期刊文献+
共找到851篇文章
< 1 2 43 >
每页显示 20 50 100
An optimal design of the liquid-cooling plate channel in a power battery based on response surface methodology
1
作者 Jinbo Zheng Jibin Jiang +2 位作者 Xiwei Yu Bingjun Yan Guofu Lian 《中国科学技术大学学报》 北大核心 2025年第2期52-65,51,I0002,共16页
The work takes a new liquid-cooling plate in a power battery with pin fins inside the channel as the object.A mathematical model is established via the central composite design of the response surface to study the rel... The work takes a new liquid-cooling plate in a power battery with pin fins inside the channel as the object.A mathematical model is established via the central composite design of the response surface to study the relationships among the length,width,height,and spacing of pin fins;the maximum temperature and temperature difference of the battery module;and the pressure drop of the liquid-cooling plate.Model accuracy is verified via variance analysis.The new liquid-cooling plate enables the power battery to work within an optimal temperature range.Appropriately increasing the length,width,and height and reducing the spacing of pin fins could reduce the temperature of the power battery module and improve the temperature uniformity.However,the pressure drop of the liquid-cooling plate increases.The structural parameters of the pin fins are optimized to minimize the maximum temperature and the temperature difference of the battery module as well as the pressure drop of the liquid-cooling plate.The errors between the values predicted and actual by the simulation test are 0.58%,4%,and 0.48%,respectively,which further verifies the model accuracy.The results reveal the influence of the structural parameters of the pin fins inside the liquid-cooling plate on its heat dissipation performance and pressure drop characteristics.A theoretical basis is provided for the design of liquid-cooling plates in power batteries and the optimization of structural parameters. 展开更多
关键词 response surface methodology power battery cooling channel optimal design
在线阅读 下载PDF
Heat treatment optimization for tensile properties of 8011 Al/15% SiCp metal matrix composite using response surface methodology 被引量:7
2
作者 V.VEMBU G.GANESAN 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2015年第4期390-395,共6页
In this study,a mathematical model was developed to optimize the heat treatment process for maximum tensile strength and ductility of aluminum(8011) silicon carbide particulate composites.The process parameters are so... In this study,a mathematical model was developed to optimize the heat treatment process for maximum tensile strength and ductility of aluminum(8011) silicon carbide particulate composites.The process parameters are solutionizing time,aging temperature,and aging time.The experiments were performed on an universal testing machine according to centre rotatable design matrix.A mathematical model was developed with the main and interactive effects of the parameters considered.The analysis of variance technique was used to check the adequacy of the developed model.The optimum parameters were obtained for maximum tensile strength.Fractographic examination shows the cracks and dimples on the fractured surfaces of heat-treated specimen. 展开更多
关键词 热处理工艺优化 颗粒复合材料 响应曲面法 拉伸性能 金属基体 万能试验机 开发模型
在线阅读 下载PDF
Optimal design of butterfly-shaped linear ultrasonic motor using finite element method and response surface methodology 被引量:9
3
作者 时运来 陈超 赵淳生 《Journal of Central South University》 SCIE EI CAS 2013年第2期393-404,共12页
A new method for optimizing a butterfly-shaped linear ultrasonic motor was proposed to maximize its mechanical output. The finite element analysis technology and response surface methodology were combined together to ... A new method for optimizing a butterfly-shaped linear ultrasonic motor was proposed to maximize its mechanical output. The finite element analysis technology and response surface methodology were combined together to realize the optimal design of the butterfly-shaped linear ultrasonic motor. First, the operation principle of the motor was introduced. Second, the finite element parameterized model of the stator of the motor was built using ANSYS parametric design language and some structure parameters of the stator were selected as design variables. Third, the sample points were selected in design variable space using latin hypercube Design. Through modal analysis and harmonic response analysis of the stator based on these sample points, the target responses were obtained. These sample points and response values were combined together to build a response surface model. Finally, the simplex method was used to find the optimal solution. The experimental results showed that many aspects of the design requirements of the butterfly-shaped linear ultrasonic motor have been fulfilled. The prototype motor fabricated based on the optimal design result exhibited considerably high dynamic performance, such as no-load speed of 873 ram/s, maximal thrust of 27.5 N, maximal efficiency of 43%, and thrust-weight ratio of 45.8. 展开更多
关键词 linear ultrasonic motor PIEZOELECTRIC optimal design response surface methodology finite element method
在线阅读 下载PDF
Response surface methodology-based hybrid robust design optimization for complex product under mixed uncertainties 被引量:1
4
作者 WAN Liangqi CHEN Hongzhuan OUYANG Linhan 《Journal of Systems Engineering and Electronics》 SCIE EI CSCD 2019年第2期308-318,共11页
Minimizing the impact of the mixed uncertainties(i.e.,the aleatory uncertainty and the epistemic uncertainty) for a complex product of compliant mechanism(CPCM) quality improvement signifies a fascinating research top... Minimizing the impact of the mixed uncertainties(i.e.,the aleatory uncertainty and the epistemic uncertainty) for a complex product of compliant mechanism(CPCM) quality improvement signifies a fascinating research topic to enhance the robustness.However, most of the existing works in the CPCM robust design optimization neglect the mixed uncertainties, which might result in an unstable design or even an infeasible design. To solve this issue, a response surface methodology-based hybrid robust design optimization(RSM-based HRDO) approach is proposed to improve the robustness of the quality characteristic for the CPCM via considering the mixed uncertainties in the robust design optimization. A bridge-type amplification mechanism is used to manifest the effectiveness of the proposed approach. The comparison results prove that the proposed approach can not only keep its superiority in the robustness, but also provide a robust scheme for optimizing the design parameters. 展开更多
关键词 response surface methodology (RSM) HYBRID robust design optimization (HRDO) uncertainty complex product of compliant mechanism (CPCM)
在线阅读 下载PDF
Deformation prediction and analysis of underground mining during stacking of dry gangue in open-pit based on response surface methodology 被引量:6
5
作者 QIU Xian-yang CHEN Jia-yao +3 位作者 SHI Xiu-zhi ZHANG Shu ZHOU Jian CHEN Xin 《Journal of Central South University》 SCIE EI CAS CSCD 2018年第2期406-417,共12页
Deformation prediction and the analysis of underground goaf are important to the safe and efficient recovery of residual ore when shifting from open-pit mining to underground mining.To address the comprehensive proble... Deformation prediction and the analysis of underground goaf are important to the safe and efficient recovery of residual ore when shifting from open-pit mining to underground mining.To address the comprehensive problem of stability in the double mined-out area of the Tong-Lv-Shan(TLS)mine,which employed the dry stacked gangue technology,this paper applies the function fitting theory and a regression analysis method to screen the sensitive interval of four influencing factors based on single-factor experiments and the numerical simulation software FLAC3D.The influencing factors of the TLS mine consist of the column thickness(d),gob area span(D),boundary pillar thickness(h)and height of tailing gangue(H).The fitting degree between the four factors and the displacement of the gob roof(W)is reasonable because the correlation coefficient(R2)is greater than0.9701.After establishing29groups that satisfy the principles of Box-Behnken design(BBD),the dry gangue tailings process was re-simulated for the selected sensitive interval.Using a combination of an analysis of variance(ANOVA),regression equations and a significance analysis,the prediction results of the response surface methodology(RSM)show that the significant degree for the stability of the mined-out area for the factors satisfies the relationship of h>D>d>H.The importance of the four factors cannot be disregarded in a comparison of the prediction results of the engineering test stope in the TLS mine.By comparing the data of monitoring points and function prediction,the proposed method has shown promising results,and the prediction accuracy of RSM model is acceptable.The relative errors of the two test stopes are1.67%and3.85%,respectively,which yield satisfactory reliability and reference values for the mines. 展开更多
关键词 response surface methodology (RSM) Box-Behnken design (BBD) numerical simulation boundary pillar deformation prediction
在线阅读 下载PDF
Multiple-response optimization for melting process of aluminum melting furnace based on response surface methodology with desirability function 被引量:3
6
作者 周孑民 王计敏 +2 位作者 闫红杰 李世轩 贵广臣 《Journal of Central South University》 SCIE EI CAS 2012年第10期2875-2885,共11页
To reduce the fuel consumption and emissions and also enhance the molten aluminum quality, a mathematical model with user-developed melting model and burning capacity model, were established according to the features ... To reduce the fuel consumption and emissions and also enhance the molten aluminum quality, a mathematical model with user-developed melting model and burning capacity model, were established according to the features of melting process of regenerative aluminum melting furnaces. Based on validating results by heat balance test for an aluminum melting furnace, CFD (computational fluid dynamics) technique, in association with statistical experimental design were used to optimize the melting process of the aluminum melting furnace. Four important factors influencing the melting time, such as horizontal angle between burners, height-to-radius ratio, natural gas mass flow and air preheated temperature, were identified by PLACKETT-BURMAN design. A steepest descent method was undertaken to determine the optimal regions of these factors. Response surface methodology with BOX-BEHNKEN design was adopted to further investigate the mutual interactions between these variables on RSD (relative standard deviation) of aluminum temperature, RSD of furnace temperature and melting time. Multiple-response optimization by desirability function approach was used to determine the optimum melting process parameters. The results indicate that the interaction between the height-to-radius ratio and horizontal angle between burners affects the response variables significantly. The predicted results show that the minimum RSD of aluminum temperature (12.13%), RSD of furnace temperature (18.50%) and melting time (3.9 h) could be obtained under the optimum conditions of horizontal angle between burners as 64°, height-to-radius ratio as 0.3, natural gas mass flow as 599 m3/h, and air preheated temperature as 639 ℃. These predicted values were further verified by validation experiments. The excellent correlation between the predicted and experimental values confirms the validity and practicability of this statistical optimum strategy. 展开更多
关键词 aluminum melting furnace melting process response surface methodology desirability function multiple response parameter optimization numerical simulation PLACKETT-BURMAN design BOX-BEHNKEN design
在线阅读 下载PDF
Optimization of Supercritical Fluid Extraction of Tea Flower Polysaccharides by Using Response Surface Method 被引量:1
7
作者 Xing-Hai Zhang Fei Que +2 位作者 Jin-Wei Xu Pei-Li Yu You-Ying Tu 《茶叶》 2013年第4期442-451,共10页
Polysaccharide production from tea flower(TFPS) was carried out using supercritical fluid extraction(SFE).Response surface methodology(RSM),based on a five level,four variable small central composite design,was employ... Polysaccharide production from tea flower(TFPS) was carried out using supercritical fluid extraction(SFE).Response surface methodology(RSM),based on a five level,four variable small central composite design,was employed to obtain the best possible combination of extraction time,pressure,temperature and ethanol content of modifier for maximum production.The optimum conditions were as follows:extraction time of 170 min,pressure of45 MPa,temperature of 75 ℃,and 50% aqueous ethanol solution as modifier.Under these conditions,the experimental yield was 6.56 ± 0.37%,which was similar to the value predicted by the model.Monosaccharide composition of TFPS was fucose,rhamnose,arabinose,xylose,galactose,glucose,mannose,fructose,ribose,galacturonic acid and glucuronic acid in a molar percent of 31.69,0.21,0.49,1.29,35.82,0.97,1.63,18.34,7.88,1.06 and 0.63.Compared to other extraction methods,SFE could achieve higher yield and gain more types of monosaccharide. 展开更多
关键词 超临界流体萃取 茶多糖 响应曲面法 葡萄糖醛酸 半乳糖醛酸 优化 花卉 中心复合设计
在线阅读 下载PDF
Age hardening process modeling and optimization of aluminum alloy A356/Cow horn particulate composite for brake drum application using RSM,ANN and simulated annealing
8
作者 Chidozie Chukwuemeka Nwobi-Okoye Basil Quent Ochieze 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2018年第4期336-345,共10页
Most conventional ceramic based aluminum metal matrix composites(MMCs) are either heavy,costly or combination of both. In order to reduce cost and weight,while at the same time maintaining quality,cow horn particles(C... Most conventional ceramic based aluminum metal matrix composites(MMCs) are either heavy,costly or combination of both. In order to reduce cost and weight,while at the same time maintaining quality,cow horn particles(CHp) was used with aluminum alloy A356 to produce MMC for brake drum application and other engineering uses. The aim of this research is to model the age hardening process of the produced composite using response surface methodology(RSM) and artificial neural network(ANN),and to use the developed ANN as fitness function for a simulated annealing optimization algorithm(SA-NN system) for optimization of age hardening process parameters. The results show that ANN modeled the age hardening data excellently and better than RSM with a correlation coefficient of experimental response with ANN predictions being 0.9921 as against 0.9583 for the RSM. The SA-NN system optimized process parameters were in very close agreement with the experimental values with the maximum relative error of 1.2%,minimum of 0.35% and average of 0.71%. 展开更多
关键词 Artificial neural network response surface methodology Simulated ANNEALING Age HARDENING Metal matrix composite
在线阅读 下载PDF
原子吸收光谱法测定矿石中Au的分析技术及最优化模型研究
9
作者 王鹏 门倩妮 +7 位作者 甘黎明 白金峰 王啸 井斌强 寇少磊 刘慧蓝 何涛 刘玖芬 《光谱学与光谱分析》 北大核心 2025年第2期426-433,共8页
矿石中Au通常以颗粒金或者晶格金的形式存在,在不同类型的金矿石中赋存状态不同,其特殊的延展性引起的颗粒效应对于Au样品的分析技术带来挑战,并且其制备流程要素繁多且不易控制,直接影响Au分析的准确性和稳定性。以矿石中金元素为研究... 矿石中Au通常以颗粒金或者晶格金的形式存在,在不同类型的金矿石中赋存状态不同,其特殊的延展性引起的颗粒效应对于Au样品的分析技术带来挑战,并且其制备流程要素繁多且不易控制,直接影响Au分析的准确性和稳定性。以矿石中金元素为研究对象,建立泡塑吸附-原子吸收光谱法测定矿石中Au的分析方法,针对样品测试流程中的关键要素进行定性判断和定量计算,提出基于灰色关联度-响应曲面法的最优化模型。讨论样品分析技术中焙烧、消解、富集和解脱等重要环节,确定焙烧方式、消解酸度、富集时间和硫脲浓度为优化要素,设计正交试验并进行相关性分析,计算灰色关联系数并进行极差确定,定性判断各优化要素的显著性。中心组合设计结合响应曲面法原理制作显著水平表,建立二次多项式回归方程的预测模型并进行显著性分析,绘制三维响应曲面图和二维等高线图对实验数据进行拟合分析,确定最优化模型参数焙烧方式、消解酸度、富集时间和硫脲浓度分别为阶梯式分段焙烧、10.58%、40.00 min、11.65 g·L^(-1)。实验结果表明,在最优化模型条件下对金矿石国家一级标准物质进行制备测试,其方法检出限为0.021,测定下限为0.077,加标回收率为91.6%~104.5%,其正确度和精密度均符合GB/T 20899.2—2019质量控制要求;同时对陕西西秦岭地区和甘肃梅川地区外检样品进行方法验证比对,其相对偏差不超过10%且评价结果均为优秀,表明该检测优化模型方法在实际样品中的应用依然准确可靠,具备正确性和科学性。该研究对于地质矿产实验室快速、准确、简便分析Au元素提出新方法,为检验检测领域中优化多目标参数组合的课题提供了新的思路,同时为新一轮战略找矿行动的准确测试贡献力量。 展开更多
关键词 原子吸收光谱法 灰色关联度 响应曲面法 中心组合设计 质量控制
在线阅读 下载PDF
基于瞬态流场分析的小排量潜油螺杆泵的结构优化设计
10
作者 祖海英 付灵芝 +2 位作者 叶卫东 刘永鹏 张维良 《流体机械》 北大核心 2025年第6期58-66,共9页
针对小排量潜油螺杆泵因泄漏量大导致容积效率低的问题,以GLB-20型螺杆泵为研究对象,借助Ansys Fluent软件,基于用户自定义函数(UDF)和动网格技术构建流体仿真模型,对小排量潜油螺杆泵的瞬态与稳态流场进行模拟;探究偏心距、定子导程、... 针对小排量潜油螺杆泵因泄漏量大导致容积效率低的问题,以GLB-20型螺杆泵为研究对象,借助Ansys Fluent软件,基于用户自定义函数(UDF)和动网格技术构建流体仿真模型,对小排量潜油螺杆泵的瞬态与稳态流场进行模拟;探究偏心距、定子导程、间隙等结构参数对流场流速及泄漏量的影响规律,并通过试验验证优化结果,获得螺杆泵结构的最优设计方案。结果表明,螺杆泵运行时呈现显著的谐波变化特性,流量在单个周期内出现2次脉动,与定转子导程比值一致;瞬态流场较稳态流场更贴合实际工况;间隙是影响泄漏量和流场流速的最关键因素,其中定子导程对流场流速的影响程度大于偏心距,而偏心距对泄漏量的影响程度大于定子导程。采用Box-Behnken设计法(BBD)优化后的螺杆泵结构参数:偏心距1.8 mm、定子导程78 mm、间隙0.3 mm,泄漏量较优化前减少12.7%,容积效率显著提升且流动稳定性增强。该研究成果可为小排量潜油螺杆泵的开发与应用提供设计依据和参考。 展开更多
关键词 小排量潜油螺杆泵 瞬态流场 用户自定义函数(UDF) BBD响应面法 结构优化设计
在线阅读 下载PDF
基于响应面法的某粉质黏土深基坑土钉参数分析与优化
11
作者 樊成 王子源 +2 位作者 祁鹏飞 张宏斌 张条条 《长江科学院院报》 北大核心 2025年第4期142-148,158,共8页
为揭示土钉设计中空间形态参数等因素对粉质黏土深基坑三维稳定性的影响规律,以河北某粉质黏土地区深基坑为工程背景,基于响应面法设计Plackett-Burman与Box-Behnken试验,采用MIDAS-GTS与Design-Expert软件建立试验模型。通过数值模拟... 为揭示土钉设计中空间形态参数等因素对粉质黏土深基坑三维稳定性的影响规律,以河北某粉质黏土地区深基坑为工程背景,基于响应面法设计Plackett-Burman与Box-Behnken试验,采用MIDAS-GTS与Design-Expert软件建立试验模型。通过数值模拟与监测数据分析了各参数对粉质黏土深基坑土钉支护安全性的影响规律及优化方案的适用性。结果表明:各参数对粉质黏土地区基坑支护稳定性的影响程度从大到小依次为土钉长度、放坡坡角、土钉间距、土钉倾角、土钉直径。在支护参数的组合作用中,土钉长度与土钉间距对安全系数的影响最大。利用响应面法建立的预测模型能够提供最佳的优化方案,优化方案使土体滑移面后移,基坑的最大水平位移由9.33 mm减至5.42 mm,最大竖直沉降由16.9 mm减至11.8 mm,为该类型基坑土钉支护设计提供了参考。 展开更多
关键词 基坑 土钉支护 响应面法 MIDAS-GTS 优化设计
在线阅读 下载PDF
基于BP-ANN的人工渗滤系统去除总磷过程优化
12
作者 刘元坤 曹塬琪 +2 位作者 于艾鑫 李星 郭晓天 《中国环境科学》 北大核心 2025年第6期3151-3160,共10页
本文利用BBD响应面法(BBD-RSM)和反向传播人工神经网络(BP-ANN)算法对活性炭吸附总磷(TP)的过程参数(接触时间、初始浓度、温度、pH值)进行了建模和预测,并结合遗传算法(GA)对BP-ANN模型中的反应条件进行优化.结果表明,在BBD-RSM模型中,... 本文利用BBD响应面法(BBD-RSM)和反向传播人工神经网络(BP-ANN)算法对活性炭吸附总磷(TP)的过程参数(接触时间、初始浓度、温度、pH值)进行了建模和预测,并结合遗传算法(GA)对BP-ANN模型中的反应条件进行优化.结果表明,在BBD-RSM模型中,P<0.0001,可较好的对TP的去除过程进行预测,接触时间为TP去除率最显著的参数,TP吸附过程中各因素的相对影响顺序为:接触时间>pH值>温度>初始浓度.采用BP-ANN模型进行优化,最佳网络结构为4-8-1.敏感性分析表明,影响TP去除率的因素依次为接触时间(34.05%)>pH值(28.67%)>温度(19.56%)>初始浓度(17.72%).基于BP-ANN模型,采用GA优化人工渗滤系统运行条件,对TP去除过程的优化结果为:接触时间为720.53min、初始浓度为2.75mg/L、温度为30.62℃、pH为5,达到最佳去除率(99.63%).试验验证分析表明,BP-ANN-GA较BBD-RSM的预测值与实验值相比拥有较高的R 2(0.9939)和较低的RSME(1.2851),说明该模型具有更好的预测能力,能更好的描述人工快速渗滤系统对TP的去除过程. 展开更多
关键词 BBD响应面法 反向传播人工神经网络 遗传算法 总磷 人工快速渗滤系统
在线阅读 下载PDF
复方麝香黄芪滴丸成型工艺优选及挥发性成分含量测定 被引量:1
13
作者 邵梦迪 张舒彦 +4 位作者 郑淇 常春辉 李家豪 张运克 贾永艳 《医药导报》 CAS 北大核心 2025年第1期88-95,共8页
目的优选复方麝香黄芪滴丸成型工艺,并完善该复方的质量标准。方法通过单因素实验筛选复方麝香黄芪滴丸的基质种类、基质和药液比例、滴距的最佳考察范围;以外观性状、丸重差异、溶散时限等作为评价指标,采用星点设计-效应面法优选复方... 目的优选复方麝香黄芪滴丸成型工艺,并完善该复方的质量标准。方法通过单因素实验筛选复方麝香黄芪滴丸的基质种类、基质和药液比例、滴距的最佳考察范围;以外观性状、丸重差异、溶散时限等作为评价指标,采用星点设计-效应面法优选复方麝香黄芪滴丸最佳成型工艺条件;以3批复方麝香黄芪滴丸为检测样品,采用气相色谱法测定龙脑、麝香酮和藁本内酯含量;色谱柱为HP-5石英毛细管柱,进样口温度260℃,程序升温,检测器温度300℃,分流比10:1,载气为氮气,流速为1.0 mL·min^(-1)。结果复方麝香黄芪滴丸的最佳成型工艺条件为基质:基质=0.99、药物:基质=0.55、滴距=6.00,综合评分为0.8452;龙脑、麝香酮和藁本内酯与相邻成分色谱峰均达到基线分离;3种成分的线性范围依次为0.327~1.962、0.140~0.840、0.7105~4.263μg(均r>0.999);平均加样回收率依次为92.30%(RSD=1.65%,n=6)、101.28%(RSD=0.81%,n=6)、98.99%(RSD=0.65%,n=6);3种成分的平均含量依次为0.2017、0.0847、1.3829 mg·g^(-1)。结论该成型工艺稳定可行,可为复方麝香黄芪滴丸的开发及应用提供参考;建立的气相色谱法能同时测定复方麝香黄芪滴丸中龙脑、麝香酮和藁本内酯的含量,可用于复方麝香黄芪滴丸的质量控制。 展开更多
关键词 复方麝香黄芪滴丸 星点设计-效应面法 成型工艺 气相色谱法 含量测定
在线阅读 下载PDF
碳基复合材料用作电芬顿阴极处理垃圾渗滤液的效果研究 被引量:1
14
作者 魏一恺 杨俊 +3 位作者 武梦杰 周欣然 游自强 王趁义 《环境污染与防治》 北大核心 2025年第1期42-48,58,共8页
针对目前电芬顿复合电极原料昂贵及制备工艺复杂等问题,以活性炭和Fe_(3)O_(4)为基础原料,以钛网、不锈钢网、铁网为导电基底制备3种碳基复合阴极材料(CEM),分别记为TBT、SSBT、IBT。通过单因素试验筛选CEM的最佳制备条件,选取性能最优... 针对目前电芬顿复合电极原料昂贵及制备工艺复杂等问题,以活性炭和Fe_(3)O_(4)为基础原料,以钛网、不锈钢网、铁网为导电基底制备3种碳基复合阴极材料(CEM),分别记为TBT、SSBT、IBT。通过单因素试验筛选CEM的最佳制备条件,选取性能最优的CEM用于电芬顿处理垃圾渗滤液,用响应面法得到电芬顿处理的初始pH、外接电压、Fe^(2+)投加量与COD去除率之间的二次多项式模型,优化电芬顿的运行条件。结果表明:3种CEM材料中SSBT的性能最优,其最佳制备条件为黏结剂(Na_(2)SiO_(3)·9H_(2)O)∶基础原料的质量比为4∶10,基础原料中Fe_(3)O_(4)的掺杂量为2%(质量分数),煅烧温度为600℃;SSBT用于电芬顿处理垃圾渗滤液的最佳运行条件为初始pH 2.6,外接电压10.08 V,Fe^(2+)投加量0.47 mmol/L,在此条件下COD的去除率的实测值与预测值分别为86.10%和86.41%,平均绝对误差为0.36%,说明模型模拟结果符合实际;SSBT表面三维结构丰富,Fe_(3)O_(4)在材料中稳定负载,经15次重复性测试,SSBT的COD去除率仅下降7.81百分点,表明其具有良好的稳定性。研究结果可为电芬顿CEM材料的设计和运行条件的优化提供参考。 展开更多
关键词 电芬顿 碳基复合阴极 制备与表征 垃圾渗滤液 响应面法
在线阅读 下载PDF
基于UPLC-Q-TOF-MS/MS结合响应面法与主成分分析优化肠炎合剂Ⅱ提取工艺
15
作者 汪树林 商晶 +6 位作者 刘文君 蔡泽荣 钱梦雨 胡晓欣 曹亮 王振中 肖伟 《南京中医药大学学报》 北大核心 2025年第4期501-512,共12页
目的基于UPLC-Q-TOF-MS/MS技术结合响应面分析构建肠炎合剂Ⅱ提取工艺方法,并对其提取工艺进行优化。方法通过UPLC-Q-TOF-MS/MS技术对肠炎合剂Ⅱ中化学成分进行定性分析,并挑选出质谱响应度有较好线性关系的化学成分为工艺考察指标;利用... 目的基于UPLC-Q-TOF-MS/MS技术结合响应面分析构建肠炎合剂Ⅱ提取工艺方法,并对其提取工艺进行优化。方法通过UPLC-Q-TOF-MS/MS技术对肠炎合剂Ⅱ中化学成分进行定性分析,并挑选出质谱响应度有较好线性关系的化学成分为工艺考察指标;利用Box-Behnken设计对提取工艺参数(加水量、提取时间及浸泡时间)进行考察;通过主成分分析(Principal component analysis,PCA)得到综合评分,并以综合得分结合响应面分析确定最优工艺。结果通过定性分析从肠炎合剂Ⅱ中推测和鉴定了110个成分,包括有机酸2种、黄酮类82种、萜类化合物13种、生物碱类13种,基于定性分析结果,通过UPLC-Q-TOF-MS/MS结合Masshunter质谱数据分析软件导出48个具有良好线性关系的指标成分质谱响应度,进行PCA并计算综合得分,以综合得分为指标进行响应面分析,综合响应面预测结果及生产实际得到的最优提取工艺为:浸泡45 min,溶剂倍量8倍,提取2次,每次120 min。结论为中药复方提取工艺的考察提供了一种新思路,为中药复方开发拓展一种新方法。 展开更多
关键词 提取工艺 Box-Behnken设计-响应面法 主成分分析 葛根素 甘草酸 木香烃内酯 芍药苷
在线阅读 下载PDF
以参苓咀嚼片提取工艺探究中心组合响应面法与正交试验法的区别
16
作者 吴承潮 陆丽蓉 +4 位作者 钟绍辉 鲁方奇 郑云枫 刘陶世 程建明 《世界中医药》 北大核心 2025年第5期711-717,725,共8页
目的:分别应用中心组合设计-响应面法与正交试验,结合层次分析法(AHP)-熵权法(EWM)优化中药复方的提取工艺,为中药提取试验方法的优选提供依据。方法:以葛根素、橙皮苷、甘草苷转移率及复方出膏率的综合评分为响应值,以加水倍数、提取... 目的:分别应用中心组合设计-响应面法与正交试验,结合层次分析法(AHP)-熵权法(EWM)优化中药复方的提取工艺,为中药提取试验方法的优选提供依据。方法:以葛根素、橙皮苷、甘草苷转移率及复方出膏率的综合评分为响应值,以加水倍数、提取时间、提取次数为关键工艺参数,采用AHP-EWM法确定各种评价指标的权重系数,并进行综合评分,以中心组合响应面法及正交试验分别设计优化提取工艺参数,并进行验证与比较。结果:以参苓咀嚼片的提取工艺为例,分别采取正交试验法与响应面法得出的最佳工艺不同,但3批验证实验相对标准差(RSD)均小于3.0%,综合评分接近各自试验预测值。结论:响应面法工艺优选设计相对精细,但重复性和可操作性好,较正交试验更精细,更适合参苓咀嚼片的生产实际提取。 展开更多
关键词 参苓咀嚼片 功能性食品 提取工艺优选 高效液相色谱法 层次分析法-信息熵权重法 中心组合-响应面法 正交试验法 生产实际
在线阅读 下载PDF
响应面法优化e-PTFE膜层压复合织物的热压工艺
17
作者 宋丽伟 金肖克 +3 位作者 缪永达 刘鑫宇 祝成炎 田伟 《现代纺织技术》 北大核心 2025年第4期33-42,共10页
选取聚酰胺共聚物(PA)热熔胶网膜作为黏合剂,通过改变热压工艺中热压时间、温度、压强和上胶量4个工艺参数,制备不同参数的膨体聚四氟乙烯(e-PTFE)膜层压复合织物,并在单因素的基础上通过Box-Behnken响应面法分析不同e-PTFE膜层压复合... 选取聚酰胺共聚物(PA)热熔胶网膜作为黏合剂,通过改变热压工艺中热压时间、温度、压强和上胶量4个工艺参数,制备不同参数的膨体聚四氟乙烯(e-PTFE)膜层压复合织物,并在单因素的基础上通过Box-Behnken响应面法分析不同e-PTFE膜层压复合织物的防风性、透湿性以及剥离强力,得出最优热压工艺。结果表明:制备e-PTFE膜层压复合织物的最优热压工艺为热压时间15 s、热压温度150℃、热压压强0.5 MPa、上胶量10 g/m^(2)。在该工艺条件下得到的e-PTFE膜层压复合织物的剥离强力为2.63 N、透气率为1.96 mm/s、透湿量为5670.60 g/(m^(2)·24h)。研究结果发现,采用的Box-Behnken响应面法得出的最优热压工艺结果更加准确,且制备的层压复合织物与原织物相比防风性和透湿性均有所改善,可为后续制备热湿管理织物提供研究思路。 展开更多
关键词 Box-Behnken响应面法 膨体聚四氟乙烯(e-PTFE)膜 层压复合织物 热压工艺 剥离强力
在线阅读 下载PDF
层次分析-熵权法结合中心复合设计-响应面法优选高乌头根酒蒸工艺研究
18
作者 马佳荣 王玉辉 +2 位作者 李莉 赵敏 李芸 《天然产物研究与开发》 北大核心 2025年第4期723-731,共9页
探究酒蒸高乌头根的最佳炮制工艺。本研究以总生物碱、高乌甲素及冉乌头碱含量的综合评分作为评价指标,采用紫外分光光度法测定总生物碱含量,超高效液相色谱法测定高乌甲素和冉乌头碱含量。为探究加黄酒量、闷润时间、蒸制时间对酒蒸高... 探究酒蒸高乌头根的最佳炮制工艺。本研究以总生物碱、高乌甲素及冉乌头碱含量的综合评分作为评价指标,采用紫外分光光度法测定总生物碱含量,超高效液相色谱法测定高乌甲素和冉乌头碱含量。为探究加黄酒量、闷润时间、蒸制时间对酒蒸高乌头根炮制工艺的影响,开展了单因素考察试验。采用层次分析-熵权法确定总生物碱、高乌甲素、冉乌头碱含量的权重,以三者的综合评分结合中心复合设计-响应面法确定酒蒸高乌头根的最佳炮制工艺。结果表明酒蒸高乌头根的最佳炮制工艺为:高乌头根重量15%的加酒量、闷润时间2 h、蒸制时间5 h、蒸制温度127℃、蒸制压力0.15 MPa。本研究拓宽了高乌头根炮制方法且所建立的炮制工艺评价体系准确、可信,为高乌头根炮制相关研究及临床安全提供参考。 展开更多
关键词 层次分析-熵权法 中心复合设计-响应面法 酒蒸高乌头根 总生物碱 高乌甲素 冉乌头碱
在线阅读 下载PDF
Box-Behnken Design-响应面法优化绿原酸转化为新绿原酸的工艺研究 被引量:2
19
作者 温建辉 倪付勇 +4 位作者 王雪晶 李明 宋亚玲 王振中 萧伟 《世界科学技术-中医药现代化》 CSCD 2017年第7期1239-1244,共6页
利用Box-Behnken-响应面法优化绿原酸转化为新绿原酸的工艺条件。在单因素实验基础上,采用Box-Behnken Design实验设计,考察反应温度、反应时间及p H值对新绿原酸产率的影响,优化绿原酸转化为新绿原酸的工艺参数,得到模型预测公式。优... 利用Box-Behnken-响应面法优化绿原酸转化为新绿原酸的工艺条件。在单因素实验基础上,采用Box-Behnken Design实验设计,考察反应温度、反应时间及p H值对新绿原酸产率的影响,优化绿原酸转化为新绿原酸的工艺参数,得到模型预测公式。优化条件为:反应温度107℃,反应时间60 min,p H值为4.72时新绿原酸产率为64.20%,与模型预测值接近,方程拟合良好。采用优选工艺制备新绿原酸并精制纯化,分别运用HPLC、1H-NMR、13C-NMR、ESI-MS等方法对其进行含量测定和结构表征,结果表明纯化后纯度达98.78%,收率为87.37%。 展开更多
关键词 绿原酸 新绿原酸 Box-Behnken design响应面法 结构鉴定
在线阅读 下载PDF
五指毛桃盐卤鸡制作工艺的优化
20
作者 李哲峰 王文娟 +1 位作者 梁洪玮 杨铭铎 《中国调味品》 北大核心 2025年第7期174-179,共6页
五指毛桃盐卤鸡不仅具有独特的风味,而且能起到健脾补肺的作用。为提高五指毛桃盐卤鸡的品质,先采用星点设计-响应面法优化卤水制作工艺参数,然后采用Box-Behnken设计优化五指毛桃盐卤鸡的卤制工艺参数。结果表明,以1250 g鸡肉为基准,... 五指毛桃盐卤鸡不仅具有独特的风味,而且能起到健脾补肺的作用。为提高五指毛桃盐卤鸡的品质,先采用星点设计-响应面法优化卤水制作工艺参数,然后采用Box-Behnken设计优化五指毛桃盐卤鸡的卤制工艺参数。结果表明,以1250 g鸡肉为基准,将五指毛桃和香辛料以17倍水浸提,在微沸条件下熬煮90 min,过滤后添加5%食用盐溶解,制得卤水,然后将鸡肉浸入卤水中,在微沸条件下卤制30 min,关火后继续浸卤40 min,此条件下所制作的五指毛桃盐卤鸡的口感、滋味最佳。 展开更多
关键词 五指毛桃盐卤鸡 星点设计-响应面法 卤水制作工艺 Box-Behnken试验 盐卤鸡制作工艺
在线阅读 下载PDF
上一页 1 2 43 下一页 到第
使用帮助 返回顶部