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基于微流控技术的可见异物标准物质制备方法研究
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作者 梁文轩 卢佳振 +1 位作者 任军 刘俊杰 《计量学报》 北大核心 2025年第8期1188-1197,共10页
为满足液体制剂可见异物分析仪的校准需求,并准确获得可见异物颗粒的测量结果,提出一种可见异物有证标准物质(certified reference materials,CRMs)的制备及定值方法。该方法通过微流控技术并结合基于YOLO-v11技术的颗粒计数模型,实现... 为满足液体制剂可见异物分析仪的校准需求,并准确获得可见异物颗粒的测量结果,提出一种可见异物有证标准物质(certified reference materials,CRMs)的制备及定值方法。该方法通过微流控技术并结合基于YOLO-v11技术的颗粒计数模型,实现对固体颗粒在微流控芯片通道中的定量输送和颗粒数的准确测量。此外,还探究了系统施加压力和悬浮液颗粒浓度对颗粒识别和计数的影响。最终,制备得到标称粒径为40、50和60μm,且颗粒数量已知的3种可见异物CRMs。与传统方法相比,该方法可以很好地控制可见异物CRMs中颗粒数量的均匀性,具有较好的技术优势和应用前景。 展开更多
关键词 颗粒计量 标准物质 可见异物 微流控技术 算法识别
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Experimental study on convection heat transfer and air drag in sinter layer 被引量:2
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作者 潘利生 魏小林 +2 位作者 彭岩 时小宝 刘怀亮 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第7期2841-2848,共8页
Convection heat transfer coefficient and air pressure drop in sinter layer are important factors for the design of sinter cooling craft. Due to the lack of necessary data, the two parameters are studied by experimenta... Convection heat transfer coefficient and air pressure drop in sinter layer are important factors for the design of sinter cooling craft. Due to the lack of necessary data, the two parameters are studied by experimental method. The experimental results show that heat conduction of sinter impacts the measurement of convection heat transfer coefficient. Convection heat transfer increases with the increase of air volumetric flow rate. Sinter layer without small particles(sample I) gives higher convection heat transfer coefficient than that with small particles(sample II). Under the considered conditions, volumetric convection heat transfer coefficient is in the range of 400-1800 W/(m3·°C). Air pressure drop in sinter layer increases with the increase of normal superficial velocity, as well as with the rise of air temperature. Additionally, air pressure drop also depends on sinter particle size distribution. In considered experimental conditions, pressure drop in sinter sample II is 2-3 times that in sinter sample I, which resulted from 17% small scale particles in sinter sample II. 展开更多
关键词 sinter layer convection heat transfer pressure drop
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