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基于ICP-AES的膨润土胶体浓度分析方法 被引量:1
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作者 翟秀芳 李伟平 +3 位作者 王煜 徐辉 张瑞荣 韩小元 《光谱学与光谱分析》 SCIE EI CAS CSCD 北大核心 2016年第S1期455-456,共2页
介绍了一种利用发射光谱测量胶体浓度的方法。研究了利用膨润土胶体的主要骨架元素定量胶体浓度的可行性和基于ICP-AES分析膨润土胶体浓度的方法。结果表明,采用HNO3-HF混合溶液浸泡的预处理方法可溶出绝大多数骨架元素;胶体含量与Si含... 介绍了一种利用发射光谱测量胶体浓度的方法。研究了利用膨润土胶体的主要骨架元素定量胶体浓度的可行性和基于ICP-AES分析膨润土胶体浓度的方法。结果表明,采用HNO3-HF混合溶液浸泡的预处理方法可溶出绝大多数骨架元素;胶体含量与Si含量相关性较差,Mn的含量较低,不确定度大,而Fe和Al可作为膨润土胶体浓度检测的基准元素,其浓度与胶体浓度呈现良好的线性关系;样品的Fe/Al测量比值与荧光光谱分析法一致;加入内标元素Ni则显著提升了测量精度。 展开更多
关键词 ICP-AES 胶体浓度 膨润土 FE AL
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胶体浓度对粒径的分布及ξ电势的影响
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作者 楼台芳 朱琳娜 +2 位作者 桂雪梅 夏春兰 吴玲 《广西师范大学学报(自然科学版)》 CAS 2003年第z1期268-269,共2页
论文作者讨论了Fe(OH)3胶体浓度对胶粒粒径的分布、ξ电势及聚沉值的影响.实验数据表明,胶体浓度增加,平均粒径、电势及聚沉值均变小.用水解法制备的胶体粒径分布不均,胶体不稳定,粒径测定的误差很大.
关键词 胶体浓度 粒径分布 ξ电势 聚沉值
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Quantitative investigation on micro-parameters of cemented paste backfill and its sensitivity analysis 被引量:12
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作者 LIU Lang ZHOU Peng +2 位作者 FENG Yan ZHANG Bo SONG Ki-il 《Journal of Central South University》 SCIE EI CAS CSCD 2020年第1期267-276,共10页
The mechanical properties of cemented paste backfill(CPB) depend heavily on its pore structural characteristics and micro-structural changes. In order to explore the variation mechanisms of macro-mechanical characteri... The mechanical properties of cemented paste backfill(CPB) depend heavily on its pore structural characteristics and micro-structural changes. In order to explore the variation mechanisms of macro-mechanical characteristics and micro-structure of CPB. CPB specimens with different mass concentrations prepared from the full tailings of Xianglushan Tungsten Ore were micro-tests. Moreover, acquired pore digital images were processed by using the pores(particles) and cracks analysis system(PCAS), and a sensitivity analysis was performed. The results show that as the mass concentration of CPB increases from 70% to 78%, the porosity, the average pore area and the number of pores drop overall, leading to a decline in the pores opening degree and enhancing the mechanical characteristics. As the mass concentration of CPB increases, the trend of fractal dimension, probability entropy and roundness is reduced, constant and increased, which can result in an enhancement of the uniformity, an unchanged directionality and more round pores. According to the definition of sensitivity, the sensitivities of various micro-parameters were calculated and can be ranked as porosity > average pore area > number of pores > roundness > fractal dimension > probability entropy. 展开更多
关键词 cemented paste backfill mass concentration sensitivity analysis micro-parameters
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A novel approach to investigate effect of magnetic field on dynamic properties of natural rubber based isotropic thick magnetorheological elastomers in shear mode
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作者 Sriharsha Hegde Katari Kiran K V Gangadharan 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第7期2612-2619,共8页
The preparation of natural rubber based isotropic thick magnetorheological elastomers(MRE) was focused on by varying the percentage volume concentration of carbonyl iron powder and developing a test set up to test the... The preparation of natural rubber based isotropic thick magnetorheological elastomers(MRE) was focused on by varying the percentage volume concentration of carbonyl iron powder and developing a test set up to test the dynamic properties. Effect of magnetic field on the damping ratio was studied on the amplification region of the transmissibility curve. The viscoelastic dynamic damping nature of the elastomer was also studied by analyzing the force-displacement hysteresis graphs. The results show that MR effect increases with the increase in magnetic field as well as carbonyl iron powder particle concentration. It is observed that softer matrix material produces more MR effect. A maximum of 125% improvement in the loss factor is observed for the MRE with 25% carbonyl iron volume concentration. FEMM simulation shows that as carbonyl iron particle distribution becomes denser, MR effect is improved. FEMM analysis also reveals that if the distance between the adjacent iron particles are reduced from 20 μm to 10 μm, a 40% increase in stored energy is observed. 展开更多
关键词 magnetorheological elastomer natural rubber carbonyl iron powder(CIP) dynamic analysis
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