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高HA含量的PEKK/HA复合材料的制备及其力学相容性 被引量:1
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作者 厉从雷 包黎凤 +2 位作者 吴健 董明建 张祥成 《材料科学与工程学报》 CAS CSCD 北大核心 2019年第2期205-209,218,共6页
本研究合成了一种由高分子聚醚酮酮(PEKK)和羟基磷灰石(HA)组成的复合材料,其中部分HA被PEKK包裹,制得的PEKK/HA复合材料中HA的质量分数达到50%,与人体骨骼中HA的含量相近。该复合材料中HA在PEKK中分布均匀,无明显的相分离现象,模量为14... 本研究合成了一种由高分子聚醚酮酮(PEKK)和羟基磷灰石(HA)组成的复合材料,其中部分HA被PEKK包裹,制得的PEKK/HA复合材料中HA的质量分数达到50%,与人体骨骼中HA的含量相近。该复合材料中HA在PEKK中分布均匀,无明显的相分离现象,模量为14.5GPa,硬度为0.5GPa,断裂屈服强度为167.65MPa,此三项力学性能均与人体骨骼的性能接近。 展开更多
关键词 聚醚酮酮 羟基磷灰石 力学相容 纳米压痕性
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Mechanical heterogeneity characterization of coal materials based on nano-indentation experiments
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作者 ZHANG Qi LI Xiang-chun +3 位作者 LI Biao MENG Jun-qing NIE Bai-sheng LU Wei-dong 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第9期3142-3155,共14页
To investigate the complex macro-mechanical properties of coal from a micro-mechanical perspective,we have conducted a series of micro-mechanical experiments on coal using a nano-indentation instrument.These experimen... To investigate the complex macro-mechanical properties of coal from a micro-mechanical perspective,we have conducted a series of micro-mechanical experiments on coal using a nano-indentation instrument.These experiments were conducted under both dynamic and static loading conditions,allowing us to gather the micro-mechanical parameters of coal for further analysis of its micro-mechanical heterogeneity using the box counting statistical method and the Weibull model.The research findings indicate that the load–displacement curves of the coal mass under the two different loading modes exhibit noticeable discreteness.This can be attributed to the stress concentration phenomenon caused by variations in the mechanical properties of the micro-units during the loading process of the coal mass.Consequently,there are significant fluctuations in the micro-mechanical parameters of the coal mass.Moreover,the mechanical heterogeneity of the coal at the nanoscale was confirmed based on the calculation results of the standard deviation coefficient and Weibull modulus of the coal body’s micromechanical parameters.These results reveal the influence of microstructural defects and minerals on the uniformity of the stress field distribution within the loaded coal body,as well as on the ductility characteristics of the micro-defect structure.Furthermore,there is a pronounced heterogeneity in the micromechanical parameters.Furthermore,we have established a relationship between the macro and micro elastic modulus of coal by applying the Mori-Tanaka homogenization method.This relationship holds great significance for revealing the micro-mechanical failure mechanism of coal. 展开更多
关键词 nano-indentation experiment MICROMECHANICS heterogeneity characterization COAL
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Mechanical properties of 3D carbon/carbon composites by nanoindentation technique 被引量:5
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作者 WEI Li-ming ZHANG Yue +2 位作者 XU Cheng-hai QI Fei MENG Song-he 《Journal of Central South University》 SCIE EI CAS 2012年第1期36-40,共5页
Nanoindentation tests were conducted to investigate the near-surface mechanical properties of the individual components(fiber and matrix) for three-dimensional reinforced carbon/carbon composites(3D C/C).Optical micro... Nanoindentation tests were conducted to investigate the near-surface mechanical properties of the individual components(fiber and matrix) for three-dimensional reinforced carbon/carbon composites(3D C/C).Optical microscope and polarizing light microscope were used to characterize the microstructure of 3D C/C.The microscopy results show that large number of pores and cracks exist at both bundle/matrix interface and pitch carbon matrix.These defects have important effect on the mechanical behavior of 3D C/C.The in situ properties for components of 3D C/C were acquired by nanoindentation technique.Relative to the matrix sample,the fiber samples have more larger values for modulus,stiffness and hardness.However,there is no significant difference of modulus and stiffness among fiber samples with different directions. 展开更多
关键词 C/C composites mechanical properties NANOINDENTATION MICROSTRUCTURE
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