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火焰原子吸收法测定松花粉中铜质量分数的不确定度评定 被引量:3
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作者 屈明华 丁明 费学谦 《东北林业大学学报》 CAS CSCD 北大核心 2008年第1期43-44,72,共3页
通过火焰原子吸收法对松花粉中铜质量分数重复测定6次,并做标准添加,计算实验标准差、回收率等,从而阐明了铜质量分数测量不确定度的评定步骤和评定方法,归纳提出了影响松花粉中铜质量分数测量不确定度的主要因素和不确定度分量的主要... 通过火焰原子吸收法对松花粉中铜质量分数重复测定6次,并做标准添加,计算实验标准差、回收率等,从而阐明了铜质量分数测量不确定度的评定步骤和评定方法,归纳提出了影响松花粉中铜质量分数测量不确定度的主要因素和不确定度分量的主要来源为样品制备过程消化样品所带来的不确定度,并且给出了相对标准不确定度分量,得出了松花粉中铜质量分数测量不确定度的评定结果。本实验不确定度的评定可以体现出消化过程是分析测试松花粉中铜质量分数需要特别关注的步骤。 展开更多
关键词 铜质量分数 不确定度 评定 原子吸收法
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A new manufacture method of backfill samples in lab——Illustrated with a case study 被引量:1
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作者 杜坤 李夕兵 殷志强 《Journal of Central South University》 SCIE EI CAS 2013年第4期1022-1028,共7页
The differences between the formation processes of lab backfill samples and field backfill were analysed. An improved sampling mold, containing an outer box shell and inner sampling mold, was put forward. The new and ... The differences between the formation processes of lab backfill samples and field backfill were analysed. An improved sampling mold, containing an outer box shell and inner sampling mold, was put forward. The new and traditional test molds were applied to make subsequent-backfill samples of Yong-ping Copper Mine. The observation of mass fraction and theory analysis of settlement and distribution of tailing particles were carried out. The research results show that the magnitude of the strength of the backfill forming in new mold is lower than that of backfill forming in traditional mold, and the biggest gap amounts to 36%. 展开更多
关键词 subsequent backfilling SETTLEMENT distribution of particle strength
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