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压力及扩散反应对非晶Fe-Mo-Si-B结晶粒度的影响
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作者 刘力 姚斌 +1 位作者 苏文辉 魏连昌 《吉林大学自然科学学报》 CAS CSCD 1998年第2期63-65,共3页
在780~930K,3~6GPa条件下,研究Al与非晶(Fe0.99,Mo0.01)78Si9B13(FMSB)界面扩散反应对非晶FMSB结晶粒度的影响.结果表明,有界面反应的非晶FMSB晶化的α-Fe固溶体的晶粒尺寸小于纯非晶FMSB晶化的α-Fe固溶体,并随Al含量的... 在780~930K,3~6GPa条件下,研究Al与非晶(Fe0.99,Mo0.01)78Si9B13(FMSB)界面扩散反应对非晶FMSB结晶粒度的影响.结果表明,有界面反应的非晶FMSB晶化的α-Fe固溶体的晶粒尺寸小于纯非晶FMSB晶化的α-Fe固溶体,并随Al含量的增加而减小. 展开更多
关键词 扩散反应 结晶粒度 压力 FMSB 非晶态合金
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甘氨酸亚铁结晶粒度和均匀性研究 被引量:1
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作者 杨佳 余润兰 +4 位作者 姚亚军 彭红星 余肇璟 曾伟民 刘学端 《饲料工业》 北大核心 2016年第14期54-57,共4页
试验研究搅拌速度、添加晶种、降温速度等因素对甘氨酸亚铁结晶粒度和均匀度的影响。结果表明:搅拌速度很大程度地影响晶体粒度及均匀度;添加晶种的结晶粒度是自然结晶粒度的5倍左右,乙醇结晶的粒度是自然结晶粒度的1.5~2倍,且二者的... 试验研究搅拌速度、添加晶种、降温速度等因素对甘氨酸亚铁结晶粒度和均匀度的影响。结果表明:搅拌速度很大程度地影响晶体粒度及均匀度;添加晶种的结晶粒度是自然结晶粒度的5倍左右,乙醇结晶的粒度是自然结晶粒度的1.5~2倍,且二者的结晶粒度更大,均匀性更好;降温速度越快,晶体粒度越小,粒径分布越集中。 展开更多
关键词 甘氨酸亚铁 搅拌速度 降温速度 结晶粒度
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精炼糖连续结晶在联合吉达糖业的应用经验 被引量:1
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作者 A.S.Vawda A.E.Muneef M Voelling 《广西蔗糖》 2011年第4期42-51,共10页
为当其它大多数单元操作已成为连续操作时,精炼糖厂的煮糖大多还在使用间歇罐设备。立式连续煮糖罐自2007年起在吉达联合糖业得以成功地运行。由于两种系统同时在使用,因而可以比较间歇和连续运行情况。总而言之,连续工艺比间歇工艺具... 为当其它大多数单元操作已成为连续操作时,精炼糖厂的煮糖大多还在使用间歇罐设备。立式连续煮糖罐自2007年起在吉达联合糖业得以成功地运行。由于两种系统同时在使用,因而可以比较间歇和连续运行情况。总而言之,连续工艺比间歇工艺具有以下优点:装置利用率高;较高的运行和节能效率;较简单的工艺操作。本论文着重论述吉达连续结晶装置基于下述条件的性能表现:1.设计特点;2.传热和传质;3.运行经验;4.结晶粒度分布;5.糖质量;6.积垢和聚糖;7.仪表和控制。 展开更多
关键词 连续煮糖罐 精炼糖 结晶粒度分布 传热系数 分散系数 过饱和
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共沉淀法制备纳米羟基磷灰石 被引量:4
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作者 石和彬 钟宏 +3 位作者 刘羽 田兴 顾金燕 杨昌盛 《化学与生物工程》 CAS 2012年第8期16-20,共5页
以硝酸钙、磷酸混合水溶液为前驱体,以氨水为沉淀剂,采用共沉淀法制备纳米羟基磷灰石。探讨了加料方式、加料速度、Ca-P溶液初始浓度、陈化温度、陈化时间以及反应pH值等工艺条件对纳米羟基磷灰石的结晶粒度与分散性的影响。结果表明,... 以硝酸钙、磷酸混合水溶液为前驱体,以氨水为沉淀剂,采用共沉淀法制备纳米羟基磷灰石。探讨了加料方式、加料速度、Ca-P溶液初始浓度、陈化温度、陈化时间以及反应pH值等工艺条件对纳米羟基磷灰石的结晶粒度与分散性的影响。结果表明,采用将氨水加入Ca-P溶液、快速加料的方式,在Ca2+浓度为1.0mol.L-1、陈化温度为60℃、陈化时间为12h、反应pH值为10的条件下可高效制备分散性较好的短棒状纳米羟基磷灰石粉体。 展开更多
关键词 纳米羟基磷灰石 共沉淀 加料方法 结晶粒度 分散性
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Strength criterion for crystalline rocks considering grain size effect and tensile-compressive strength ratio
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作者 ZHANG Cheng-han JI Hong-guang +3 位作者 JIANG Peng YOU Shuang GENG Qian-cheng JIAO Chen-jiang 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第7期2365-2378,共14页
The macroscopic mechanical properties of rocks are significantly influenced by their microstructure.As a material bonded by mineral grains,the grain morphology of crystalline rock is the primary factor influencing the... The macroscopic mechanical properties of rocks are significantly influenced by their microstructure.As a material bonded by mineral grains,the grain morphology of crystalline rock is the primary factor influencing the strength.However,most strength criteria neglect the strength variations caused by different grain characteristics in rocks.Furthermore,the traditional linear criteria tend to overestimate tensile strength and exhibit apex singularity.To address these shortcomings,a piecewise strength criterion that considers the grain size effect has been proposed.A part of an ellipse was employed to construct the envelope of the tensive-shear region on the meridian plane,to accurately reproduce the low tensile-compressive strength ratio.Based on the analysis of experimental data,both linear and exponential modification functions that account for grain size effects were integrated into the proposed criterion.The corresponding finite element algorithm has been implemented.The accuracy and applicability of the proposed criterion were validated by comparing with the experimental data. 展开更多
关键词 crystalline rock grain size effect strength criterion tensile-compressive strength ratio finite element algorithm
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用“冷分解-筛分法”生产氯化钾的新工艺研究 被引量:5
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作者 陈默 沙作良 《无机盐工业》 CAS CSCD 北大核心 2021年第1期65-67,共3页
针对目前国内盐化工企业生产氯化钾的主要生产工艺存在的不足与可改进方面,开发研究了"冷分解-筛分法"新工艺,节约投入,避免浮选剂的残留。实验结果表明,察尔汗盐湖和大浪滩盐湖光卤石原矿粒径大于0.246 mm,常温分解后,固相... 针对目前国内盐化工企业生产氯化钾的主要生产工艺存在的不足与可改进方面,开发研究了"冷分解-筛分法"新工艺,节约投入,避免浮选剂的残留。实验结果表明,察尔汗盐湖和大浪滩盐湖光卤石原矿粒径大于0.246 mm,常温分解后,固相中氯化钾的粒径集中在0.1 mm左右,通过优选筛分目数,发现在使用0.246 mm的标准筛进行振动湿筛分时,氯化钾取得率为81.0%,氯化钠分离率为88.8%,溶解在分解液中的氯化钠为6.6%,取得最优结果。实验证明了"冷分解-筛分法"新工艺的可行性。 展开更多
关键词 光卤石矿 氯化钾 冷分解-筛分法 结晶粒度
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Simulation of dynamic recrystallization for aluminium alloy 7050 using cellular automaton 被引量:4
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作者 黄始全 易幼平 刘超 《Journal of Central South University》 SCIE EI CAS 2009年第1期18-24,共7页
The prediction of microstructure evolution plays an important role in the design of forging process. In the present work, the cellular automaton (CA) program was developed to simulate the process of dynamic recrystall... The prediction of microstructure evolution plays an important role in the design of forging process. In the present work, the cellular automaton (CA) program was developed to simulate the process of dynamic recrystallization (DRX) for aluminium alloy 7050. The material constants in CA models, including dislocation density, nucleation rate and grain growth, were determined by the isothermal compress tests on Gleeble 1500 machine. The model of dislocation density was obtained by linear regression method based on the experimental results. The influences of the deformation parameters on the percentage of DRX and the mean grain size for aluminium alloy 7050 were investigated in details by means of CA simulation. The simulation results show that, as temperature increases from 350 to 450 ℃ at a strain rate of 0.01 s?1, the percentage of DRX also increases greatly and the mean grain size decreases from 50 to 39.3 μm. The mean size of the recrystallied grains (R-grains) mainly depends on the Zener-Hollomon parameter. To obtain fine grain, the desired deformation temperature is determined from 400 to 450 ℃. 展开更多
关键词 aluminium alloy 7050 dynamic recrystallization cellular automaton
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Effect of ultrasonic power and casting speed on solidification structure of 7050 aluminum alloy ingot in ultrasonic field 被引量:21
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作者 张立华 余军 张晓明 《Journal of Central South University》 SCIE EI CAS 2010年第3期431-436,共6页
With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting... With the experiment and finite element simulation, the influences of power ultrasonic on the solidification structure of 7050 aluminum alloy ingot in semi-continuous casting were researched, and the effects of casting speed on solidification structure in ultrasonic field were also analyzed. The experiment and simulation results show that the solidification structure of the ingot is homogeneously distributed, and its grain size is obviously refined at ultrasonic power of 240 W. The average grain sizes, which can be seen from the Leica microscope, are less than 100 μm. When the casting speed is 45-50 mm/min, the best grain refinement is obtained. 展开更多
关键词 7050 aluminum alloy ultrasonic power casting speed semi-continuous casting solidification structure
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