In order to improve the quality of 3D printed raspberry preserves after post-processing,microwave ovens combining infrared and microwave methods were utilized.The effects of infrared heating temperature,infrared heati...In order to improve the quality of 3D printed raspberry preserves after post-processing,microwave ovens combining infrared and microwave methods were utilized.The effects of infrared heating temperature,infrared heating time,microwave power,microwave heating time on the center temperature,moisture content,the chroma(C*),the total color difference(ΔE*),shape fidelity,hardness,and the total anthocyanin content of 3D printed raspberry preserves were analyzed by response surface method(RSM).The results showed that under combining with the two methods,infrared heating improved the fidelity and quality degradation of printed products,while microwave heating enhanced the efficiency of infrared heating.Infrared-microwave combination cooking could maintain relatively stable color appearance and shape of 3D printed raspberry preserves.The AHP–CRITIC hybrid weighting method combined with the response surface test to determine the comprehensive weights of the evaluation indicators optimized the process parameters,and the optimal process parameters were obtained:infrared heating temperature of 190℃,infrared heating time of 10 min and 30 s,microwave power of 300 W,and microwave heating time of 2 min and 6 s.The 3D printed raspberry cooking methods obtained under the optimal conditions seldom had color variation,porous structure,uniform texture,and high shape fidelity,which retained the characteristics of personalized manufacturing by 3D printing.This study could provide a reference for the postprocessing and quality control of 3D cooking methods.展开更多
Due to their high hardness and high strength,VC reinforced hard materials such as high vanadium high-speed steel(HVHSS)are not suitable for machining to obtain complex shape with low cost.Therefore,3D gel printing(3DG...Due to their high hardness and high strength,VC reinforced hard materials such as high vanadium high-speed steel(HVHSS)are not suitable for machining to obtain complex shape with low cost.Therefore,3D gel printing(3DGP)was employed to print HVHSS parts,using highly loaded slurry with 60%solid content as printing slurry.After printing parameters optimization,the printing sample had good surface quality,and obvious printing lines were observed.The extruded filament was in-situ cured,thus enough to maintain the designed shape.Uniform sintering shrinkage with a shrinkage rate of about 15%was obtained in the as-sintered sample with relative density of 99%.The surface roughness decreased from 6.5μm to 3.8μm.Fine carbides(<1μm)and dense microstructure were achieved.Besides,the as-sintered sample had comprehensive performance of HRC60 in hardness,3000 MPa in bend strength,and 20−26 J in impact energy.This study proposed one promising method to directly manufacture complex-shaped hard materials without subsequent machining.展开更多
A direct 3D extrusion printing technique was used to produce Ti-TiB filaments and microlattices.The sintering properties of 3D ink extrusion and sintering of in situ Ti-TiB composite structures made from TiH_(2)+TiB_(...A direct 3D extrusion printing technique was used to produce Ti-TiB filaments and microlattices.The sintering properties of 3D ink extrusion and sintering of in situ Ti-TiB composite structures made from TiH_(2)+TiB_(2) ink were investigated.The sintering kinetics of TiH2+TiB2 inks was studied during densification by pressureless sintering at 1050−1200℃ for 4−24 h in Ar.The linear shrinkage,grain size,microhardness,X-ray diffraction(XRD)patterns,and microstructural evolution of the Ti-TiB composite were studied.The sintering temperature had a more pronounced influence than the sintering time on the density of the Ti-TiB composite.There were two kinds of pores,irregular and spherical,caused by the Kirkendall effect and indiffusable gases.The TiB formed by in situ synthesis existed as either separated TiB whiskers(needle-like shapes)or clusters of TiB whiskers.The results of this work could be useful for controlling microporosity through incomplete sintering within filaments,especially for the production of in situ Ti-TiB with high volume fractions of TiB or other composites.展开更多
In practical engineering applications,rock mass are often found to be subjected to a triaxial stress state.Concurrently,defects like joints and fractures have a notable impact on the mechanical behavior of rock mass.S...In practical engineering applications,rock mass are often found to be subjected to a triaxial stress state.Concurrently,defects like joints and fractures have a notable impact on the mechanical behavior of rock mass.Such defects are identified as crucial contributors to the failure and instability of the surrounding rock,subsequently impacting the engineering stability.The study aimed to investigate the impact of fracture geometry and confining pressure on the deformation,failure characteristics,and strength of specimens using sand powder 3D printing technology and conventional triaxial compression tests.The results indicate that the number of fractures present considerably influences the peak strength,axial peak strain and elastic modulus of the specimens.Confining pressure is an important factor affecting the failure pattern of the specimen,under which the specimen is more prone to shear failure,but the initiation,expansion and penetration processes of secondary cracks in different fracture specimens are different.This study confirmed the feasibility of using sand powder 3D printing specimens as soft rock analogs for triaxial compression research.The insights from this research are deemed essential for a deeper understanding of the mechanical behavior of fractured surrounding rocks when under triaxial stress state.展开更多
In order to obtain better quality cookies, food 3D printing technology was employed to prepare cookies. The texture, color, deformation, moisture content, and temperature of the cookie as evaluation indicators, the in...In order to obtain better quality cookies, food 3D printing technology was employed to prepare cookies. The texture, color, deformation, moisture content, and temperature of the cookie as evaluation indicators, the influences of baking process parameters, such as baking time, surface heating temperature and bottom heating temperature, on the quality of the cookie were studied to optimize the baking process parameters. The results showed that the baking process parameters had obvious effects on the texture, color, deformation, moisture content, and temperature of the cookie. All of the roasting surface heating temperature, bottom heating temperature and baking time had positive influences on the hardness, crunchiness, crispiness, and the total color difference(ΔE) of the cookie. When the heating temperatures of the surfac and bottom increased, the diameter and thickness deformation rate of the cookie increased. However,with the extension of baking time, the diameter and thickness deformation rate of the cookie first increased and then decreased. With the surface heating temperature of 180 ℃, the bottom heating temperature of 150 ℃, and baking time of 15 min, the cookie was crisp and moderate with moderate deformation and uniform color. There was no burnt phenomenon with the desired quality. Research results provided a theoretical basis for cookie manufactory based on food 3D printing technology.展开更多
3D printing technology enhances the combustion characteristics of hybrid rocket fuels by enabling complex geometries. However, improvements in regression rates and energy properties of monotonous 3D printed fuels have...3D printing technology enhances the combustion characteristics of hybrid rocket fuels by enabling complex geometries. However, improvements in regression rates and energy properties of monotonous 3D printed fuels have been limited. This study explores the impact of poly(vinylidene fluoride) and polydopamine-coated aluminum particles on the thermal and combustion properties of 3D printed hybrid rocket fuels. Physical self-assembly and anti-solvent methods were employed for constructing composite μAl particles. Characterization using SEM, XRD, XPS, FTIR, and μCT revealed a core-shell structure and homogeneous elemental distribution. Thermal analysis showed that PVDF coatings significantly increased the heat of combustion for aluminum particles, with maximum enhancement observed in μAl@PDA@PVDF(denoted as μAl@PF) at 6.20 k J/g. Subsequently, 3D printed fuels with varying pure and composite μAl particle contents were prepared using 3D printing. Combustion tests indicated higher regression rates for Al@PF/Resin composites compared to pure resin, positively correlating with particle content. The fluorocarbon-alumina reaction during the combustion stage intensified Al particle combustion, reducing residue size. A comprehensive model based on experiments provides insights into the combustion process of PDA and PVDF-coated droplets. This study advances the design of 3D-printed hybrid rocket fuels, offering strategies to improve regression rates and energy release, crucial for enhancing solid fuel performance for hybrid propulsion.展开更多
基金Supported by the National Natural Science Foundation of China(32072352)。
文摘In order to improve the quality of 3D printed raspberry preserves after post-processing,microwave ovens combining infrared and microwave methods were utilized.The effects of infrared heating temperature,infrared heating time,microwave power,microwave heating time on the center temperature,moisture content,the chroma(C*),the total color difference(ΔE*),shape fidelity,hardness,and the total anthocyanin content of 3D printed raspberry preserves were analyzed by response surface method(RSM).The results showed that under combining with the two methods,infrared heating improved the fidelity and quality degradation of printed products,while microwave heating enhanced the efficiency of infrared heating.Infrared-microwave combination cooking could maintain relatively stable color appearance and shape of 3D printed raspberry preserves.The AHP–CRITIC hybrid weighting method combined with the response surface test to determine the comprehensive weights of the evaluation indicators optimized the process parameters,and the optimal process parameters were obtained:infrared heating temperature of 190℃,infrared heating time of 10 min and 30 s,microwave power of 300 W,and microwave heating time of 2 min and 6 s.The 3D printed raspberry cooking methods obtained under the optimal conditions seldom had color variation,porous structure,uniform texture,and high shape fidelity,which retained the characteristics of personalized manufacturing by 3D printing.This study could provide a reference for the postprocessing and quality control of 3D cooking methods.
基金Projects(2019-ZD08,2020-Z17)supported by the State Key Lab of Advanced Metals and Materials,ChinaProject(52004027)supported by the National Natural Science Foundation of China+2 种基金Project(GDOE[2019]A16)supported by the Guangdong MEPP Fund,ChinaProject(311020012)supported by the Innovation Group Project of Southern Marine Science and Engineering Guangdong Laboratory(Zhuhai),ChinaProject(FRF-GF-20-05A)supported by the Fundamental Research Funds for the Central Universities,China。
文摘Due to their high hardness and high strength,VC reinforced hard materials such as high vanadium high-speed steel(HVHSS)are not suitable for machining to obtain complex shape with low cost.Therefore,3D gel printing(3DGP)was employed to print HVHSS parts,using highly loaded slurry with 60%solid content as printing slurry.After printing parameters optimization,the printing sample had good surface quality,and obvious printing lines were observed.The extruded filament was in-situ cured,thus enough to maintain the designed shape.Uniform sintering shrinkage with a shrinkage rate of about 15%was obtained in the as-sintered sample with relative density of 99%.The surface roughness decreased from 6.5μm to 3.8μm.Fine carbides(<1μm)and dense microstructure were achieved.Besides,the as-sintered sample had comprehensive performance of HRC60 in hardness,3000 MPa in bend strength,and 20−26 J in impact energy.This study proposed one promising method to directly manufacture complex-shaped hard materials without subsequent machining.
基金Project(201806920003)supported by the China Scholarship CouncilProject(172180)supported by the Swiss National Science FoundationProjects(ECCS-1542205,DMR-1720139)supported by the National Natural Science Foundation,USA。
文摘A direct 3D extrusion printing technique was used to produce Ti-TiB filaments and microlattices.The sintering properties of 3D ink extrusion and sintering of in situ Ti-TiB composite structures made from TiH_(2)+TiB_(2) ink were investigated.The sintering kinetics of TiH2+TiB2 inks was studied during densification by pressureless sintering at 1050−1200℃ for 4−24 h in Ar.The linear shrinkage,grain size,microhardness,X-ray diffraction(XRD)patterns,and microstructural evolution of the Ti-TiB composite were studied.The sintering temperature had a more pronounced influence than the sintering time on the density of the Ti-TiB composite.There were two kinds of pores,irregular and spherical,caused by the Kirkendall effect and indiffusable gases.The TiB formed by in situ synthesis existed as either separated TiB whiskers(needle-like shapes)or clusters of TiB whiskers.The results of this work could be useful for controlling microporosity through incomplete sintering within filaments,especially for the production of in situ Ti-TiB with high volume fractions of TiB or other composites.
基金Project(2021YFC2900600)supported by the Young Scientist Project of National Key Research and Development Program of ChinaProject(52074166)supported by the National Natural Science Foundation of China+1 种基金Projects(ZR2021YQ38,ZR2020QE121)supported by the Natural Science Foundation of Shandong Province,ChinaProject(2022KJ101)supported by the Science and Technology Support Plan for Youth Innovation of Colleges and Universities in Shandong Province,China。
文摘In practical engineering applications,rock mass are often found to be subjected to a triaxial stress state.Concurrently,defects like joints and fractures have a notable impact on the mechanical behavior of rock mass.Such defects are identified as crucial contributors to the failure and instability of the surrounding rock,subsequently impacting the engineering stability.The study aimed to investigate the impact of fracture geometry and confining pressure on the deformation,failure characteristics,and strength of specimens using sand powder 3D printing technology and conventional triaxial compression tests.The results indicate that the number of fractures present considerably influences the peak strength,axial peak strain and elastic modulus of the specimens.Confining pressure is an important factor affecting the failure pattern of the specimen,under which the specimen is more prone to shear failure,but the initiation,expansion and penetration processes of secondary cracks in different fracture specimens are different.This study confirmed the feasibility of using sand powder 3D printing specimens as soft rock analogs for triaxial compression research.The insights from this research are deemed essential for a deeper understanding of the mechanical behavior of fractured surrounding rocks when under triaxial stress state.
基金Supported by Heilongjiang Provincial Fruit Tree Modernization Agro-industrial Technology Collaborative Innovation and Promotion System Project(2019-13)。
文摘In order to obtain better quality cookies, food 3D printing technology was employed to prepare cookies. The texture, color, deformation, moisture content, and temperature of the cookie as evaluation indicators, the influences of baking process parameters, such as baking time, surface heating temperature and bottom heating temperature, on the quality of the cookie were studied to optimize the baking process parameters. The results showed that the baking process parameters had obvious effects on the texture, color, deformation, moisture content, and temperature of the cookie. All of the roasting surface heating temperature, bottom heating temperature and baking time had positive influences on the hardness, crunchiness, crispiness, and the total color difference(ΔE) of the cookie. When the heating temperatures of the surfac and bottom increased, the diameter and thickness deformation rate of the cookie increased. However,with the extension of baking time, the diameter and thickness deformation rate of the cookie first increased and then decreased. With the surface heating temperature of 180 ℃, the bottom heating temperature of 150 ℃, and baking time of 15 min, the cookie was crisp and moderate with moderate deformation and uniform color. There was no burnt phenomenon with the desired quality. Research results provided a theoretical basis for cookie manufactory based on food 3D printing technology.
基金funded by the National Natural Science Foundation of China(Grant No.06101213)the National Natural Science Foundation of China(Grant No.22105160).
文摘3D printing technology enhances the combustion characteristics of hybrid rocket fuels by enabling complex geometries. However, improvements in regression rates and energy properties of monotonous 3D printed fuels have been limited. This study explores the impact of poly(vinylidene fluoride) and polydopamine-coated aluminum particles on the thermal and combustion properties of 3D printed hybrid rocket fuels. Physical self-assembly and anti-solvent methods were employed for constructing composite μAl particles. Characterization using SEM, XRD, XPS, FTIR, and μCT revealed a core-shell structure and homogeneous elemental distribution. Thermal analysis showed that PVDF coatings significantly increased the heat of combustion for aluminum particles, with maximum enhancement observed in μAl@PDA@PVDF(denoted as μAl@PF) at 6.20 k J/g. Subsequently, 3D printed fuels with varying pure and composite μAl particle contents were prepared using 3D printing. Combustion tests indicated higher regression rates for Al@PF/Resin composites compared to pure resin, positively correlating with particle content. The fluorocarbon-alumina reaction during the combustion stage intensified Al particle combustion, reducing residue size. A comprehensive model based on experiments provides insights into the combustion process of PDA and PVDF-coated droplets. This study advances the design of 3D-printed hybrid rocket fuels, offering strategies to improve regression rates and energy release, crucial for enhancing solid fuel performance for hybrid propulsion.
