTISOL Isotope dilution mass spectrometry
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ID-TIMS 准确测定国际关键比对大米粉中痕量镉
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作者 王军 赵墨田 逯海 《质谱学报》 EI CAS CSCD 2005年第z1期1-2,共2页
The method of isotope dilution thermal ionization mass spectrometry able to trace to SI was developed to accurately measure trace amount of cadmium in the rice powder sample from CCQM-K24 international key comparison ... The method of isotope dilution thermal ionization mass spectrometry able to trace to SI was developed to accurately measure trace amount of cadmium in the rice powder sample from CCQM-K24 international key comparison organized by CCQM(Comité Consultatif pour la Quantité de Matière, Paris). By comparison with our previous work, there was much improvement in aspects of digestion of the rice powder sample, separation of cadmium from the sample and dry-mass correction. As a result, the blank of this procedure was reduced and the measurement precisions of isotopic ratios of cadmium were increased. In addition, the uncertainty evaluation of the entire process of measurement was profoundly studied. The analytical result of this work (14.53±0.15) nmol/g was in agreement with the certified value. 展开更多
关键词 ISOTOPE dilution thermal ionization mass SPECTROMETRY international comparison cadmium rice powder
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质谱法分析机油中铀的样品处理技术
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作者 张海路 肖吉群 袁莉 《质谱学报》 EI CAS CSCD 2005年第z1期25-26,共2页
The technique of sample handling for uranium in machine oil was introduced by burning, nitric acid and vitriol. The effects of separations were analyzed by isotope dilution mass spectrum (IDMS). The effect of separati... The technique of sample handling for uranium in machine oil was introduced by burning, nitric acid and vitriol. The effects of separations were analyzed by isotope dilution mass spectrum (IDMS). The effect of separation by vitriol and nitric acid are better than that by burning. Vitriol can carbonize oil better. 展开更多
关键词 machine OIL URANIUM vitriol CARBONIZATION ISOTOPE dilution
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液相色谱-同位素稀释质谱精确测定奶粉中的核苷酸含量
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作者 高运华 武利庆 王晶 《分析测试学报》 CAS CSCD 北大核心 2007年第z1期236-238,241,共4页
Adenosine 5′-monophosphate in powdered milk was quantitated by liquid chromatography-isotope dilution mass spectrometry.The uncertainty was calculated.This could provide information for the further quantitative measu... Adenosine 5′-monophosphate in powdered milk was quantitated by liquid chromatography-isotope dilution mass spectrometry.The uncertainty was calculated.This could provide information for the further quantitative measurement and utilization of 5′-nucleotide acid as food additive. 展开更多
关键词 QUANTITATION Adenosine 5′-monophosphate Liquid chromatography-isotope dilution mass spectrometry Powdered milk
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同位素稀释质谱法对溶液中血管紧张素Ⅰ含量的测定 被引量:2
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作者 武利庆 王晶 +3 位作者 张玲 盛灵慧 杨彬 黎朋 《分析测试学报》 CAS CSCD 北大核心 2008年第S1期21-22,25,共3页
The presented work is to determine the mass fraction of angiotensinⅠ in solution by isotope dilution method,which is a pilot study organized by Consultative Committee for Amount of Substance.Firstly,the hydrolysis ti... The presented work is to determine the mass fraction of angiotensinⅠ in solution by isotope dilution method,which is a pilot study organized by Consultative Committee for Amount of Substance.Firstly,the hydrolysis time and hydrochloric acid addition volume ratio were optimized and the degradation of natural and isotope labeled proline,valine,leucine and phenylalanine during the hydrolysis process were investigated.Secondly,the mass fractions of proline,valine,isoleucine and phenylalanine in the angiotensinⅠhydrolysis solution was determined employing isotope dilution method with their reference materials as standards.Finally,the angiotensinⅠ mass fraction and associated uncertainty were calculated according to the amino acid mass fraction obtained,which was(75.2±2.6) μg/g.It showed that the result obtained in this paper has good equivalence with the average.It can be concluded that the isotope dilution method for peptide quantification is accurate and is suitable for peptide reference materials production. 展开更多
关键词 angiotensinⅠ PEPTIDE quantification ISOTOPE dilution mass SPECTROMETRY
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白酒中挥发性苦涩味物质的提取和分离 被引量:21
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作者 王尹叶 范文来 徐岩 《食品与发酵工业》 CAS CSCD 北大核心 2018年第6期240-244,共5页
为鉴定白酒中挥发性苦味和涩味化合物,建立了一种新的提取和分离白酒中苦味和涩味物质的方法。通过梯度减压蒸馏将白酒样品分成4个组分(A、B、C和D),具有强烈苦味和涩味的组分B通过半制备液相再分离,得到10个亚组分,每个亚组分分别用戊... 为鉴定白酒中挥发性苦味和涩味化合物,建立了一种新的提取和分离白酒中苦味和涩味物质的方法。通过梯度减压蒸馏将白酒样品分成4个组分(A、B、C和D),具有强烈苦味和涩味的组分B通过半制备液相再分离,得到10个亚组分,每个亚组分分别用戊烷和乙醚萃取,收集乙醚萃取相。将每一个乙醚相平均分成两份,一份用纯净水洗涤,水洗相用真空旋转蒸发除去溶剂,用于味觉稀释分析(taste dilution analysis,TDA);另一份氮吹浓缩至250μL进行GC-MS分析。TDA结果表明,4个乙醚萃取组分B-8-Ⅱ、B-2-Ⅱ、B-3-Ⅱ和B-4-Ⅱ具有较高的TD值,其涩味TD值分别为128、64、32和8,苦味TD值分别为32、16、16和8。通过GC-MS共鉴定出7种呈味化合物,经标准品验证,2-苯乙醇和乳酸乙酯呈现涩味;糠醛、2-甲基丙醇、3-甲基丁醇、1-丁醇和正丙醇呈涩味和苦味,其中,2-苯乙醇的味觉特征是首次报道。 展开更多
关键词 白酒 苦味 涩味 味觉稀释分析(taste dilution analysis TDA) 2-苯乙醇
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高效液相色谱-同位素稀释质谱法测定血清中的苯丙氨酸 被引量:4
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作者 武利庆 王晶 《分析测试学报》 CAS CSCD 北大核心 2007年第z1期98-99,103,共3页
Phenylalanine in serum was determined by HPLC isotope dilution mass spectrometry method with D8 labeled phenylalanine as internal standard.Phenylalanine and its isotope labeled analogue were monitored at the transitio... Phenylalanine in serum was determined by HPLC isotope dilution mass spectrometry method with D8 labeled phenylalanine as internal standard.Phenylalanine and its isotope labeled analogue were monitored at the transitions m/z=166→120 and 172→126 in multiple reaction monitoring (MRM) mode,respectively,which effectively eliminated the matrix effect.The RSD for 5 repeats measurement of the same sample was 0.5%.Uncertainty was evaluated,which showed the main uncertainty was from the purity assessment of phenylalanine reference material and the variation of method.The presented method can be applied into value assessment of reference material of phenylalanine in serum,and it can be also used for traceability establishment of the measurement of phenylalanine in serum. 展开更多
关键词 SERUM PHENYLALANINE Isotope dilution mass spectrometry UNCERTAINTY
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基于构型优选的5G集群无人机协同导航方法 被引量:2
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作者 高超 黄郑 +2 位作者 赵轩 王红星 龙涛 《系统仿真学报》 CAS CSCD 北大核心 2024年第4期981-990,共10页
针对现有基于测距的集群UAV协同导航方法普遍忽略了空间构型对定位定能的影响,难以获得精确的导航定位结果,提出一种基于空间构型优选的5G集群UAV协同导航方法。构建了复杂环境下基于5G信号的UAV相对测距误差模型,基于最小几何精度因子(... 针对现有基于测距的集群UAV协同导航方法普遍忽略了空间构型对定位定能的影响,难以获得精确的导航定位结果,提出一种基于空间构型优选的5G集群UAV协同导航方法。构建了复杂环境下基于5G信号的UAV相对测距误差模型,基于最小几何精度因子(geometric dilution of precision,GDOP)准则建立了协同导航节点寻优策略,实现了协同导航空间构型的实时优选;设计了基于5G测距网络的协同导航滤波器,对UAV导航信息进行在线估计和实时补偿,提高集群UAV的协同定位精度。仿真结果表明:该方法从机定位精度平均提升了约42.05%,为集群UAV实现在卫星不可用条件下的自主导航提供了一种有效的新方法。 展开更多
关键词 5G测距 协同导航 多无人机 GDOP(geometric dilution of precision) 最优构型
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Cavity 3D modeling and correlative techniques based on cavity monitoring 被引量:25
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作者 罗周全 刘晓明 +2 位作者 张保 鹿浩 李畅 《Journal of Central South University of Technology》 EI 2008年第5期639-644,共6页
According to the mining method for Dongguashan Copper Mine and Tongkeng Mine in China, and with the help of the cavity monitoring system(CMS) and mining software Surpac, the 3D cavity models were established exactly... According to the mining method for Dongguashan Copper Mine and Tongkeng Mine in China, and with the help of the cavity monitoring system(CMS) and mining software Surpac, the 3D cavity models were established exactly. A series of correlative techniques for calculating stope over-excavation and under-excavation, stope dilution and ore loss rates, and the blasting design of the pillar with complicated irregular boundaries were developed. These techniques were applied in Dongguashan Copper Mine and Tongkeng Mine successfully. Using these techniques, the dilution rates of stopes 52-2^#, 52-6^#, 52-8^#and 52-10^# of Dongguashan Copper Mine are calculated to be 2.12%, 8.46%, 12-67% and 10.68%, respectively, and the ore loss rates of stopes 52-6^# and 5-8^# are 4.41% and 3.70%, severally. Furthermore, according to the design accomplished by the technique for a pillar of Tongkeng Mine with irregular boundary, the volume, total length of boreholes and the dynamite quantity of the pillar are computed to be 1.2 ×10^4 m^3, 2.98 km and 10.97 t, correspondingly. 展开更多
关键词 cavity 3D modeling cavity monitoring system STOPE dilution loss rate pillar blasting
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Cooperative localization against GPS signal loss in multiple UAVs flight 被引量:7
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作者 Yaohong Qu Youmin Zhang 《Journal of Systems Engineering and Electronics》 SCIE EI CSCD 2011年第1期103-112,共10页
Based on multiple unmanned aerial vehicles(UAVs) flight at a constant altitude,a fault-tolerant cooperative localization algorithm against global positioning system(GPS) signal loss due to GPS receiver malfunction... Based on multiple unmanned aerial vehicles(UAVs) flight at a constant altitude,a fault-tolerant cooperative localization algorithm against global positioning system(GPS) signal loss due to GPS receiver malfunction is proposed.Contrast to the traditional means with single UAV,the proposed method is based on the use of inter-UAV relative range measurements against GPS signal loss and more suitable for the small-size and low-cost UAV applications.Firstly,for re-localizing an UAV with a malfunction in its GPS receiver,an algorithm which makes use of any other three healthy UAVs in the cooperative flight as the reference points for re-localization is proposed.Secondly,by using the relative ranges from the faulty UAV to the other three UAVs,its horizontal location can be determined after the GPS signal is lost.In order to improve an accuracy of the localization,a Kalman filter is further exploited to provide the estimated location of the UAV with the GPS signal loss.The Kalman filter calculates the variance of observations in terms of horizontal dilution of positioning(HDOP) automatically.Then,during each discrete computing time step,the best reference points are selected adaptively by minimizing the HDOP.Finally,two simulation examples in Matlab/Simulink environment with five UAVs in cooperative flight are shown to evaluate the effectiveness of the proposed method. 展开更多
关键词 unmanned aerial vehicle(UAV) cooperative localization Kalman filter horizontal dilution of positioning(HDOP).
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Optimality of Group Testing with Differential Misclassification
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作者 LI Yiming ZHANG Hong LIU Aiyi 《应用概率统计》 CSCD 北大核心 2024年第4期644-662,共19页
Group testing is a method that can be used to estimate the prevalence of rare infectious diseases,which can effectively save time and reduce costs compared to the method of random sampling.However,previous literature ... Group testing is a method that can be used to estimate the prevalence of rare infectious diseases,which can effectively save time and reduce costs compared to the method of random sampling.However,previous literature only demonstrated the optimality of group testing strategy while estimating prevalence under some strong assumptions.This article weakens the assumption of misclassification rate in the previous literature,considers the misclassification rate of the infected samples as a differentiable function of the pool size,and explores some optimal properties of group testing for estimating prevalence in the presence of differential misclassification conforming to this assumption.This article theoretically demonstrates that the group testing strategy performs better than the sample by sample procedure in estimating disease prevalence when the total number of sample pools is given or the size of the test population is determined.Numerical simulation experiments were conducted to evaluate the performance of group tests in estimating prevalence in the presence of dilution effect. 展开更多
关键词 group testing sensitivity SPECIFICITY dilution effect differential misclassification PREVALENCE
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Determination of Thermokinetic Parameters in Dissolution Process of DMF of Carbohydrazide Styphnates by Microcalorimetry
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作者 LIU Ying YANG Li ZHANG Tong-lai 《火炸药学报》 EI CAS CSCD 北大核心 2013年第5期49-53,共5页
The dissolving processes,thermochemical properties and thermokinetic parameters of manganese carbohydrazide styph-nate([Mn2(CHZ)2(TNR)2(H2O)4]),nickel carbohydrazide styphnate([Ni(CHZ),(TNR)],)and lead carbohydrazide ... The dissolving processes,thermochemical properties and thermokinetic parameters of manganese carbohydrazide styph-nate([Mn2(CHZ)2(TNR)2(H2O)4]),nickel carbohydrazide styphnate([Ni(CHZ),(TNR)],)and lead carbohydrazide styphnate([Pb_(2)(CHZ)_(2)(TNR)_(2)(H_(2)O)_(2)])in N,N-dimethylformamide(DMF)at 298,15 K were studied by a SETARAM C80 calorime-ter.The results show that the dissolving process of them in DMF are exothermic,however the exothermic peaks are different.The results are associated with the different molecular structure and polarity of solutes.The empirical formulas for the enthalpies of dis-solution(△mH),the relative apparent molar enthalpies(ΦL;),the relative partial molar enthalpies(L,),and the enthalpies of di-lution(△aHt.:)are respectively deduced by polynomial fitting of experimental data.The standard enthalpies of dissolution(Aai H)are calculated respectively as-17.75kJ·mol^(-1),-29.76kJ·mol^(-1)and-15.35 kJ·mol^(-1).The rate constant of dissolution reaction(k),and the reaction order(n)are obtained from the kinetic formulas. 展开更多
关键词 physical chemistry thermochemistrys kinetics CARBOHYDRAZIDE styphnis acid enthalpies of solution enthalpies of dilution
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