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硅酸钠对胶结膏体充填材料凝结性能的影响机制 被引量:3
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作者 焦华喆 吴爱祥 +1 位作者 容苡 刘晓辉 《硅酸盐通报》 CAS CSCD 北大核心 2015年第11期3303-3307,3314,共6页
膏体充填材料的缓凝事故严重影响资源的有效回采。本文针对会泽矿全尾砂-水淬渣胶结膏体充填物料缓凝问题,开展多因素均匀实验,研究材料凝固、强度性能的影响规律及权重。回归分析表明,随着水玻璃单耗的增加(水泥重量的2%~12%),膏体... 膏体充填材料的缓凝事故严重影响资源的有效回采。本文针对会泽矿全尾砂-水淬渣胶结膏体充填物料缓凝问题,开展多因素均匀实验,研究材料凝固、强度性能的影响规律及权重。回归分析表明,随着水玻璃单耗的增加(水泥重量的2%~12%),膏体凝结时间减少。对于凝结时间影响权重最大的因素为灰砂比(18.6%),其次为水玻璃单耗(5.1%)。水玻璃单耗的增加能够促进膏体强度的提高,但影响权重较小(仅为4.6%),决定充填体强度的因素仍为灰砂比(57.1%)。当膏体配比为全尾砂∶水淬渣∶水泥=7∶1∶1,浓度为78%~80%,水玻璃单耗3%~4%时,膏体凝结时间为8.2~12.5 h,28 d强度为2.33~2.76 MPa,符合膏体充填工艺的要求。 展开更多
关键词 硅酸钠 胶结膏体 缓凝事故 影响机制
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石灰石粉对胶结膏体充填材料性能的影响 被引量:5
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作者 郑娟荣 谷迪 赵雪飞 《金属矿山》 CAS 北大核心 2016年第1期193-196,共4页
为满足矿山对质优价廉、不同粒度分级尾砂胶结充填材料的需求,以粗、细两种分级尾砂胶结充填材料为对象,研究了外掺粗、细、超细石灰石粉对胶结充填材料性能的影响。结果表明:固体质量浓度为65%的细粒尾砂胶结充填料和固体质量浓度... 为满足矿山对质优价廉、不同粒度分级尾砂胶结充填材料的需求,以粗、细两种分级尾砂胶结充填材料为对象,研究了外掺粗、细、超细石灰石粉对胶结充填材料性能的影响。结果表明:固体质量浓度为65%的细粒尾砂胶结充填料和固体质量浓度为75%的粗粒尾砂胶结充填料外掺15%的超细石灰石粉,均可制成胶结膏体充填材料,其充填料的坍落度均超过200mm、脱水率均低于2%、28d硬化体的抗压强度在0.3~1.2MPa、28d硬化体沉缩率均低于2%;继续增加超细石灰石粉的掺量,充填料的坍落度和脱水率下降,28d硬化体的抗压强度略有提升、沉缩率进一步下降。如何提高28d硬化体的抗压强度是今后研究的重点。 展开更多
关键词 胶结膏体充填材料 石灰石粉 坍落度 脱水率 抗压强度 沉缩率
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尾矿膏体胶结充填料的微观结构和力学性能研究 被引量:1
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作者 陈莉薇 高莉 +2 位作者 夏楚林 马明英 党君 《硅酸盐通报》 CAS CSCD 北大核心 2016年第6期1861-1866,共6页
以低含硫量尾矿(含硫量约为0.49wt%)为主要成分,同时添加粘结剂(普通硅酸盐水泥)和絮凝剂(聚合氯化铝)制备尾矿膏体胶结充填料,并通过淋滤实验确定了粘结剂和絮凝剂配比。采用XRD、SEM-EDS、BET等分析方法,对膏体胶结充填料的微观结构... 以低含硫量尾矿(含硫量约为0.49wt%)为主要成分,同时添加粘结剂(普通硅酸盐水泥)和絮凝剂(聚合氯化铝)制备尾矿膏体胶结充填料,并通过淋滤实验确定了粘结剂和絮凝剂配比。采用XRD、SEM-EDS、BET等分析方法,对膏体胶结充填料的微观结构和力学性能进行了深入研究。结果表明,絮凝剂的添加不仅大大地降低了粘结剂的添加量,而且改善了充填料的力学性能和耐水性。随着粘结剂和絮凝剂添加量的增加,尾矿膏体胶结充填料的比表面积逐渐增大,无侧限抗压强度也随之增大。养护龄期为28 d时,絮凝剂添加量为100 g/L的尾矿膏体胶结充填料的强度均达到2 MPa以上,能够达到满足矿山采空区回填要求。 展开更多
关键词 尾矿 充填 渗滤液 微观 无侧限抗压强度
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架间底板拖管充填采空区浆液流动特性试验研究
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作者 成云海 王旭东 +1 位作者 申昊 黄国栩 《煤炭工程》 北大核心 2024年第2期99-104,共6页
为解决矿山充填与煤炭开采之间时空干涉难题,实现矿井安全、高效充填开采。结合李家壕矿井生产系统和开采条件,提出采空区架间底板拖管非胶结膏体充填技术。为确保该技术可行及充填参数的有据可依,遂建立非胶结膏体架间底板拖管充填采... 为解决矿山充填与煤炭开采之间时空干涉难题,实现矿井安全、高效充填开采。结合李家壕矿井生产系统和开采条件,提出采空区架间底板拖管非胶结膏体充填技术。为确保该技术可行及充填参数的有据可依,遂建立非胶结膏体架间底板拖管充填采空区物理模型,以矸石和粉煤灰为骨料制备非胶结膏体充填材料,分析最大粒径和质量浓度对浆液采空区内流动特性的交互影响。研究结果表明:①浆液充填量主要受矸石粒度的影响,质量浓度主要影响浆液在采空区内的扩散速度;②随着浆液充填量的增加,采空区内的空隙逐渐趋于饱和,且渗透方式呈现出以管口为球心的半球形扩散分布;③模拟试验揭示了浆液中矸石颗粒在采空区流动扩散阻塞机理;④沿管道走向依次剖开断面,浆液中矸石级配和质量浓度有明显的分选性。 展开更多
关键词 架间底板拖管 胶结膏体 流动特性 配比参数
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Evaluation of time-dependent rheological properties of cemented paste backfill incorporating superplasticizer with special focus on thixotropy and static yield stress 被引量:4
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作者 WANG Xiao-lin WANG Hong-jiang +3 位作者 WU Ai-xiang JIANG Hai-qiang PENG Qing-song ZHANG Xi 《Journal of Central South University》 SCIE EI CAS CSCD 2022年第4期1239-1249,共11页
Superplasticizers are widely used to reduce the pipe flow resistance of cemented paste backfill(CPB), which is characterised by high concentration and high yield stress. This study aimed to assess the time-dependent r... Superplasticizers are widely used to reduce the pipe flow resistance of cemented paste backfill(CPB), which is characterised by high concentration and high yield stress. This study aimed to assess the time-dependent rheological properties of CPB containing superplasticizer, with special focus on static yield stress and thixotropy. The results indicate that with the increase of the superplasticizer dosage, the static yield stress, dynamic yield stress and thixotropy of CPB decreased significantly, while the plastic viscosity decreased slightly. The curing time has a significant effect on the static yield stress, dynamic yield stress and thixotropy of CPB containing superplasticizer, which increase by 46.6%-87.1%,15.2%-35.6% and 79.4%-138.2%, respectively, within 2 h. The static yield stress, dynamic yield stress and thixotropy of CPB without superplasticizer only increase by 4.9%, 6.3% and 16.1%, respectively, within 2 h. The curing time has a significant influence on the plastic viscosity of CPB regardless of superplasticizer addition, the plastic viscosity increases by 13.2%-19.7% within 2 h. Regardless of superplasticizer dosage, plotting of both static yield stress and dynamic yield stress versus thixotropy produces clearly linear curves. The findings of this study are conducive to the design of pipe transportation of CPB containing superplasticizer. 展开更多
关键词 cemented paste backfill SUPERPLASTICIZER curing time yield stress THIXOTROPY
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Paste-like cemented backfilling technology and rheological characteristics analysis based on jigging sands 被引量:1
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作者 魏冲 王新民 +1 位作者 张云海 张钦礼 《Journal of Central South University》 SCIE EI CAS CSCD 2017年第1期155-167,共13页
To make backfilling body meet strength requirement,physical-chemical evaluation and proportioning tests were conducted on several backfilling materials.Jigging sands,#32.5 cement and fly ash were determined as backfil... To make backfilling body meet strength requirement,physical-chemical evaluation and proportioning tests were conducted on several backfilling materials.Jigging sands,#32.5 cement and fly ash were determined as backfilling aggregate,binding material and modified material,respectively.An optimized proportion of backfilling materials with a solid mass fraction of 78%and cement:fly ash:jigging sands mass ratio of 1:2:14,was suggested to Jiangan Pyrite Mine,China.The slurry made by optimized proportion produced obvious shear thinning phenomena,and was confirmed as paste-like slurry.To analyze its rheological characteristics,L-type pipeline test and Haake VT550 rotational viscometer test were conducted.Bingham and Casson fluid models were applied to several paste-like slurry samples to simulate flow and stress states;Casson fluid model was proved to have better simulation effect on paste-like slurry with shear thinning phenomena;rheological parameters of backfilling slurry made by suggested proportion were measured.Initial yield stress,average apparent viscosity and limiting viscosity are 55.35 Pa,1.216 Pa-s and 0.48 Pa-s,respectively.Compared with Bingham fluid model,Casson fluid model has a better simulation effect on paste-like slurry with shear thinning phenomena,through calculating the residual standard deviations. 展开更多
关键词 paste-like slurry jigging sands shear thinning Casson fluid model backfilling system
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